Spesifikasi Alat

Tangki 1
Organic Compounds
Densitas = A x B ^ [-(1 - T/Tc)^n], density = g/mL, T = K
Komponen
A B
C6H6 0.3009 0.2677
C7H8 0.29999 0.27108
temperatur 30 C
Komponen Densitas (g/ml) Densitas(lb/cu.ft)

C6H6 0.8680972779 54.1935768637
C7H8 0.8601884774 53.699846265
Densitas campuran (lb/cu.ft)
Volume (cu.ft/jam)
Volume (cu.ft)
V tangki (cu.ft)
d (ft)
H (ft)
Lingkaran Bawah (ft.sq) 5526.7495567726

Tinggi Cairan (ft) _( )=((1)(12))/(2144)+
1118.764818519
Tebal Allowable stress (S/F) (psi) 12650

Ef 0.8
_( )=(_)/(250000 )
Faktor korosi S/Cc (in) 0.125
Tebal tangki (f) 3.2480762723 ft
=(_)/(250000 _( ) )
Tutup Tangki Young 267 conical roof
=/(430_( ) )
tebal tutup (t) 8.4914249726 irwan (in)
0.3902667972 mba fit (ft)
Tangki 2
Organic Compounds
Densitas = A x B ^ [-(1 - T/Tc)^n], density = g/mL, T = K
Komponen
A B
H2O 0.3471 0.274
H2O2 0.43776 0.24982
temperatur 30 C

H2O 0.995647 62.156250916
H2O2 1.4371741224 89.7199061104
Volume (cu.ft/jam)
Volume (cu.ft)
V tangki (cu.ft)
d (ft)
H (ft)
1
Tinggi Cairan (ft) 69.2656552908
Tebal Allowable stress (S/F) 17890

Ef 0.8
Tutup Tangki Young 267 conical

0.1932995031 mba fit (ft)
Tangki 3
temperatur 30 C

H2O 0.995647 62.156250916
tributil 0.976 60.929728
Volume (cu.ft/jam)
Volume (cu.ft)
V tangki (cu.ft)
d (ft)
H (ft)

Tinggi Cairan (ft) 456.3703351509
Tebal Allowable stress (S/F) 12650

Ef 0.8
Tutup Tangki Young 267 conical

0.4245305443 mba fit (ft)
mpounds
^n], density = g/mL, T = K
n Tc
0.2818 562.16
0.29889 591.79
303 K
Fraksi (%) Densitas(lb/cu.ft) Massa (kg/jam) Massa (lbm/jam)

99.8 54.08518971 210674.89711941 464458.091687389
0.2 0.1073996925 422.194182604 930.7777388525
54.1925894025 465388.869426242
8587.6846734482
6183132.9648827
927469.944732405
83.9073613889
167.8147227779
))/(2144)+
young tabel 13.1

young tabel 13.2
timmerhauss hal 542 untuk 10 tahun
99.00136 cm
) )
30 derajat kemiringan 0.5
21.56822 cm
11.89533 cm
mpounds
^n], density = g/mL, T = K
n Tc
0.28571 647.13
0.2877 730.15
303 K

70 43.5093756412 5833.3333333333 12860.2833333333
30 26.9159718331 2500 5511.55
70.4253474743 18371.8333333333
260.8696157308
93913.0616630712
112695.673995685
41.5593931745
83.118786349
young tabel 13.1

young tabel 13.2
25.1377 cm
15.10787 cm
5.891769 cm
303 K

1 0.6215625092 1145.8619112944 2526.1900868778
99 60.32043072 113440.32921814 250092.818600905
60.9419932292 252619.008687782
4145.2370574402
2984570.68135693
1193828.27254277
91.2740670302
182.5481340604
young tabel 13.1

young tabel 13.2
130.5399 cm
23.46182 cm
12.93969 cm
1 g/ml 62.428 (lb/cu.ft)
1 kg 2.20462 lbm
1 bulan 30 hari
1 hari 24 jam
waktu penyimpanan 720 jam H/D 2

SA 283 C
jumlah tangki 8
772891.620610337
26263.1664249875 m3
25.5749637513 m
51.1499275027 m
1 g/ml 62.428 (lb/cu.ft)

1 kg 2.20462 lbm
1 bulan 15 hari
1 hari 24 jam
.
316 L
jumlah tangki 1 al (Mpa) 124
al (psi) 17980
93913.0616630712
3191.2034005358 m3
12.6673030396 m
25.3346060792 m
1 g/ml 62.428 (lb/cu.ft)

1 kg 2.20462 lbm
1 bulan 30 hari
1 hari 24 jam
.
SA 283 C
jumlah tangki 3
994856.893785643
33805.6351935936 m3
27.8203356308 m
55.6406712616 m
Contoh perhitungan spesifikasi alat
A. Perhitungan Tangki Penyimpanan
F. Perhitungan Separator
Separator 01 (S-01)
Tugas : Memisahkan campuran gas dan cairan yang keluar dari hidrogenato
sebanyak 409270.1439 kg/jam
Alat : Silinder vertikal
Perhitungan :
Feed flowrate (F) 409270.1439 kg/jam = 902285.1446
Vapor flowrate (Wv) 61.1232 kg/jam = 134.7535
Liquid flowrate (Wl) 409209.0206 kg/jam = 902150.3911
Kondisi operasi :
T= 50.00 C = 323.15 K
P= 3 atm
R= 0.08206
Komposisi fase gas :
Komposisi kg/jam BM kmol/jam yi yi x BM
H2 61.1232 2.02 30.2590 1 2.02
Total 61.1232 30.2590 1 2.02
pgas = P x BM
RxT
= 3 x 2.02
0.08206 x 323.15
= 0.2285 g/L
= 0.0143 lb/ft3
Volume gas = massa total

p gas total
= 134.7535 lb/jam
0.0143 lb/ft3
= 9444.0552 ft3/jam
Komposisi fase cair :
Komposisi kg/jam BM kmol/jam xi wi
C16H12O2 40514.403 236.28 171.4678 0.0484 0.0990

C12H27PO4 113440.33 265.49 427.2866 0.1206 0.2772
H2O 1145.8619 18.01 63.6236 0.0180 0.0028
C6H6 210674.9 78.12 2696.8113 0.7609 0.5148
C7H8 422.19418 92.15 4.5816 0.0013 0.0010
C16H14O2 43011.335 238.3 180.4924 0.0509 0.1051
Total 409209.0 3544.26331 1.0000 1.0000
p cair = 0.9372 g/cm3
= 58.5157 lb/ft3
Volume cair = massa total
p cair total
= 902150.3911 lb/jam
58.5157 lb/ft3
= 15417.2365 ft3/jam
1 Perhitungan Gas-Liquid separation factor :

f = Wl pv 0.5
x
Wv pl
= 902150.3911 0.0143 0.5
x
134.7535 58.5157
= 104.5427
2 Perhitungan Maximum design vapor velocity :

Dari Fig 5-1 Evans, diperoleh design vapor velocity factor :
Kv = 0.035
Uvmax = pl - pg 0.5
Kv x
pg
= 58.5157 - 0.0143
x
0.0143
= 2.2411 ft/jam
3 Perhitungan Liquid Flowrate :

Ql = Wl
pl
= 902150.3911 lb/jam
58.5157 lb/ft3
= 15417.2365 ft3/jam
Minimum vessel cross sectional area :

Amin liquid = Ql
Uvmax
= 15417.2365 ft3/jam
2.2411 ft/jam
= 6879.3269 ft2
4 Perhitungan Vapor Flowrate :

Qv = Wv
pv
= 134.7535 lb/jam
0.0143 lb/ft3
= 9444.0552 ft3/jam

Amin gas = Qv
Uvmax
= 9444.0552 ft3/jam
2.2411
= 4214.0330 ft2
5 Perhitungan diameter vessel :

Dmin = 4 x Amin

= 4 x 4214.0330 = 878.99270487
= 146.49878415
= 73.249392073 ft dibagi 6
= 22.326414704 m
Diambil ukuran standar dengan pembulatan kelipatan 6 In, D = 24 In
6 Estimasi vapor liquid nozzle

p campuran = 58.5300 lb/ft3
uv max nozzle = 100 p

= 100 58.5300
= 765.048815 ft/jam
uv min nozzle = 60 p
= 60 58.5300
= 459.029289 ft/jam
A = Qv
Uvmin nozzle
= 9444.0552 ft3/jam
459.02928928 ft/jam
= 20.5740 ft2
ID = 4xA

