Bimbingan Teknis Pengelolaan Limbah B3

“Uji Karakteristik & Pengujian

Limbah B3 lainnya”

PT. Syslab (Integrated Lab Services)

3 Desember 2013, Hotel Utami
MATERI PRESENTASI :

1 Tujuan Presentasi

2 Dasar Hukum Pengujian Limbah B3

3 Identifikasi dan Uji Limbah B3

4 Pengujian Terhadap Lahan Terkontaminasi

5 Pengujian Emisi Incenerator (Isokinetik Method 5)

6 Laboratorium Lingkungan PT. Syslab

7
Pengalaman Kerja Study Lingkungan
TUJUAN PRESENTASI

1. Mengetahui regulasi mengenai limbah B3 yang berkaitan dengan

Laboratorium Penguji Lingkungan.
2. Mengetahui karakteristik dan pengujian yang dilakukan oleh
Laboratorium Penguji Lingkungan.
3. Mengetahui sekilas mengenai teknik sampling, teknik preparasi dan
analisis limbah B-3 atau tanah/sedimen terkontaminasi B3.
4. Mengetahui sekilas mengenai TBT (Trial Burner Test) untuk emisi
insenerator.
5. Dasar Laboratorium Lingkungan Beroperasi di Indonesia
DASAR HUKUM

• UU RI No. 32 / 2009 ttg “Perlindungan dan Pengelolaan Lingkungan Hidup”.

• PP RI No. 18 / 1999 Jo. PP No. 85 / 1999 ttg “Pengelolaan Limbah B3”
• PP RI No. 27 /1999 ttg “Analisis Mengenai Dampak Lingkungan”.
• Permen LH No. 30/2009 ttg Tata Laksana Perizinan dan Pengawasan
Pengelolaan Limbah B3 serta Pengawasan Pemulihan Akibat Pencemaran
Limbah B3 oleh Pemda
• Permen LH No. 33 Tahun 2009 ttg “Tata Cara Pemulihan Lahan Terkontaminasi
Limbah B3”.
• Permen LH No. 02/2008 ttg Pemanfaatan Limbah B3
• Permen LH No. 06/2009 ttg Laboratorium Lingkungan
• Kepdal 01/BAPEDAL/09/1995 ttg “ Tata Cara & Persyaratan Teknik Penyimpanan
& Pengumpulan Limbah B3”
• Kepdal 02/BAPEDAL/09/1995 ttg “Dokumen Limbah B3”.
• Kepdal 03/BAPEDAL/09/1995 ttg Persyaratan teknis pengolahan LB3
• Kepdal 04/BAPEDAL/09/1995 ttg Tata Cara Penimbunan Hasil Pengolahan
Limbah B3
• Kepdal 05/BAPEDAL/09/1995 ttg “Simbol dan Label Limbah B3”.
1. IDENTIFIKASI DAN UJI LIMBAH B3
IDENTIFIKASI & UJI LIMBAH B3
LIMBAH B3 DIIDENTIFIKASIKAN BERDASARKAN :

Uji
Sumbernya Karakteristik

Limbah Test Lindi

Karakteristik
B3 TCLP

LD 50/LC 50
Toxicity Acute, Sub
Choric and
Chronic

Sumber : PP No.85, Article I/6, 1999

IDENTIFIKASI & UJI LIMBAH B3
Tidak
LAMPIRAN I
PP 85 / 99
Tidak
Mudah
Mudah Mudah
Mudah
Meledak Terbakar
Ya Meledak Terbaka
Ya Beracun
r
Infeksius
Infeksius
Reakti
Reaktif Korosif
Korosi
f f
LIMBAH LIMBAH
B3  BMTCLP TCLP Test
Lampiran II PP 85/1999
< BMTCLP
 50 mg / kg BB
LD 50
> 50 mg/kg BB
Ya
Sifat Kronis
Lampiran III PP 85/1999

Tidak
Sumber Presentasi : Bpk. Iyan S - KLH LIMBAH Non B3
IDENTIFIKASI & UJI LIMBAH B3

