Data Keadaan Ruang

Hari ke-1 Hari ke-2

Parameter
Awal Akhir Awal Akhir
Suhu (⁰C) 26.7 27.5 27 26.2
Tekanan (mBar) 959 958 960 959

Kalibrasi Termometer
Percobaan Literatur
Jenis Termometer
Tb (˚C) Td (˚C) Tb (˚C) Td (˚C)
Termometer Alkohol 200 ⁰C 2 96 0 98.5
Termometer Raksa 200 ⁰C 0 98 0 98.5

Kalibrasi Piknometer
Massa Massa
Massa
Piknomet Piknomet
Piknomet
Massa Piknometer kosong (g) er + er + mA (g) mM (g) mA (kg) mM (kg)
er kosong
Aquadest Metanol
(g)
(g) (g)
11.4182 21.7002 11.9455 19.0656 10.2820 7.1201 0.0103 0.0071

Kalibrasi Refraktometer
Indeks Bias Interpolasi Indeks bi
Nama Zat Rata-rata Literatur
1 2 3 Suhu
Aquadest 1.330 1.330 1.330 1.330 1.332 34.50
Benzene 1.488 1.485 1.483 1.486 1.492 35.00
54.34

Penentuan Indeks Bias Campuran dengan Fraksi mol Methanol

Massa
Massa Massa Botol
Botol Botol Kosong + Massa Massa
Botol Cuplikan Kosong Aquades+ nA (mol) nm (mol)
Kosong
+Aquades Metanol Aquadest Metanol
(gr)
(gr) (gr)
1 13.2736 18.1483 18.1483 4.8747 0.0000 0.2708 0.0000
2 13.5007 17.8667 18.1070 4.3660 0.2403 0.2426 0.0075
3 13.2311 17.1045 17.6680 3.8734 0.5635 0.2152 0.0176
4 13.4163 16.7425 17.8090 3.3262 1.0665 0.1848 0.0333
5 13.0742 15.8681 17.4184 2.7939 1.5503 0.1552 0.0484
6 13.2465 15.5066 17.3910 2.2601 1.8844 0.1256 0.0589
7 13.3563 15.0650 17.3361 1.7087 2.2711 0.0949 0.0710
8 12.7827 13.9796 16.6420 1.1969 2.6624 0.0665 0.0832
9 13.3365 14.1159 17.0515 0.7794 2.9356 0.0433 0.0917
10 13.7819 14.2131 17.5412 0.4312 3.3281 0.0240 0.1040
11 13.7052 13.7052 17.4179 0.0000 3.7127 0.0000 0.1160
 K u r v a K a l i b r a si T er m o m et er A l k o h o l 200⁰C
120

100
f(x) = 1.02559652928417 x
R² = 0.999566160520607

T literatur (ºC)
80

60

40

20

0
0 20 40 60 80 100 120
T percobaan (ºC)

ρA (g/ml) ρM (g/ml) V (ml)

KALIBRASI REFRAKT
0.9970 0.6904 10.3129 1.550

1.500
f(x) = 1.00285830519799 x
Interpolasi Indeks bias 1.450 R² = 0.999997978829022
benzene aquadest
Axis Title
1.400
1.4922 1.3318
1.4919 1.3317 1.350
1.4791 1.3287
1.300

1.250
1.320 1.340 1.360 1.380 1.400 1.42
𝜂
xm Rata-rata Koreksi Axis Title
1 2 3
0.0000 1.332 1.331 1.331 1.331 1.333
0.0300 1.333 1.333 1.332 1.332 1.334
0.0756 1.335 1.333 1.335 1.334 1.336 KURVA INDEX BIAS TER
0.1528 1.337 1.337 1.338 1.337 1.339
0.2379 1.339 1.338 1.339 1.339 1.340 1.345
0.3193 1.339 1.339 1.339 1.339 1.341
0.4278 1.338 1.338 1.338 1.338 1.340
0.5558 1.335 1.336 1.336 1.336 1.337 1.340
0.6793 1.333 1.333 1.333 1.333 1.335
0.8128 1.330 1.330 1.330 1.330 1.332
1.0000 1.326 1.327 1.326 1.326 1.328 1.335
INDEX BIAS

1.330

1.325
INDEX BIA
1.330

1.325

1.320
0.0000 0.2000 0.4000

FR
o l 200⁰C Kur va Kal i br as i Te r mome t e r A i r R aks a
200⁰C
120

100
f(x) = 1.00510204081633 x
T literatur (ºC)
80 R² = 1

60

40

20

0
100 120 0 20 40 60 80 100 120
T percobaan (ºC)

ALIBRASI REFRAKTOMETER

) = 1.00285830519799 x
= 0.999997978829022

40 1.360 1.380 1.400 1.420 1.440 1.460 1.480 1.500

Axis Title

KURVA INDEX BIAS TERHADAP FRAKSI METANOL

0.2000 0.4000 0.6000 0.8000 1.0000 1.2000

FRAKSI METANOL