= 4 x 20.5740

= 5.1181630612 ft
= 61.417956734 in
OD = 5.563 in (Appendix F, Brownell)

= 0.4636 ft
Hv = 36 in + 0.5 (Feed Nozzle OD)
= 70.7815 in
= 5.8982 ft
Hv min = 72 in
7 Full Surge Volume
t= 1 menit = 60 s
Ql = Wl
pl
= 902150.3911 lb/jam
58.5157 lb/ft3
= 15417.2365 ft3/jam
= 4.2826 ft3/s
V = Ql x t
= 4.2826 x 60
= 256.9539 ft3/s
Hl = 4
V x
x D^2
= 256.9539 x 4
x D^2
= 10.5718 ft
= 126.8611 in
Melakukan Pengecekan Geometri

Hv + Hl
3< <5
D
Hv + Hl 70.7815 + 126.8611
= = 426.35381402
D 5.563
H = Hv + Hl
= 70.7815 + 126.8611
= 197.6426 in
8 Menghitung Tebal Shell
t Pr
= + c
f x E - 0.1 x P
=
Separator 02 (S-02)
Tugas : Memisahkan campuran gas dan cairan yang keluar dari oksidator
sebanyak 440193.5464 kg/jam
Alat : Silinder vertikal
Perhitungan :
Feed flowrate (F) 440193.5464 kg/jam = 970459.4963
Vapor flowrate (Wv) 25497.5573 kg/jam = 56212.4249
Liquid flowrate (Wl) 414695.9891 kg/jam = 914247.0715
Kondisi operasi :
T= 70.00 C = 343.15 K
P= 1 atm
R= 0.08206
Komposisi fase gas :
Komposisi kg/jam BM kmol/jam yi yi x BM
N2 (79%) 23764.83 28 848.7439 1 28
O2 (21%) 1732.7269 32 54.147715 1 32
Total 25497.56 902.8917 1 60.0000
BM = (BM N2 x %Berat N2) + (BM O2 x %Berat O2)

= (28 x 0.79) + (32 x 0,21)
= 28.84
pgas = P x BM
RxT
= 1 x 28.84
0.08206 x 343.15
= 1.0242 g/L
= 0.0639 lb/ft3
Volume gas = massa total

p gas total
= 56212.4249 lb/jam
0.0639 lb/ft3
= 879038.9433 ft3/jam
Komposisi fase cair :
Komposisi kg/jam BM kmol/jam xi wi
C16H12O2 81028.807 236.28 342.9355 0.0923 0.1954

C12H27PO4 113440.33 265.49 427.2866 0.1150 0.2736
H2O 1145.8619 18.01 63.6236 0.0171 0.0028
C6H6 210674.9 78.12 2696.8113 0.7258 0.5080
C7H8 422.19418 92.15 4.5816 0.0012 0.0010
C16H14O2 2150.5667 238.3 9.0246 0.0024 0.0052
H2O2 5833.3333 34.02 171.4678 0.0461 0.0141
Total 414696.0 3715.7311 1.0000 1.0000
p cair = 0.9465 g/cm3

= 59.0941 lb/ft3
Volume cair = massa total

p cair total
= 914247.0715 lb/jam
59.0941 ft3/jam
= 438157.78874 ft3/jam
1 Perhitungan Vapor-Liquid separation factor :

f = Wl pv 0.5
x
Wv pl
= 914247.07148 0.0614 0.5
x
56212.4249 59.0941
= 0.5244
2 Perhitungan Maximum design vapor velocity :

Dari Fig ... Evans, diperoleh design vapor velocity factor :
Kv = 0.24
Uvmax = pl - pg 0.5
Kv x
pg
= 59.0941 - 0.0614
x
0.0614
= 7.2918 ft/jam
3 Perhitungan Liquid Flowrate :

Ql = Wl
pl
= 914247.0715 lb/jam
59.0941 lb/ft3
= 15471.0509 ft3/jam

Amin liquid = Ql
Uvmax
= 15471.0509 ft3/jam
7.2918
= 2121.6996 ft2
4 Perhitungan Vapor Flowrate :

Qv = Wv
pv
= 56212.4249 lb/jam
0.0639 lb/ft3
= 879038.9433 ft3/jam
Amin gas = Qv
Uvmax
= 879038.9433 ft3/jam
7.2918
= 120551.38491 ft2
5 Perhitungan diameter vessel :

Dmin = 4 x Amin

= 4 x 122983.3471

= 391.77900715 ft = 4701.3480858
= 119.41424138 m
Diambil ukuran standar dengan pembulatan kelipatan 6 In, D = 4704 In
6 Estimasi vapor liquid nozzle

p campuran = 59.1580 lb/ft3
Uv max nozzle = 100 p

= 100 59.1555
= 769.142371 ft/jam
Uv min nozzle = 60 p
= 60 59.1555
= 461.485422 ft/jam
A = Qv
Uvmin nozzle
= 879038.9433 ft3/jam
461.48542238 ft/jam
= 1904.8033 ft2
ID = 4xA

= 4 x 1982.5584

= 49.247039027 ft
= 590.96446833 in
OD = 5.563 in (Appendix F, Brownell)

= 0.4636 ft
Hv = 36 in + 0.5 (Feed Nozzle OD)

= 70.7815 in
= 5.8982 ft
Hv min = 72 in
7 Full Surge Volume
t= 1 menit = 60 s
Ql = Wl
pl
= 914247.0715 lb/jam
59.0941 lb/ft3
= 15471.0509 ft3/jam
= 4.2975 ft3/s
V = Ql x t
= 4.2826 x 60
= 257.8508 ft3/s
Hl = 4
V x
x D^2
= 257.8508 x 4
x D^2
= 10.6087 ft
Melakukan Pengecekan Geometri
Hv + Hl
3< <5
D
Hv + Hl 70.7815 + 10.6087
= = 35.608578446
D 0.4636
eluar dari hidrogenator
lb/jam
lb/jam
lb/jam
pi
pcair
(g/cm3)
1.1223 0.1111
0.9760 0.2706
0.9880 0.0028
0.8478 0.4365
0.8412 0.0009
1.0981 0.1154
0.9372
0.5
in
in
in
eluar dari oksidator
lb/jam
lb/jam
lb/jam
pi
pcair
(g/cm3)
1.1223 0.2193
0.9760 0.2670
0.9880 0.0027
0.8478 0.4307
0.8412 0.0009
1.0981 0.0057
1.4372 0.0202
0.9465
0.5
in
ft
Perhitungan Dimensi Separator 1 (S-0
Densitas campuran liquid (L)
Komponen F (kg/jam) Xi (kg/m3)
C16H12O2 40514.4032921938 0.0990066231 1122.3

C12H27PO4 113440.329218143 0.2772185448 976
H2O 1145.8619112944 0.0028001873 988.037
C6H6 210674.897119408 0.5148344403 847.76
C7H8 422.194182604 0.0010317323 841.17
C16H14O2 43011.3349216663 0.1051084721 1098.1
TOTAL 409209.020645308 1
Perhitungan tebal shell heater dan dimensi ves
Spesifikasi evaporator (heater dan separator) :
Tekanan operasi = 3 atm
Tekanan design = 29.392 psig
Bahan konstruksi = Carbon steel SA-283 grade C
Allowable stress (S) = 12650 psi
Tipe pengelasan = Double welded butt joint
Efisiensi pengelasan (Ef) = 0.8
Corrosion allowance (Cc) = 0.125 in
Jenis separator = Cylindrical vessel
Jenis tutup = Torispherical Head
Tebal shell heater :
t shell = ((P x r)/((S x Ef)-(0.6 x P)))+Cc = 0.181733647
Dimensi dan tebal vessel separator :
Waktu tinggal = 1 min
0.0166666667 jam
QL = 436.6337031507 m3/jam
VL = 7.2772283858 m3
Faktor kelonggaran volume separator (vessel) = 20%
V vessel = 8.732674063 m3
H vessel = 1.5 x D vessel
V vessel = (1/4) x x D^2 x H = 1.1775*D^3
D vessel = (V/1.1775)^(1/3) = 1.950123482
H vessel = 2.9251852224 m 9.596947678
t vessel = ((P x r)/((S x Ef)-(0.6 x P)))+Cc 0.236686122
Dimensi dan tebal head separator :
OD = 76.7755814204 in
Dari tabel 5.7 brownell & young berdasarkan nilai OD dipilih :
OD = 40 in
r= 40 in
icr = 2.5 in
w= (1/4) x (3+((r/icr)^0.5)) = 1.75
t head = ((P x r x w)/((2 x S x Ef) - (0.2 x P)))+Cc =
Dari tabel 5.7 brownell & young dipilih tebal head standar (th) =
ID = OD - (2 x th) = 39.5 in
b= r - (((((r-icr)^2)-(((ID/2)-icr)^2))^0.5) =
Dari tabel 5.6 brownell & young berdasarkan nilai th, maka dipilih Sf :
Sf = 1.5 in
Maka :
Tinggi head (OA) = th + b + Sf = 8.453040679
0.214707663
Perhitungan Dimensi Separator 1 (S-0