Sumber :
KEPALA BADAN PENGENDALIAN DAMPAK LINGKUNGAN KEP–03/BAPEDAL/09/1995
TENTANG PERSYARATAN TEKNIS PENGOLAHAN LIMBAH BAHAN BERBAHAYA DAN BERACUN
PENGUJIAN TERHADAP LAHAN
TERKONTAMINASI
PENGUJIAN TERHADAP LAHAN
TERKONTAMINASI

Lahan Terkontaminasi

Suvei Lahan Terkontaminasi Limbah B3

Penentuan Lokasi Titik Sampling Lahan

Limbah B3

Kegiatan Pemulihan Lahan Terkontaminasi

Limbah B3

Penentuan Tingkat Keberhasilan Pemulihan

Lahan B3

SSPLT
(Surat Status Penyelesaian Lahan Terkontaminasi)

SUMBER : Permen LH No. 33 Tahun 2009

PENGUJIAN TERHADAP LAHAN TERKONTAMINASI
Typical Sample
Analysis Distribution : Sample

Wet
VOC SVOC Chemis Metals
try

40 ml/10g 1 L/30g Various 250ml/10g

Internal Surrogate
Standard &
1. Colorimetric Digestion
Surrogate
Addition 2. Gravimetric
Additions 3. Spectrophotometric
4. Titrimetric AA or ICP
Extraction
GC/MS or 5. others Analysis
GC Analysis
GC/MS or
GC Analysis Sumber : Kepdal 04/BAPEDAL/09/1995 ttg Tata
Cara Penimbunan Hasil Pengolahan Limbah B3
PENGUJIAN TERHADAP LAHAN TERKONTAMINASI

Sampling activities :

Picture 1. Sampling Soil and Underground Water

PENGUJIAN TERHADAP LAHAN TERKONTAMINASI

Sampling activities :

Picture 2. Containers
PENGUJIAN TERHADAP LAHAN TERKONTAMINASI

VOC, S-VOC Metals Analyses

PENGUJIAN TRIAL BURNED TEST
(ISOKINETIC METHOD 5)
PENGUJIAN EMISI INSENERATOR
(ISOKINETIC METHOD 5)

Sampling Isokinetic :
Melibatkan pengumpulan polutan yang memiliki
energi kinetik (biasanya ada sebagai bentuk
partikulat & uap).

Untuk mendapatkan sampel yang representatif

aliran gas yang mengandung partikel padat atau cair,
sampel harus ditarik dari sumber emisi sehingga
kecepatan dan arah memasuki gas sampling nozzel
adalah sama dengan gas dalam saluran pada titik
sampling.

Acuan Pengujian :
NOMOR: KEP-205/BAPEDAL/07/1996 TENTANG PEDOMAN TEKNIS PENGENDALIAN
PENCEMARAN UDARA SUMBER TIDAK BERGERAK

Acuan Nilai Ambang Batas :

NOMOR: KEP–03/BAPEDAL/09/1995 TENTANG PERSYARATAN TEKNIS PENGOLAHAN
LIMBAH BAHAN BERBAHAYA DAN BERACUN
PENGUJIAN EMISI INSENERATOR
(ISOKINETIC METHOD 5)

Dalam US Code of Federal Reference (CFR) 40 Part 60 Appendix A, terdapat lima

Metode dasar:

1. USEPA Method 1: Pemilihan lokasi dan pengambilan titik sampel dan traverse
(sampling) point
2. USEPA Method 2: Penentuan kecepatan gas cerobong dan volume laju alir
3. USEPA Method 3: Penentuan berat molekul kering
4. USEPA Method 4: Penentuan kadar air pada gas cerobong
5. USEPA Method 5: Penentuan emisi partikulat dari sumber tidak bergerak
PENGUJIAN EMISI INSENERATOR
(ISOKINETIC METHOD 5)

Rencana Trial Burn terdiri dari 5 elemen utama:

