Melter ( M-01)

Tugas : meleburkan bahan baku phenol

Jenis : Tangki berpengaduk dilengkapi steam jacket
kondisi operasi : Tekanan = 1 atm, Suhu 132 405 K
T lebur = 115 C
388 K
T ruang = 30 C
303 K

m
Kapasitas bahan baku tiap jam untuk proses = 5,650 kg/jam
Volume yang dibutuhkan untuk padatan = 2.79408419 m^3

Volume yang dibutuhkan cairan = 199027828 ml

199.027828 m^3
Panas peleburan sulfur, HL = 1727 kJ/mol 412.47668 kcal/mol
Panas Spesifik solid, Cp,s = 2.4036E+01 J/mol.K 5.7408E-03 kcal/mol.K
Panas spesifik cair, Cp,l = 4.5189E+01 J/mol.K 1.0793E-02 kcal/mol.K

Diambil design untuk Volume Tangki = 3.35290103 m^3

belum termasuk Vol. Head

Panas yang diperlukan = 7.2950E+07 kcal/jam

2.8948E+08 Btu/jam

Estimasi awal,
ambil waktu tinggal,t= 30 menit

Volume cairan = 99.5139137704 m^3

Over design 120% = 119.4166965244 m^3 4217.161 ft^3

Ambil L/D = 3
V =phi/4*D^2*L
D= 3.7013320444 m 12.14348 ft
tinggi, Z= 11.1039961333 m

Ambil, panjang paddle agitator,

L = 0,4 * D
L= 4.8573911344 ft
tebal (vertikal) h= 0.6939130192 ft L/7 ????

Speed dari agitator

ambil N= 250 rpm T=
15000 rev/jam
 Rho = 1.770697117 lb/ft^3 DATA K (W/m k)
k= 0.076319 Btu/hr ft F A
Cp = 1.09 Btu/lb/F -0.1271
miu = 56606.66 lb/ft/jam dibenerin lg miu nya
DATA MIU
Re j = L^*N*rho/miu A
11.0706765 326.3558
fig.20.3, Kern
j= 1400 =hj*Dj/k *(c*miu/k)^(-1/3)*(miu/miu w)^(-0,14)
didapat,
hj = 820.6116126 btu/jam/ft^2/F
Untuk Steam dlm Jacket,
hoi = 1500 btu/jam/ft^2/F
maka,
Uc = hoi*hj/(hoi+hj)
530.4280183 btu/jam/ft^2/F
Rd = 0.005
1/Ud = 1/Uc + Rd
Ud = 145.2375881

Perhitungan untuk Bottom berupa elliptical dished head,

A = phi*Dj*Z + phi/4 * Dj^2
1504.870671 ft^2
Q = Ud*A*delT
DelT = 1324.482178 F
saturated steam,
Tc1 = 86 F Th = 190 F
Tc2 = 269.6 F

Jadi Suhu Steam yg digunakan pada T = 190 F

Hf, pada T = 190 F = 984.1 btu/lb

Kebutuhan Steam = 2.9416E+05 lb/j

miu = 56606.66 kg/m/men

Re = 11.0706765

Dt/Di = 3
ZL/Di = 0.4

Dari gambar 477 brown, dipakai marine propeller 3 blade

Pitch = 0m jumlah baffle = 4
Wi/Di = 0.1 , maka W= 0m
teta = 0.8

P = teta*N^3*Di^5*rho/550/gc
= 6.287690115 hp

Power total = 2*P*0,9

11.31784221 hp
pakai motor standar = 1 hp
APAINI.XLSC

rho Liq
T
rho Liq
C sulfur
CP sulfur
liq
solid

Rho L pada 323

Komp rho ref T ref Tc
kg/m^3 K K
kmol H2O 998.714 293 647.3
176.570875 kmol/j Phenol 1059 313 694.2
2794.08419 dm^3
Rho L = 1048.802 kg/m^3

199027.828 dm^3 rhosukfur padat Eq : Y = A + BT

12889.8963 kcal/kg A B
1.7940E-01 kcal/kg.K 66.073 -0.00711
0.33728531 kcal/kg.K 63.19454 kmol/m3

405 K
DATA K (W/m k) Y= A +BT + CT2 +DT3+ET4
B C K (w/m k) btu/hr ft F
0.000938 -7.37E-07 0.1320 0.076319

DATA MIU Pa.s

B C D miu (cP) lb/ft j
-5.54E+04 -6.08E-01 3.72E-04 2.34E+04 56606.66

323

3.5765398 cp
0.0357654 g/cm/det
C K
132 405
A B n Tc rho (g/ml) rho (kg/m^3)
0.20468 0.1044 0.114 1313 0.028389337 28.38934
A B C D CP
108.05 -2.3743E-01 2.2729E-04 -5.9964E-08 4.5189E+01 Cp (J/mol.K) = A
2.003 1.2002E-01 -1.6202E-04 2.4036E+01 Cp (J/mol.K) =A+B

K
B dv/m v/m rho i mi/rho i
1/K kg/m^3
0.001002 3.0089388E-05 0.001031377 969.57752382 0.011655113
0.000956 9.0253734E-06 0.000953312 1048.9740421 5.375697813
5.387352927

T = T operasi
PERANCANGAN MELTER

Tugas = meleburkan sulfur sebagai umpan di furnace

kondisi operasi =
P= 1 atm
T= 132 C 405 K

umpan sulfur = 5650.202 kg/j

T umpan = 30 C 303 K

1. neraca panas umpan ke melter

T ref = 25 C

komponenm mol cp x dT Q = m cp dT
S 5650.202 176.5688