Densitas campuran liquid (L)
C16H12O2 81028.8065843748 0.1953932729 1122.3

C12H27PO4 113440.329218143 0.2735505821 976
H2O 1145.8619112944 0.0027631372 977.771
C6H6 210674.897119408 0.5080225096 847.76
C7H8 422.194182604 0.0010180812 841.17
C16H14O2 2150.5667460833 0.0051858875 1098.1
H2O2 5833.3333333333 0.0140665294 1437.174122
TOTAL 414695.98909524 1
Perhitungan tebal shell heater dan dimensi ves

Spesifikasi evaporator (heater dan separator) :
Tekanan operasi = 1 atm
Tekanan design = 0 psig
Bahan konstruksi = Stainless Steel 316 L
Allowable stress (S) = 214 MPa
Tipe pengelasan = Double welded butt joint
Efisiensi pengelasan (Ef) = 0.8
Corrosion allowance (Cc) = 0.125 in
Jenis separator = Cylindrical vessel
Jenis tutup = Flanged standar dished and flanged shallow
Tebal shell heater :
t shell = ((P x r)/((S x Ef)-(0.6 x P)))+Cc = 0.125
Dimensi dan tebal vessel separator :
Waktu tinggal = 1 min
0.0166666667 jam
QL = 438.1709212518 m3/jam
VL = 7.3028486875 m3
Faktor kelonggaran volume separator (vessel) = 20%
V vessel = 8.763418425 m3
H vessel = 1.5 x D vessel
V vessel = (1/4) x x D^2 x H = 1.1775*D^3
D vessel = (V/1.1775)^(1/3) = 1.952409344
H vessel = 2.9286140163 m 9.608196865
t vessel = ((P x r)/((S x Ef)-(0.6 x P)))+Cc 0.125
Dimensi dan tebal head separator :
OD = 76.8655749176 in
Dari tabel 5.7 brownell & young berdasarkan nilai OD dipilih :
OD = 78 in
r= 78 in
icr = 4.75 in
w= (1/4) x (3+((r/icr)^0.5)) = 1.76307245
t head = ((P x r x w)/((2 x S x Ef) - (0.2 x P)))+Cc =
Dari tabel 5.7 brownell & young dipilih tebal head standar (th) =
ID = OD - (2 x th) = 77.625 in
b= r - (((((r-icr)^2)-(((ID/2)-icr)^2))^0.5) =
Dari tabel 5.6 brownell & young berdasarkan nilai th, maka dipilih Sf :
Sf = 1.5 in
Maka :
Tinggi head (OA) = th + b + Sf = 14.83914926
0.376915145
an Dimensi Separator 1 (S-01)
Densitas campuran gas (g)
campuran campuran
(kg/m3) (kg/m3)
111.115133 H2 61.12321 1 0.2285 0.2285267
270.5653
2.76668868
436.456045
0.8678623
115.419613
937.190642 TOTAL 61.12321 1 0.2285267
ell heater dan dimensi vessel separator
44.088 psi
in
m 6.3979651184 ft 76.77558 in
ft 115.1633721306 in
in 0.6011827491 cm
pilih :
0.22668171 in
r (th) = 0.25 in
6.70304068 in
dipilih Sf :
in
m
an Dimensi Separator 1 (S-02)

Densitas campuran gas (g)
campuran
Komponen F (kg/jam) Xi BM %
(kg/m3)
219.28987 N2 23764.83 0.932043 28 79
266.985368 O2 1732.727 0.067957 32 21
2.70171542
430.681163
0.85637935
5.69462306
20.2160521
946.425171 TOTAL 25497.56 1 campuran 1.0242
ell heater dan dimensi vessel separator
14.696 psi
31.03 psi
Brownell tabel 3.2 hal 254
dished and flanged shallow dished heads
in
m 6.4054645765 ft 76.86557 in
ft 115.2983623765 in
in 0.3175 cm
pilih :
0.125 in
r (th) = 0.1875 in
13.1516493 in
dipilih Sf :
in
m
T= 50.00 C = 323.15
P= 3 atm
R= 0.08206
BM H2 2.02
pgas = P x BM
RxT
= 3 x 2.02
0.08206 x 323.15
= 0.2285 g/L
= 0.2285 kg/m3
Spesifikasi shell dan tube

Shell side
Dari tabel 9 kern berdasarkan nilai OD tube, pitch dan jumlah
tube maka dipilih spesifikasi shell :
ID shell = 39 in
Baffle space (B) 10 in
Passes = 1
T= 70.00 C = 343.15
P= 1 atm
R= 0.08206
BM N2 28 % 0.79
BM O2 32 % 0.21
BM Campuran = (BM N2 x %Berat N2) + (BM O2 x %Berat O2)
= (28 x 0.79) + (32 x 0.21)
= 28.84
pgas = P x BM
RxT
= 1 x 28.84
0.08206 x 343.15
= 1.0242 g/L
= 1.0242 kg/m3

Shell side
Dari tabel 9 kern berdasarkan nilai OD tube, pitch dan jumlah
tube maka dipilih spesifikasi shell :
ID shell = 39 in
Baffle space (B) 10 in
Passes = 1
K
Komponen (g/cm3) (kg/m3)
C16H12O2 1.1223 1122.3

C12H27PO4 0.976 976
H2O 0.988037 988.037
C6H6 0.84776 847.76
C7H8 0.84117 841.17
C16H14O2 1.0981 1098.1

Tube side
Dari tabel 10 kern dipilih spesifikasi tube :
Jumlah (Nt) = 1330

Panjang (L) = 20 ft
OD tube = 0.75 in (3/4 in)
BWG = 16
ID tube = 0.62 in
Thickness = 0.065 in
Pitch (PT) = 0.9375 in. triangular (15/16 in)
C" = PT - OD = 0.1875 in
Passes = 2
K
Komponen (g/cm3) (kg/m3)
C16H12O2 1.1223 1122.3

+ (BM O2 x %Berat O2) C12H27PO4 0.976 976
H2O 0.988037 988.037
C6H6 0.84776 847.76
C7H8 0.84117 841.17
C16H14O2 1.0981 1098.1
H2O2 1.437174122 1437.174