1. Analisis limbah
• Screening test
• Variasi dalam senyawa-senyawa ini dan dalam
semua komposisi limbah.
• Seleksi POHC untuk analisis.
• Kandungan abu (non-combustible) dari limbah
harus ditentukan.
• Pengukuran kadar C, H, S, N, P dan O serta
kadar air dari limbah yang diumpankan
diperlukan untuk menghitung kebutuhan
udara dan udara lebih (excess air).
• Pengukuran khlorida dalam limbah diperlukan
untuk menentukan potensi emisi gas hidrogen
khlorida.
PENGUJIAN EMISI INSENERATOR
(ISOKINETIC METHOD 5)

2. Deskripsi enjinering unit

• Dimensi komponen insinerator
• Desain laju udara dan limbah yang
diumpankan
• Sistem penyalur bahan bakar
• Deskripsi alat monitoring secara
kontinyu.

3. Prosedur sampling dan analisis

• Operasi proses monitoring.
• Laju alir udara dan bahan bakar yang
digunakan.
• Komposisi gas di cerobong terkait
dengan POHC, partikulat dan HCl.
PENGUJIAN EMISI INSENERATOR
(ISOKINETIC METHOD 5)

4. Jadwal dan protokol tes

• Tanggal dan durasi trial burn.
• Kuantitas limbah yang akan dibakar
• Kondisi operasi yang direncanakan untuk
masing-masing tes kinerja.

5. Informasi kontrol
• Prosedur untuk menghentikan
pengumpanan limbah.
• Penghentian operasi insinerator.
• Mengontrol emisi ketika peralatan tidak
berfungsi atau keadaan darurat lainnya.
LABORATORIUM LINGKUNGAN
PT. SYSLAB
1. BACKGROUND
The Decree of Ministry of Environment No. 32 – 2009
- The decree is used to protect the Indonesia from pollution and / or
damage to the environment;
- Every citizen has right to know about environmental conditions and
obtain a valid quality information;

Permen 06 tahun 2009 : Laboratorium Lingkungan

• Legal Aspect : Accreditation 17025 (KAN) and
• Registered at Ministry of Environment (KLH);
• A proper Laboratory Facility and supported by competence human
resources.
2. LEGAL ASPECT

• ISO Certified - Environment Laboratory

Testing KAN - ISO 17025 : 2008 No. LP-516-
IDN;
• Registered as Environment Laboratory in
Indonesian Ministry of Environment
(Kementerian Lingkungan Hidup – KLH)
0034/LPJ/LABLING-1/LRK/KLH;
• License form Oil and Gas Directorate
(MIGAS) 0423/SKT-02/DMT/2010;
2. LEGAL ASPECT
2. LEGAL ASPECT
2. LEGAL ASPECT
RUANG LINGKUP JASA PT. SYSLAB :
• Ambient Air Quality • Emission Stack
• Noise • Generator Emission
• Indoor Air Quality • Boiler Emission
• Smell & Odor • Vehicle Emission

INDUSTRY

• Surface Water • B3 Characteristic

• Waste Water • LD50/LC50
• Clean Water • Soil Testing
• Drinking Water
• Raw Water
4. MANAJEMEN LABORATORIUM
b. Proficiency Test for Water Quality

