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HASIL PENGAMATAN SPEKTROFOTOMETRI UV-Vis

a. Catat Identitas sampel

Nama Sampel Bentuk Komposisi No. Batch Exp. date

(pabrik) Sediaan

Kesetaraan bahan aktif : ...................................................................................

...............................................................................................................................

b. Penimbangan Larutan Standar Induk ..............................

Standar 1 =..............................mg

Standar 2 =..............................mg

Standar 3 =..............................mg

c. Perhitungan Konsentrasi Standar Induk (ppm)

Standar Induk 1 =...........................................................................ppm

Standar Induk 2 =............................................................................ppm

Standar Induk 3 =............................................................................ppm

Pengenceran Larutan Standar Induk (SI)

Standar 1

.......ml/....... ml dari SI .........ppm

 Standar 2

.......ml/....... ml dari SI .........ppm

Standar 3

.......ml/....... ml dari SI .........ppm

Standar 4

.......ml/....... ml dari SI .........ppm

Standar 5

.......ml/....... ml dari SI .........ppm

d. Penimbangan sampel .................................

Penimbangan berat tablet/kapsul sebanyak 10 tablet/kapsul Sampel

……………….. Sampel ………………..

Rata – rata berat kapsul / tablet Rata – rata berat kapsul / tablet
= ................... = ...........................

Rata2 berat kapsul kosong = ............ Rata2 berat kapsul kosong = ............

Berat Isi kapsul = ...................... Berat Isi kapsul = ......................

*Penimbangan/pemipetan sampel
Sampel ............................

Replikasi 1 =.............................................mg/ ml

Replikasi 2 =.............................................mg/ ml

Replikasi 3 =.............................................mg/ ml

Sampel ..............................

Replikasi 1 =.............................................mg/ ml

Replikasi 2 =.............................................mg/ ml

Replikasi 3 =.............................................mg/ ml

*coret yang tidak perlu

e. Perhitungan Konsentrasi Sampel Teoritis

Sampel ............................

Replikasi 1 =........................................................................ppm

Replikasi 2 =........................................................................ppm

Replikasi 3 =........................................................................ppm

Sampel ..............................

Replikasi 1 =........................................................................ppm

Replikasi 2 =........................................................................ppm

Replikasi 3 =........................................................................ppm

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f. Kondisi Analisis

a. Panj Gelombang Pengamatan : ……………………………………..

b. Pelarut : ……………………………………..

g. Kadar Sampel

% rekoveri kadar sampel = Konsentrasi hasil percobaan X 100%

Konsentrasi hasil perhitungan teoritis

% rekoveri kadar sampel...............................

Replikasi 1 =

Replikasi 2 =

Replikasi 3 =

% rekoveri kadar sampel..........................rata-rata =

% rekoveri kadar sampel...............................

Replikasi 1 =

Replikasi 2 =

Replikasi 3 =

% rekoveri kadar sampel..........................rata-rata =

h. Kesimpulan

% rekoveri kadar sampel (..............................) = memenuhi /tidak memenuhi syarat

% rekoveri kadar sampel (..............................) = memenuhi /tidak memenuhi syarat