Tube side
Dari tabel 10 kern dipilih spesifikasi tube :
Jumlah (Nt) = 1330

Panjang (L) = 20 ft
OD tube = 0.75 in (3/4 in)
BWG = 16
ID tube = 0.62 in
Thickness = 0.065 in
Pitch (PT) = 0.9375 in. triangular (15/16 in)
C" = PT - OD = 0.1875 in
Passes = 2
D. Perhitungan Pompa dan Kompresor
Pompa 1 (P-01)
Fungsi : Mengalirkan benzene dari tangki penyimpanan (T-01)

menuju mixer (M-01)
Jenis : Centrifugal pump
Bahan : Commercial Steel
Kondisi operasi : - Temperatur = 30 C = 303.15
- Tekanan (P1) = 1 atm = 14.696
(P2) = 1 atm = 14.696
Dasar perhitungan :
Rate liquid = 211097.0913 kg/jam = 58.6381
liquid (densitas) = 847.7468 kg/m3 = 52.9230
Viskositas campuran () = (Dari buku Yaws Tabel 22-1 Hal. 482)
Viskositas
Komponen A B C D Xi
(log 10)
C6H6 -7.4005 1181.50 0.0149 0.0000 -0.2500 0.998
C7H8 -5.1649 810.680 0.0105 0.0000 -0.2854 0.002
Total 1.0000
# rumus : log10 n11q = A + B/T + CxT + DxT^2
= 0.0006 kg/m.s
a. Menghitung rate volumetric
rate liquid
Ql =
liquid
211097.091 kg/jam
=
847.7468 kg/m3
= 249.0096 m3/jam
= 2.4427 ft3/s
b. Menghitung ID optimal
ID = 3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496)
= 3.9 x ((2.4427)^0.45 ft3/s) x ((52.9230)^0.13 lbm/ft3)
= 14.0049 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844) = 16

OD 16.0 in 0.4064 m
ID 15.25 in 0.3874 m
Sehingga diperoleh :
Standarisasi ID = OD - ID
= (0.4064 - 0.3874) m
= 0.0191 m
A = ID ^2
x 3.14
2
= 0.3874 m ^2
x 3.14
2
= 0.1178 m2
Dimana :
ID = Inside diameter (in)
OD = Outside diameter (in)
Ql = Rate volumetric (ft3/s)
= Densitas liquid (lbm/ft3)
c. Menentukan friction factor

Kecepatan Linear (V) = Ql
A
= 249.0096 m3/jam
0.1178 m2
= 2114.1671 m/jam
= 0.5873 m/s
= 1.9267 ft/s
NRe = DxVx

= 0.3874 m x 0.5873 m/s x 847.7468 kg/m3
0.0006 kg/m.s
= 21412.565
Nre > 2.100, maka alirannya adalah turbulen
Dimana :
NRe = Bilangan Reynold
D = Diameter (m)
V = Kecepatan linear (m/s)
= Densitas campuran (kg/m3)
= Viskositas (kg/m.s)
= 0.00005 m (Commercial Steel)

D = 0.3874 m
Relative roughness ( r ) =
D
= 0.000046 m
0.3874 m
= 0.0001
f = 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0001 5.74 2
log +
3.7 x 0.3874 21412.565^0.9
= 0.0262
d. Menentukan Head Loss

hf = f x L x V^2
ID x 2g
= 0.0262 x 7.826 m x (0.5873 m/s)^2
0.3874 m x 2 x 9.8 m/s^2
= 0.0093 m
= 0.00000 ft
Dimana :
hf = head loss akibat gesekan (m)
f = friction coefficient
L = panjang pipa (m)
V = laju aliran fluida (m/s)
ID = diameter dalam pipa (m)
g = percepatan gravitasi (m/s2)
kfit = 1.5 ft (1 elbow 90, coulson tabel 5.3 hal. 204)

hfit = kfit V^2 x n
2gc
= 1.5 ft x (1.9267 ft)^2 x 1
2 x 32.2
= 0.0865 ft
Dimana :
hfit = head loss akibat fitting (ft)
kfit = coefficient loss akibat fitting (ft) = 1.5 (1 elbow 90)
V = laju aliran fluida (ft/s)
g = percepatan gravitasi (ft/s^2)
n = jumlah fitting
e. Perhitungan head pompa (Hp)

Hp = 144 x (P2 - P1) + (Z2 - Z1) + (V2^2 - V1^2) +
2g
= 144 x (14.696 - + 10 + 0 + 0.00000
52.9230 14.696) psia
= 10.0865 ft
= 3.0744 m
Dimana :
Hp = head yang dibutuhkan pompa (ft)
hf = head loss akibat gesekan (ft)
= densitas (lb/ft3)
P2 = tekanan pada titik akhir
P1 = tekanan pada titik awal
Z2 = ketinggian pada titik akhir (ft)
Z1 = ketinggian pada titik awal (ft)
V2 = laju aliran fluida pada titik akhir (ft/s)
V1 = laju aliran fluida pada titik awal (ft/s)
g = percepatan gravitasi (ft/s2)
f. Perhitungan daya pompa

HHP = Hp x x Ql
550
= 10.0865 ft x 52.9230 lb/ft3 x 2.4427 ft3/s
550
= 2.37077 hp
= 1767.89 Watt
Dimana :
Hp = Head pompa (ft)
= densitas (lb/ft3)
Q = laju alir volumetrik (ft3/s)
Efisiensi pompa adalah sebesar 75% 0.75

BHP = HHP
E
= 2.3708 hp
0.75
= 3.1610 hp
= 2357.18 Watt
Pompa 5 (P-05)
Fungsi : Mengalirkan air dari utilitas menuju mixer settler (MS-01)

Kondisi operasi : - Temperatur = 30 C = 303.15
- Tekanan (P1) = 1 atm = 14.696
(P2) = 1 atm = 14.696
Dasar perhitungan :
Rate liquid = 20335.60445 kg/jam = 5.6488
liquid (densitas) = 995.6470 kg/m3 = 62.1561
Viskositas
Komponen A B C D Xi
(log 10)
H2O -10.216 1792.50 0.0177 0.0000 -0.0888 1.0000
Total 1.0000
= 0.0008 kg/m.s
rate liquid
Ql =
liquid
20335.6045 kg/jam
=
995.6470 kg/m3
= 20.4245 m3/jam
= 0.2004 ft3/s
ID = 3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496)
= 3.9 x ((0.2004)^0.45 ft3/s) x ((62.1561)^0.13 lbm/ft3)
= 3.2362 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844) = 4

OD 4.5 in 0.1143 m
ID 3.826 in 0.0972 m
= (0.1143 - 0.0972) m
= 0.0171 m
A = ID ^2
x 3.14
2
= 0.0171 m ^2
x 3.14
2
= 0.0074 m2
Dimana :

A
= 20.4245 m3/jam
0.0074 m2
= 2755.019 m/jam
= 0.7653 m/s
= 2.5107 ft/s
NRe = DxVx

= 0.0171 m x 2.5107 m/s x 995.6470 kg/m3
0.0008 kg/m.s
= 90851.116

Dimana :
D = Diameter (m)

D = 0.0972 m
D
= 0.000046 m
0.0972 m
= 0.0005
f = 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0005 5.74 2
log +
3.7 x 0.0972 90851.1164^0.9
= 0.0314

hf = f x L x V^2
ID x 2g
= 0.0314 x 7.826 m x (0.7653 m/s)^2
0.0972 m x 2 x 9.8 m/s^2
= 0.0757 m
= 0.00002 ft
Dimana :

hfit = kfit V^2 x n
2gc
= 0.5 ft x (4.4315 ft)^2 x 3
2 x 32.2
= 0.1468 ft
Dimana :
n = jumlah fitting

Hp = 144 x (P2 - P1) + (Z2 - Z1) + (V2^2 - V1^2) +
2g
= 144 x 0 + 10 + 0 + 0.00002 +
995.647
= 10.1469 ft
= 3.0928 m
Dimana :
= densitas (lb/ft3)

HHP = Hp x x Ql
550
= 10.1469 ft x 62.1561 lb/ft3 x 0.2004 ft3/s
550
= 0.22975 hp
= 171.325 Watt
Dimana :
= densitas (lb/ft3)

BHP = HHP
E
= 0.2298 hp
0.75
= 0.3063 hp
= 228.434 Watt
Pompa 2 (P-02)
Fungsi : Mengalirkan tributil fosfat dari tangki penyimpan

menuju mixer (M-01)
tangki penyimpanan (T-01) Jenis : Centrifugal pump
Kondisi operasi : - Temperatur = 30
- Tekanan (P1) = 1
K (P2) = 1
psia
psia Dasar perhitungan :
Rate liquid = 114586.1911 kg/jam
liquid (densitas) = 976.1965 kg/m3
58.6381 kg/s Viskositas campuran () = (Dari buku Yaws Tabel 22-1 Hal. 482)
52.9230 lb/ft3
Komponen A B C D
Viskositas C12H27PO4 (Dari website pubchem)