Organizer :
Jaringan Lab Jawa Barat 2012 and PUSARDPEDAL with 65 participants.
 VOC, S-VOC, Organo Halide, PCB, Metals Analyses
Pesticides, BTEX, Methyl Mercaptant
Metals Analyses, Sea Water, Minerals and Alloys
WHO Limits AFR & AMR
 Oil and Gas Industries
CITIC SERAM ENERGY LIMITED
CONOCOPHILIPS INDONESIA
PETROCHINA INTERNATIONAL (JABUNG)
STAR ENERGY
KANGEAN ENERGY
BP TANGGUH
TOTAL INDONESIE
PERTAMINA HULU ENERGY WMO
SCHLUMBERGER
PETROCHINA INTERNATIONAL (BERMUDA)
PERTAMINA HULU ENERGY ONWJ
CNOOC
JOB PERTAMINA - TALISMAN
 Area Jawa Barat Area Jawa Timur
SANYO ALSTOM
Rumah Sakit Cipto Mangunkusumo SC JHONSON
MM2100 (INDUSTRIAL ESTATE) WILMAR NABATI
HOLCIM – CEMENT DUTA CIPTA
PT. BASF – CHEMICAL ETERNIT
ABBOTT – PHARMACY PELITA MEKAR
CAPSUGEL – PHARMACY SALIM IVOMAS
Toyota Motor Manufacture Indonesia (TMMIN) DUPONT AGRICULTURE (SURABAYA)
TAISHO (DEPOK) SINAR KARYA DUTA
INDOCEMENT – HEIDELBERG COMPANY TJIWI KIMIA
ENERGIZER (DEPOK) SANTOS PREMIUM
BAYER (DEPOK) JAPFA COMFEED
ASTRA OTOPART GARUDA FOOD
PEMANFAAT & PENGOLAH LIMBAH B3 RUMAH SAKIT
PLIB (BATAM) RS TEBET
LOGAM JAYA ABADI (WASTE UTILIZER) RSCM
TENANG JAYA SEJAHTERA (WASTE UTILIZER) BAROMEUS (BANDUNG)
DESA AIR CARGO (WASTE UTILIZER) RS. SOETOMO (SURABAYA)
WASTECH RS. PRINGADI (MEDAN)
WPLI KLINIK PASUTRI – BOYKE (BOGOR)
DPLI RSUD ADAM MALIK (MEDAN)
MULTI HANNA RSUD JOGJA (JATENG)
PPLI – (WASTE UTILIZER) RS. PRODIA OHI
GUNA PURNAMA (WASTE UTILIZER) RS. RASUNA MEDICAL CENTER
CV LUT PUTRA SOLDER (WASTE UTILIZER) RSAL RAMELAN (SURABAYA)
PENGALAMAN KERJA
PT. SYSLAB
OUR EXPERIENCE
Environment Baseline Study

Year : 2013
Activity : Baseline Study
Place : Mobil Cepu Limited - REKIN

Objectives:
To obtain environment data (sea water, air ambient, social, noise and
public health)
OUR EXPERIENCE
Noise & Illumination Mapping

Year : 2012 & 2013

Activity : Noise & Illumination Mapping
Place : PPEJ, Pertamina Petrochina East Java – Tuban

Objectives:
To obtain noise data and transferred to map in order to acknowledge
the hazardous area for noise.
OUR EXPERIENCE
Environment Audit

Year : 2013
Activity : Environment Audit for Office Facility, Warehouse, Expatriate
Housing
Place : Premier Oil Jakarta & Batam

Objectives:
Environment audit for Indoor air, Drinking Water, Pool Water.
OUR EXPERIENCE
Case Investigation : Mercury Legally Biding

Year : 2012
Activity : Analis Mercury
Place : PLTU Indonesia & Penambang Emas Tanpa Izin
Objectives:
To analysis Hg from Coal and Stack Emission power plant
OUR EXPERIENCE
Case Investigation : Tailing Sludge

Year : 2012
Activity : Hazardous Waste Characteristic Analysis
Place : Bangka – Belitung
Objectives:
To analysis sludge of mining
OUR EXPERIENCE
Case Investigation : SPBU di Depok

Year : 2012
Activity : Civil Ground Water Polution
Place : Depok – Jawa Barat
Objectives:
To analysis the ground water (to prove quality of ground water)
OUR EXPERIENCE
Case Investigation : Soil Contaminant

Year : 2012
Activity : Land Contamination Analysis
Place : Depok – Jawa Barat
Objectives:
To analysis soil contaminant from Pb (lead)
OUR EXPERIENCE
Environment Audit

Year : 2012
Activity : Air Quality Assessment
Place : PHE WMO – PHE Tower
Objectives:
To analysis the air quality at indoor
OUR EXPERIENCE
TRIAL BURNER TEST

