Pembuatan Silika Xerogel dari

Sekam Padi dengan Metode

Asidifikasi
Kelompok 8:
1. Muhammad Aji Pangestu 17031010045
2. Yoshafat Abia Sudarso 17031010086
 Agenda
Latar Belakang 01 Style
Tinjauan Pustaka 02
Diagram Alir 03
Kesimpulan 04
Latar Belakang
Indonesia merupakan negara agraris, dimana padi
merupakan hasil utama dalam sektor pertanian. Sebagai
salah satu negara produsen beras terbesar di kawasan
Asia Tenggara tidak dipungkiri bahwa limbah pertanian
yang dihasilkan cukup melimpah, salah satunya berupa
sekam padi. Dari proses penggilingan padi biasanya
diperoleh sekam padi sekitar 20-30% bobot awal gabah.

Sekam padi memiliki banyak potensi yang dapat

dikembangkan, salah satunya adalah pembuatan
silika xerogel.
Abu Sekam Padi
Sekam padi merupakan pelindung terluar dari padi (Oryza Sativa). Dari proses
penggilingan dihasilkan sekam banyak 20 - 30%. Sekam padi juga mengandung
unsur anorganik berupa abu dengan kandungan utamanya adalah silika 94 - 96%.
Selain itu juga terdapat komponen lain seperti kalium, kalsium, besi, fofat dan
magnesium. Komposisi anorganik dari abu sekam padi berbeda, tergantung dari
kondisi geografis, tipe padi dan tipe pupuk yang digunakan.

Molekul Komposisi
SiO2 96,34%

K2O 2,3%

MgO 0,45%
Al2O3 0,41%

CaO 0,41%
Fe2O 0,2%
Silika Gel
Silika gel merupakan gel kaku yang terdiri dari unit
SiO4 tetrahedral. Silika gel dapat dimanfaatkan sebagai
adsorben dan katalis karena luas permukaannya yang
tinggi. Silika gel dapat dimanfaatkan sebagai adsorben,
katalis, fasa diam pada kolom kromatografi, bahan
tambahan dalam pembuatan cat, dan merupakan produk
yang aman digunakan untuk menjaga kelembaban
makanan, kosmetik, maupun obat-obatan.
Ekstraksi
Indonesia merupakan negara agraris, dimana padi
merupakan hasil utama dalam sektor pertanian. Sebagai
salah satu negara produsen beras terbesar di kawasan
Asia Tenggara tidak dipungkiri bahwa limbah pertanian
yang dihasilkan cukup melimpah, salah satunya berupa
sekam padi. Dari proses penggilingan padi biasanya
diperoleh sekam padi sekitar 20-30% bobot awal gabah.
 Faktor - Faktor yang Mempengaruhi Proses Ekstraksi Silika
Kadar silika dalam bahan
semakin besar kadar silika dalam bahan
semakin besar kandungan silika dalam
produk natrium silika
Temperatur
semakin tinggi temperatur ekstraksi
waktu ekstraksi akan berjalan lebih
cepat dan silika yang larut juga lebih
besar
Waktu ekstraksi
semakin lama waktu ekstraksi silika
yang terekstraksi semakin besar dan
pada kondisi tertentu akan mencapai
titik konstan
Ukuran partikel silika
semakin kecil ukuran partikel silika
waktu ekstraksi akan semakin cepat
dan sebaliknya
 Diagram Alir
Abu
Abu Sekam
Sekam Padi
Padi
100
100 gram
gram

NaOH
NaOH 22 N
N Ekstraksi
2000
2000 mL
mL 100oC , 60 menit

Filtrasi Residu
Residu

Natrium
Natrium Silika
Silika

Air
Air Pengenceran
Demineralisasi
Demineralisasi

C
C22H
H22O
O44 Asidifikasi
0,5
0,5 NN Hingga pH = 4

Aging

Air
Air Pencucian

Pengeringan Pada
Suhu Kamar (T = 27oC)

Silika
Silika Xerogel
Xerogel
Reaksi yang Terjadi
1. Reaksi pada saat ekstraksi silika dengan NaOH
SiO2 + 2NaOH Na2SiO3 + H2O

2. Reaksi pada saat ekstraksi silika dengan NaOH

 Kesimpulan
Sintesis silika gel dari sodium silikat dilakukan dengan cara mencampur sodium
silikat dengan asam oksalat sehingga diperoleh asam silikat. Selanjutnya dilakukan
proses aging untuk penguatan jaringan dan meningkatkan kekakuan gel. Tahap akhir
adalah pengeringan yang bertujuan untuk menghilangkan pelarut sehingga diperoleh
gel kering.
K
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