Xi
(, cp) H2O -10.216 1792.50 0.0177 0.0000
0.998 0.5612 Total
0.002 0.0010 # rumus : log10 n11q = A + B/T + CxT + DxT^2
1.0000 0.5622 = 0.0034
rate liquid
Ql =
liquid
114586.1911 kg/jam
=
976.1965 kg/m3
= 117.3803 m3/jam
= 1.1515 ft3/s
ID = 3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15
= 3.9 x ((1.1515)^0.45 ft3/s) x ((60.9418)^0.13 lbm/ft3)
& Timmerhaus pers. 15 hal 496) = 7.0903 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844)

OD 8.625 in 0.2191 m
in sch 30 ID 7.625 in 0.1937 m
= (0.2191 - 0.1937) m
= 0.0254 m
A = ID ^2
x 3.14
2
= 0.1937 m ^2
x 3.14
2
= 0.0294 m2
Dimana :

A
= 117.3803 m3/jam
0.0294 m2
= 3986.3760 m/jam
= 1.1073 m/s
= 3.6329 ft/s
NRe = DxVx

= 0.1937 m x 1.1073 m/s x 976.1965 kg/m3
0.0034 kg/m.s
= 62229.7786

Dimana :
D = Diameter (m)
D = 0.1937 m
D
= 0.000046 m
0.1937 m
= 0.0002
f = 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0002 5.74
log +
3.7 x 0.1937 62229.7786^0.9
= 0.0242

hf = f x L x V^2
ID x 2g
= 0.0242 x 7.826 m x (1.1073 m/s)^2
0.1937 m x 2 x 9.8 m/s^2
= 0.0611 m
= 0.00002 ft
Dimana :

hfit = kfit V^2 x n
2gc
= 1.5 ft x (3.6329 ft)^2 x 1
2 x 32.2
= 0.3074 ft
Dimana :
n = jumlah fitting

hf + hfit Hp = 144 x (P2 - P1) + (Z2 - Z1) +

0.00000 + 0.0865 = 144 x (14.696 - + 10
60.942 14.696) psia
= 10.3074 ft
= 3.1417 m
Dimana :
= densitas (lb/ft3)

HHP = Hp x x Ql
550
= 10.3074 ft x 60.9418 lb/ft3 x 1.1515 ft3/s
550
= 1.31508 hp
= 980.654 Watt
Dimana :
= densitas (lb/ft3)

BHP = HHP
E
= 1.3151 hp
0.75
= 1.7534 hp
= 1307.54 Watt
Pompa 6 (P-06)
s menuju mixer settler (MS-01) Fungsi : Mengalirkan larutan recycle dari mixer settler (M
menuju mixer (M-01)
K Bahan : Commercial Steel
psia Kondisi operasi : - Temperatur = 30
psia - Tekanan (P1) = 1
(P2) = 1
5.6488 kg/s Dasar perhitungan :

62.1561 lb/ft3 Rate liquid = 408862.6558 kg/jam
liquid (densitas) = 939.4523 kg/m3
Viskositas Viskositas campuran () = (Dari buku Yaws Tabel 22-1 Hal. 482)
Xi
(, cp)
Komponen A B C D
1.0000 0.8150
1.0000 0.8150 C16H12O2 (Coulson Tabel 8.1 Hal. 317)
C12H27PO4 (Dari website pubchem)
H2O -10.216 1792.50 0.0177 0.0000
C6H6 -7.4005 1181.50 0.0149 0.0000
C7H8 -5.1649 810.68 0.0105 0.0000
C16H14O2 (Coulson Tabel 8.1 Hal. 317)
Total
= 0.0021
rate liquid
Ql =
liquid
& Timmerhaus pers. 15 hal 496) 408862.6558 kg/jam
=
939.4523 kg/m3
= 435.2138 m3/jam
= 4.2693 ft3/s
in sch 80
ID = 3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15
= 3.9 x ((4.2693)^0.45 ft3/s) x ((58.6480)^0.13 lbm/ft3)
= 12.7232 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844)

OD 14 in 0.3556 m
ID 13.25 in 0.3366 m
= (0.3556 - 0.3366) m
= 0.0191 m
A = ID ^2
x 3.14
2
= 0.3366 m ^2
x 3.14
2
= 0.0889 m2
Dimana :

A
= 435.2138 m3/jam
0.0889 m2
= 4894.788 m/jam
= 1.3597 m/s
= 4.4608 ft/s
NRe = DxVx

= 0.3366 m x1.3597 m/s x 939.4523 kg/m3
0.0021 kg/m.s
= 208990.503
Dimana :
D = Diameter (m)

D = 0.3366 m
D
= 0.000046 m
0.3366 m
= 0.0001
f = 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0001 5.74
log +
3.7 x 0.3366 208990.5026^0.9
= 0.0183

hf = f x L x V^2
ID x 2g
= 0.0157 x 7.826 m x (1.3507 m/s)^2
0.3366 m x 2 x 9.8 m/s^2
= 0.0402 m
= 0.00001 ft
Dimana :

hfit = kfit V^2 x n
2gc
= 1.5 ft x (4.4315 ft)^2 x 1
2 x 32.2
= 0.4635 ft
Dimana :
hf + hfit kfit = coefficient loss akibat fitting (ft) = 1.5 (1 elbow 90)
0.1468 g = percepatan gravitasi (ft/s^2)
n = jumlah fitting

Hp = 144 x (P2 - P1) + (Z2 - Z1) +

= 144 x 0 + 10 + 0
939.452
= 10.4635 ft
= 3.1893 m
Dimana :
= densitas (lb/ft3)

HHP = Hp x x Ql
550
= 10.4574 ft x 59.0850 lb/ft3 x 4.2413 ft3/s
550
= 4.76346 hp
= 3552.12 Watt
Dimana :
= densitas (lb/ft3)

BHP = HHP
E
= 4.7647 hp
0.75
= 6.3513 hp
= 4736.16 Watt
Pompa 3 (P-03)
irkan tributil fosfat dari tangki penyimpanan (T-01) Fungsi : Mengalirkan larutan dari mixe
hidrogenasi (R-01)
C = 303.15 K Kondisi operasi : - Temperatur
atm = 14.696 psia - Tekanan
atm = 14.696 psia
Dasar perhitungan :
kg/jam = 31.8295 kg/s Rate liquid =
kg/m3 = 60.9418 lb/ft3 liquid (densitas) =
(Dari buku Yaws Tabel 22-1 Hal. 482) Viskositas campuran () =
Viskositas Viskositas
Xi Komponen A B
(log 10) (, cp)
ari website pubchem) 0.99 3.3561 C16H12O2 (Coulson Tabel 8.1 Hal. 317
-0.0888 0.01 0.0082 C12H27PO4 (Dari website pubchem)
1.0000 3.3643 H2O -10.216 1792.50
A + B/T + CxT + DxT^2 C6H6 -7.4005 1181.50
kg/m.s C7H8 -5.1649 810.680
C16H14O2 (Coulson Tabel 8.1 Hal. 317
Total
# rumus : log10 n11q

rate liquid
Ql =
liquid
408862.6558 kg/jam
=
2491.0365 kg/m3
(Peter & Timmerhaus pers. 15 hal 496) = 164.1335 m3/jam
0.45 ft3/s) x ((60.9418)^0.13 lbm/ft3) = 1.6101 ft3/s
piran Tabel 11. Hal. 844) = 8 in sch 80 ID = 3.9 x Ql^0.45 x ^0.13
= 3.9 x ((1.6101)^0.45 ft3/s) x ((155.510
= 9.3127 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 84
OD 10.75 in 0.2731
ID 9.75 in 0.2477
= (0.2731 - 0.2477) m
= 0.0254
A = ID ^2
x 3.14
2
= 0.2477 m ^2
x
2
= 0.0481 m2
Dimana :

m/jam Kecepatan Linear (V) =
=
=
x 1.1073 m/s x 976.1965 kg/m3 =
0.0034 kg/m.s
NRe = DxVx