Year : 2012
Activity : TRIAL BURNER TEST
Location : Tenang Jaya Sejahtera
Method :
The first laboratory testing which perform TBT in Indonesia, by using
approved Protocol from KLH (reference US EPA Method 1-5, 6C, 7E, 26,
29 and 30/31). This activity is intended to capture emission from waste
incinerator in accordance with KEP 03 BAPEDAL 1995.
OUR EXPERIENCE
Air Quality Assessment

Year : 2012
Activities : Monitoring of Noise, Respirable Dust, BTX and Welding Fume
Location : Petrochina Blok Jabung

Methods of monitoring
Equipment being used : Noise dosimeter, Personnal Pump, MCEF (Mixed
Cellulise Ester Filter), Cyclone Trap, Activated Charcoal, Dust Filter
OUR EXPERIENCE
Indoor Air Quality

Year : 2011
Activities : Indoor Air Quality
Location : PHE WMO

Methods of monitoring
Using air quality standard sampling equipment
(LVS, Impinger) to generate the measurement data
according to standards.
OUR EXPERIENCE
Noise Assessment

Year : 2011
Activity : Noise Assessment in International Airport
Place : Angkasa Pura I, Djuanda International Airport

Objectives:
To obtain noise data and transferred to map in order to acknowledge the
hazardous area for noise.
OUR EXPERIENCE
Blue Sky Program 2011 & 2012

Year: 2011 & 2012

Activities:
KLH Sponsorship to perform Air Quality Monitoring in 26 cities
with the Ministry of Environment.

Methods:
Air quality sampling was calculated to obtain correlation with
the exhaust emissions from motor vehicle fuel.
OUR EXPERIENCE
PHASE II ENVIRONMENT SITE ASSESSMENT
Contaminated Land Recovery Program

Year : 2011
Activity : Solid Waste Management with KLH
Place : Kerawang, West Java

Methods of monitoring:
Monitoring of solid waste on landfill at Petrochemical company in
Kerawang.
OUR EXPERIENCE
Environmental Study for Waste Management, Handling, and Disposal

Year : 2010
Activity : Use of Oil Sludge
Location : Balongan - Pertamina UP VI

Method :
Sludge as an alternative fuel for cement kilns.
OUR EXPERIENCE
Environmental Study for Waste Management, Handling, and Disposal

Year : 2010
Activity : Handling air quality in Calcium Carbonate industry
Place : Tegal, Central Java

Method :
Air quality management in the calcium carbonate industry
Main Laboratory:
Jl. MH.Thamrin, Plaza Amsterdam
Block D2-D6, Sentul City, Bogor
16810, INDONESIA
Phone: 021-87962155
Fax: 021-87960212

Representatives:
Surabaya Office: Balikpapan Office:
Juanda Bisnis Center Jl.M.R. Iswahyudi No.30
Blok B-2 Surabaya (Gn. Bakaran) – Balikapapan 76114
CONTACT PERSON

Jakarta Office and Bogor Laboratory

1. Oges Susetio : oges.susetio@syslab.co.id (0811-972393)
2. Lurizal Hilabi : lurizal@syslab.co.id (0811941832)
3. M. Taufik : mtaufik@syslab.co.id (0813-14995039)
4. Eri Rustandi : eri.rustandi@syslab.co.id (08111637244)
5. Veralyn Andayani : veralyn@syslab.co.id (08111637229)
6. Arief Setiawan : arief.setiawan@syslab.co.id (08111637228)
7. Wulan : manikam.ratnawulan@syslab.co.id (08111637234)
8. Ayu Puspa : ayu.puspa@syslab.co.id (08111902566)
9. Bita Nenden : bita@syslab.co.id (08111637249)

Surabaya Reps
1. Agung Setiawan : a.setyawan@syslab.co.id (081330640435)
2. Deny Ferlinda : denny.ferlinda@syslab.co.id (08111637240)
3. Yoyok Aryo : yoyok.aryo@syslab.co.id (082131248934)
4. Hendra Agung : hendra.agung@syslab.co.id (08119006609)

Marketing : syslab@syslab.co.id
Website : www.syslab.co.id