= 0.2477 m x 0.9470 m/s x 2491.0
0.0021 kg/m.s
= 284295.792

(Commercial Steel)
Dimana :
D = Diameter (m)
= 0.00005 m
D = 0.2477 m
0.25
5.74 2 Relative roughness ( r )
62229.7786^0.9
f = 0.25
826 m x (1.1073 m/s)^2 r
log
1937 m x 2 x 9.8 m/s^2 3.7 x ID
= 0.25
0.0002
log
3.7 x 0.1937
= 0.0197

hf = f x L x V^2
ID x 2g
= 0.0197 x 7.826 m x (0.9470 m/s)^
0.2477 m x 2 x 9.8 m/s^
= 0.0285 m
w 90, coulson tabel 5.3 hal. 204) = 0.00001 ft
Dimana :
kfit = 0.75 ft (2 elbow 90, coulson ta

hfit = kfit V^2 x n
kibat fitting (ft) = 1.5 (1 elbow 90) 2gc
= 0.75 ft x (3.6329 ft)^2
2 x 32.2
= 0.2248 ft
Dimana :
(V2^2 - V1^2) + hf + hfit kfit = coefficient loss akibat fitting (ft) = 0.75
2g V = laju aliran fluida (ft/s)
+ 0 + 0.00002 + 0.3074 g = percepatan gravitasi (ft/s^2)
n = jumlah fitting

Hp = 144 x (P2 - P1)

= 144 x (44.088 -
155.510 14.696) psia
= 37.4414 ft
= 11.4121 m
Dimana :
= densitas (lb/ft3)
ft x 60.9418 lb/ft3 x 1.1515 ft3/s V1 = laju aliran fluida pada titik awal (ft/s)
550 g = percepatan gravitasi (ft/s2)
HHP = Hp x x Ql
550
= 37.4414 ft x 155.5100 lb/ft3 x 1
550
= 17.045 hp
= 12710.5 Watt
0.75 Dimana :
= densitas (lb/ft3)
Efisiensi pompa adalah sebesar 75%

BHP = HHP
E
= 17.045 hp
0.75
= 22.7267 hp
= 16947.3 Watt
Pompa 7 (P-07)
irkan larutan recycle dari mixer settler (MS-01) Fungsi : Mengalirkan destilat dari men
menuju tempat pengolahan l
C = 303.15 K Kondisi operasi : - Temperatur
atm = 14.696 psia - Tekanan
atm = 14.696 psia
Dasar perhitungan :
Rate liquid =
kg/jam = 113.5730 kg/s liquid (densitas) =
kg/m3 = 58.6480 lb/ft3 Viskositas campuran () =
(Dari buku Yaws Tabel 22-1 Hal. 482)
Komponen A B
Xi
(log 10) (, cp) H2O -10.216 1792.50
son Tabel 8.1 Hal. 317) 0.1982 0.7927 Total
ari website pubchem) 0.27745 0.9406 # rumus : log10 n11q
-0.0888 0.0028 0.0023
-0.2500 0.51527 0.2897 a. Menghitung rate volumetric
-0.2854 0.0010 0.0005 rate liquid
Ql =
son Tabel 8.1 Hal. 317) 0.00526 0.0311 liquid
1.0000 2.0570 17835.6045 kg/jam
=
A + B/T + CxT + DxT^2 958.3650 kg/m3
kg/m.s = 18.6105 m3/jam
= 0.1826 ft3/s
ID = 3.9 x Ql^0.45 x ^0.13
= 3.9 x ((0.1826)^0.45 ft3/s) x ((59.8286
= 3.0881 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 84

OD 4.5 in 0.1143
(Peter & Timmerhaus pers. 15 hal 496) ID 3.826 in 0.0972
0.45 ft3/s) x ((58.6480)^0.13 lbm/ft3)
= (0.1143 - 0.0972) m
= 0.0171
piran Tabel 11. Hal. 844) = 14 in sch 30 A = ID ^2
x 3.14
2
= 0.0171 m ^2
x
2
= 0.0074 m2
Dimana :

Kecepatan Linear (V) =
=
=
=
NRe = DxVx

= 0.0171 m x 0.6973 m/s x 958.3
0.0008 kg/m.s
= 79682.145
m/jam
Dimana :
D = Diameter (m)
x1.3597 m/s x 939.4523 kg/m3 = Densitas campuran (kg/m3)
0.0021 kg/m.s = Viskositas (kg/m.s)
= 0.00005 m
D = 0.0972 m
Relative roughness ( r )
f = 0.25
r
log
3.7 x ID
= 0.25
0.0005
log
3.7 x 0.0972
= 0.0316
(Commercial Steel)
hf = f x L x V^2
ID x 2g
= 0.0316 x 7.826 m x (0.6973 m/s)^
0.0972 m x 2 x 9.8 m/s^
= 0.0631 m
= 0.00002 ft
Dimana :
0.25 L = panjang pipa (m)
5.74 2 V = laju aliran fluida (m/s)
208990.5026^0.9 ID = diameter dalam pipa (m)
kfit = 0.15 ft (10 elbow 90, coulson t

hfit = kfit V^2 x n
2gc
826 m x (1.3507 m/s)^2 = 0.15 ft x (2.2877 ft)^2
3366 m x 2 x 9.8 m/s^2 2 x 32.2
= 0.1219 ft
Dimana :
kfit = coefficient loss akibat fitting (ft) = 0.5
n = jumlah fitting
w 90, coulson tabel 5.3 hal. 204) e. Perhitungan head pompa (Hp)
Hp = 144 x (P2 - P1)

= 144 x 0
958.365
= 10.1219 ft
= 3.0852 m
kibat fitting (ft) = 1.5 (1 elbow 90) Dimana :

= densitas (lb/ft3)
(V2^2 - V1^2) + hf + hfit P1 = tekanan pada titik awal
2g Z2 = ketinggian pada titik akhir (ft)
+ 0.00001 + 0.4635 Z1 = ketinggian pada titik awal (ft)

HHP = Hp x x Ql
550
= 10.1219 ft x 59.8286 lb/ft3 x 0.
550
= 0.2010 hp
= 149.894 Watt
Dimana :
= densitas (lb/ft3)
Efisiensi pompa adalah sebesar 75%

BHP = HHP
E
ft x 59.0850 lb/ft3 x 4.2413 ft3/s = 0.2010 hp
550 0.75
= 0.2680 hp
= 199.859 Watt
0.75
Pompa 4 (P-04)
Mengalirkan larutan dari mixer (M-01) menuju reaktor Fungsi

hidrogenasi (R-01)
Centrifugal pump Jenis
Commercial Steel Bahan
Temperatur = 30 C = 303.15 K Kondisi operasi
Tekanan (P1) = 1 atm = 14.696 psia
(P2) = 3 atm = 44.088 psia
Dasar perhitungan
408862.6558 kg/jam = 113.5730 kg/s Rate liquid
2491.0365 kg/m3 = 155.5100 lb/ft3 liquid (densitas)
(Dari buku Yaws Tabel 22-1 Hal. 482) Viskositas campuran ()
C D Xi Komponen
(log 10) (, cp)
(Coulson Tabel 8.1 Hal. 317) 0.1980 0.7919 C16H12O2
(Dari website pubchem) 0.27718 0.9396 C12H27PO4
0.0177 0.0000 -0.0888 0.0028 0.0023 H2O
0.0149 0.0000 -0.2500 0.51476 0.2895 C6H6
0.0105 0.0000 -0.2854 0.0010 0.0005 C7H8
(Coulson Tabel 8.1 Hal. 317) 0.00525 0.0311 C16H14O2
0.9990 2.0549 Total
= A + B/T + CxT + DxT^2 # rumus
= 0.0021 kg/m.s
Ql =
408862.6558 kg/jam
=
2491.0365 kg/m3
m3/jam =
ft3/s =
3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496) ID =
3.9 x ((1.6101)^0.45 ft3/s) x ((155.5100)^0.13 lbm/ft3) =
=
risasi ID (Kern Lampiran Tabel 11. Hal. 844) = 10 in sch 60 Standarisasi ID (Kern Lampira
0.2731 m OD 14
0.2477 m ID 13.25
Sehingga diperoleh
OD - ID Standarisasi ID
(0.2731 - 0.2477) m
0.0254 m
A =
3.14
=
3.14
=
Dimana
Inside diameter (in) ID =
Outside diameter (in) OD =
Rate volumetric (ft3/s) Ql =
Densitas liquid (lbm/ft3) =

Ql Kecepatan Linear (V)
A
164.1335 m3/jam
0.0481 m2
3409.1886 m/jam
0.9470 m/s
3.1069 ft/s
NRe
0.2477 m x 0.9470 m/s x 2491.0365 kg/m3

0.0021 kg/m.s
2.100, maka alirannya adalah turbulen Nre > 2.100, maka alirannya
Dimana
NRe =
D =
Kecepatan linear (m/s) V =
Densitas campuran (kg/m3) =
Viskositas (kg/m.s) =
(Commercial Steel) =
D =
= Relative roughness ( r )
D
= 0.000046 m
0.2477 m
= 0.0002
0.25 f
5.74 2
+
NRe^0.9
0.25
0.0002 5.74 2
+
3.7 x 0.1937 284295.7921^0.9

hf =
7.826 m x (0.9470 m/s)^2 =

0.2477 m x 2 x 9.8 m/s^2
=
=
Dimana
head loss akibat gesekan (m) hf =
f =
L =
laju aliran fluida (m/s) V =
diameter dalam pipa (m) ID =
percepatan gravitasi (m/s2) g =
(2 elbow 90, coulson tabel 5.3 hal. 204) kfit =

hfit =
(3.6329 ft)^2 x 2 =
2 x 32.2
=
Dimana
head loss akibat fitting (ft) hfit =
coefficient loss akibat fitting (ft) = 0.75 (2 elbow 90) kfit =
laju aliran fluida (ft/s) V =
percepatan gravitasi (ft/s^2) g =
n =
ngan head pompa (Hp) e. Perhitungan head pompa (Hp

+ (Z2 - Z1) + (V2^2 - V1^2) + hf + hfit Hp =
2g
(44.088 - + 10 + 0 + 0.00001 + 0.2248 =
14.696) psia
=
=
Dimana
head yang dibutuhkan pompa (ft) Hp =
head loss akibat gesekan (ft) hf =
head loss akibat fitting (ft) hfit =
=
tekanan pada titik akhir P2 =
tekanan pada titik awal P1 =
ketinggian pada titik akhir (ft) Z2 =
ketinggian pada titik awal (ft) Z1 =
laju aliran fluida pada titik akhir (ft/s) V2 =
laju aliran fluida pada titik awal (ft/s) V1 =
percepatan gravitasi (ft/s2) g =
HHP
37.4414 ft x 155.5100 lb/ft3 x 1.6101 ft3/s

550
Watt
Dimana
Hp =
=
laju alir volumetrik (ft3/s) Q =
si pompa adalah sebesar 75% 0.75 Efisiensi pompa adalah sebes

BHP
Watt
Pompa 8 (P-08)
Mengalirkan destilat dari menara destilasi (MD-01) Fungsi

menuju tempat pengolahan limbah
Centrifugal pump Jenis
Commercial Steel Bahan
Temperatur = 100 C = 373.15 K Kondisi operasi
Tekanan (P1) = 1 atm = 14.696 psia
(P2) = 1 atm = 14.696 psia
Dasar perhitungan
17835.60445 kg/jam = 4.9543 kg/s Rate liquid
958.3650 kg/m3 = 59.8286 lb/ft3 liquid (densitas)
(Dari buku Yaws Tabel 22-1 Hal. 482) Viskositas campuran ()
C D Xi Komponen
(log 10) (, cp)
0.0177 0.0000 -0.0888 1.0000 0.8150 H2O
1.0000 0.8150 H2O2
= A + B/T + CxT + DxT^2 Total
= 0.0008 kg/m.s # rumus
Ql =
17835.6045 kg/jam
958.3650 kg/m3
=
m3/jam
ft3/s =
=
3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496) b. Menghitung ID optimal
3.9 x ((0.1826)^0.45 ft3/s) x ((59.8286)^0.13 lbm/ft3) ID =
=
=
risasi ID (Kern Lampiran Tabel 11. Hal. 844) = 4 in sch 80
0.1143 m Standarisasi ID (Kern Lampira
0.0972 m OD 3.500
ID 2.900
OD - ID
(0.1143 - 0.0972) m
0.0171 m
Sehingga diperoleh
3.14
Standarisasi ID
3.14
A =
Inside diameter (in)
Outside diameter (in) =
Rate volumetric (ft3/s)
Densitas liquid (lbm/ft3) =
Dimana
ID =
Ql OD =
A Ql =
18.6105 m3/jam =
0.0074 m2
2510.325 m/jam c. Menentukan friction factor
0.6973 m/s Kecepatan Linear (V)
2.2877 ft/s
0.0171 m x 0.6973 m/s x 958.3650 kg/m3

0.0008 kg/m.s
NRe
2.100, maka alirannya adalah turbulen
Kecepatan linear (m/s)
Densitas campuran (kg/m3) Nre > 2.100, maka alirannya
Viskositas (kg/m.s) Dimana
NRe =
(Commercial Steel) D =
V =
= =
D =
= 0.000046 m
0.0972 m =
= 0.0005 D =
0.25 Relative roughness ( r )
5.74 2
+
NRe^0.9
0.25
0.0005 5.74 2
+
3.7 x 0.0972 79682.145^0.9 f
7.826 m x (0.6973 m/s)^2

0.0972 m x 2 x 9.8 m/s^2
hf =
=
head loss akibat gesekan (m)
=
=
laju aliran fluida (m/s)
diameter dalam pipa (m) Dimana
percepatan gravitasi (m/s2) hf =
f =
(10 elbow 90, coulson tabel 5.3 hal. 204) L =
V =
ID =
(2.2877 ft)^2 x 10 g =
2 x 32.2
kfit =
hfit =
head loss akibat fitting (ft)
coefficient loss akibat fitting (ft) = 0.5 (3 elbow 90) =
laju aliran fluida (ft/s)
percepatan gravitasi (ft/s^2) =
ngan head pompa (Hp) Dimana

+ (Z2 - Z1) + (V2^2 - V1^2) + hf + hfit hfit =
2g kfit =
+ 10 + 0 + 0.00002 + 0.1219 V =
g =
n =
e. Perhitungan head pompa (Hp

Hp =
head yang dibutuhkan pompa (ft)
head loss akibat gesekan (ft) =
=
tekanan pada titik akhir =
tekanan pada titik awal
ketinggian pada titik akhir (ft) Dimana
ketinggian pada titik awal (ft) Hp =
laju aliran fluida pada titik akhir (ft/s) hf =
laju aliran fluida pada titik awal (ft/s) hfit =
percepatan gravitasi (ft/s2) =
P2 =
P1 =
Z2 =
Z1 =
10.1219 ft x 59.8286 lb/ft3 x 0.1826 ft3/s V2 =
550 V1 =
g =
Watt
HHP
laju alir volumetrik (ft3/s)
si pompa adalah sebesar 75% 0.75
Dimana
Hp =
=
Q =
Watt
Efisiensi pompa adalah sebes
BHP
Pompa 4 (P-04)
: Mengalirkan larutan dari separator 1 (S-01) menuju reaktor

oksidasi (R-02)
: Centrifugal pump
: Commercial Steel
Kondisi operasi : - Temperatur = 50 C = 323.15 K
- Tekanan (P1) = 3 atm = 44.088 psia
(P2) = 1 atm = 14.696 psia
Dasar perhitungan :
= 409209.0206 kg/jam = 113.6692 kg/s
liquid (densitas) = 937.1906 kg/m3 = 58.5068 lb/ft3
A B C D Xi
(log 10) (, cp)
(Coulson Tabel 8.1 Hal. 317) 0.0990 0.3960
(Dari website pubchem) 0.27722 0.9398
-10.216 1792.50 0.0177 0.0000 -0.0888 0.0028 0.0023
-7.4005 1181.50 0.0149 0.0000 -0.2500 0.51483 0.2895
-5.1649 810.68 0.0105 0.0000 -0.2854 0.0010 0.0005
(Coulson Tabel 8.1 Hal. 317) 0.10511 0.6218
1.0000 2.2499
: log10 n11q = A + B/T + CxT + DxT^2
= 0.0022 kg/m.s
Menghitung rate volumetric
rate liquid
liquid
409209.0206 kg/jam
937.1906 kg/m3
436.6337 m3/jam
4.2832 ft3/s
Menghitung ID optimal
3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496)
3.9 x ((4.2832)^0.45 ft3/s) x ((58.5068)^0.13 lbm/ft3)
12.7379 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844) = 14 in sch 30
14 in 0.3556 m
13.25 in 0.3366 m
= (0.3556 - 0.3366) m
= 0.0191 m
ID ^2
x 3.14
2
0.3366 m ^2
x 3.14
2
0.0889 m2
:
Outside diameter (in)
Densitas liquid (lbm/ft3)
Menentukan friction factor

A
= 436.6337 m3/jam
0.0889 m2
= 4910.757 m/jam
= 1.3641 m/s
= 4.4753 ft/s
= DxVx

= 0.3366 m x 4.4753 m/s x 937.1906 kg/m3
0.0022 kg/m.s
= 191227.691

:
Bilangan Reynold
Diameter (m)
Densitas campuran (kg/m3)
Viskositas (kg/m.s)
0.00005 m (Commercial Steel)

0.3366 m
D
= 0.000046 m
0.3366 m
= 0.0001
= 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0001 5.74 2
log +
3.7 x 0.3366 191227.6912^0.9
= 0.0185
Menentukan Head Loss

f x L x V^2
ID x 2g
0.0185 x 7.826 m x (1.3641 m/s)^2
0.3366 m x 2 x 9.8 m/s^2
0.0409 m
0.00001 ft
:
friction coefficient
panjang pipa (m)
diameter dalam pipa (m)
percepatan gravitasi (m/s2)
1.5 ft (1 elbow 90, coulson tabel 5.3 hal. 204)

kfit V^2 x n
2gc
1.5 ft x (4.4753 ft)^2 x 1
2 x 32.2
0.4665 ft
:
coefficient loss akibat fitting (ft) = 1.5 (1 elbow 90)
percepatan gravitasi (ft/s^2)
jumlah fitting
Perhitungan head pompa (Hp)

144 x (P2 - P1) + (Z2 - Z1) + (V2^2 - V1^2) + hf + hfit
2g
144 x (14.696 - + 10 + 0 + 0.00001 + 0.4665
937.191 44.088) psia
5.9504 ft
1.8137 m
:
head loss akibat gesekan (ft)
densitas (lb/ft3)
tekanan pada titik akhir
ketinggian pada titik akhir (ft)
ketinggian pada titik awal (ft)
laju aliran fluida pada titik akhir (ft/s)
laju aliran fluida pada titik awal (ft/s)
percepatan gravitasi (ft/s2)
Perhitungan daya pompa
= Hp x x Ql
550
= 5.9504 ft x 58.5068 lb/ft3 x 4.2832 ft3/s
550
= 2.7112 hp
= 2021.74 Watt
:
Head pompa (ft)
densitas (lb/ft3)

= HHP
E
= 2.7112 hp
0.75
= 3.6149 hp
= 2695.66 Watt
Pompa 8 (P-08)
: Mengalirkan produk bottom dari menara destilasi (MD-01)

menuju tangki penyimpanan produk (T-03)
: Centrifugal pump
: Commercial Steel
Kondisi operasi : - Temperatur = 127 C = 400.15 K
- Tekanan (P1) = 1 atm = 14.696 psia
(P2) = 1 atm = 14.696 psia
Dasar perhitungan :
= 17835.60445 kg/jam = 4.9543 kg/s
liquid (densitas) = 1293.5310 kg/m3 = 80.7523 lb/ft3
A B C D Xi
(log 10) (, cp)
-10.216 1792.50 0.0177 0.0000 -0.0888 0.3000 0.2445
-1.615 503.800 0.0004 0.0000 0.0457 0.7000 0.7776
1.0000 1.0221
: log10 n11q = A + B/T + CxT + DxT^2
= 0.0010 kg/m.s
Menghitung rate volumetric
rate liquid
liquid
17835.6045 kg/jam
1293.5310 kg/m3
13.7883 m3/jam
0.1353 ft3/s
Menghitung ID optimal
3.9 x Ql^0.45 x ^0.13 (Peter & Timmerhaus pers. 15 hal 496)
3.9 x ((0.1353)^0.45 ft3/s) x ((80.7523)^0.13 lbm/ft3)
2.8056 in
Standarisasi ID (Kern Lampiran Tabel 11. Hal. 844) = 3 in sch 80

3.500 in 0.0889 m
2.900 in 0.0737 m
= (0.0889 - 0.0737) m
= 0.0152 m
ID ^2
x 3.14
2
0.0152 m ^2
x 3.14
2
0.0043 m2
:
Outside diameter (in)
Densitas liquid (lbm/ft3)
Menentukan friction factor

A
= 13.7883 m3/jam
0.0043 m2
= 3237.262 m/jam
= 0.8992 m/s
= 2.9502 ft/s
= DxVx

= 0.0171 m x 0.8992 m/s x 1293.5310 kg/m3
0.0010 kg/m.s
= 83824.638

:
Bilangan Reynold
Diameter (m)
Densitas campuran (kg/m3)
Viskositas (kg/m.s)
0.00005 m (Commercial Steel)

0.0737 m
D
= 0.000046 m
0.0737 m
= 0.0006
= 0.25
r 5.74 2
log +
3.7 x ID NRe^0.9
= 0.25
0.0006 5.74 2
log +
3.7 x 0.0737 83824.6377^0.9
= 0.0369
Menentukan Head Loss

f x L x V^2
ID x 2g
0.0369 x 7.826 m x (0.8992 m/s)^2
0.0737 m x 2 x 9.8 m/s^2
0.1619 m
0.00005 ft
:
friction coefficient
panjang pipa (m)
diameter dalam pipa (m)
percepatan gravitasi (m/s2)
1.0 ft (1 sudden expansion (tank inlet), coulson tabel

5.3 hal. 204)
kfit V^2 x n
2gc
1.0 ft x (2.2877 ft)^2 x 1
2 x 32.2
0.1352 ft
:
coefficient loss akibat fitting (ft) = 0.5 (3 elbow 90)
percepatan gravitasi (ft/s^2)
jumlah fitting
Perhitungan head pompa (Hp)

144 x (P2 - P1) + (Z2 - Z1) + (V2^2 - V1^2) + hf + hfit
2g
144 x 0 + 10 + 0 + 0.00005 + 0.1352
1293.53
10.1352 ft
3.0892 m
:
head loss akibat gesekan (ft)
densitas (lb/ft3)
tekanan pada titik akhir
ketinggian pada titik akhir (ft)
ketinggian pada titik awal (ft)
laju aliran fluida pada titik akhir (ft/s)
laju aliran fluida pada titik awal (ft/s)
percepatan gravitasi (ft/s2)
Perhitungan daya pompa

= Hp x x Ql
550
= 10.1352 ft x 80.7523 lb/ft3 x 0.1353 ft3/s
550
= 0.2013 hp
= 150.091 Watt
:
Head pompa (ft)
densitas (lb/ft3)

= HHP
E
= 0.2013 hp
0.75
= 0.2684 hp
= 200.121 Watt
Viskositas
(, cp)
0.3960
0.9398
0.0023
0.2895
0.0005
0.6218
2.2499
0.4665
Viskositas
(, cp)
0.2445
0.7776
1.0221
Viskositas senyawa lain
Rumus : log(log 10) = I x x 0.001 2.9 (Coulson Tabel 8.1 Hal. 317)
M
H = 2.7 Double bond = -15.5
O = 29.7 Six-member ring = -21
C = 50.2 Side group BM < 17 = -9
N = 37 Side group BM > 16 = -17
Cl = 60 Ortho / para position = 3
Br = 79 Meta position = -1
I = 110
C16H12O2 : C = 16 = 16 x 50.2 = 803.2

H = 12 = 12 x 2.7 = 32.4
O = 2= 2 x 29.7 = 59.4
Double bond = 8= 8 x (-15.5) = -124
Six-member ring = 3= 3 x (-21) = -63
Side group BM < 17 = 1= 1 x (-9) = -9
Ortho / para position = 3= 3x3 = 9
Total (I) = 708
= 1230 kg/m3
BM = 236.28 kg/kgmol
log(log 10) = 708 x 1230 x 0.001 2.9 = 0.7856

236.28
log 10 = 6.104
= 127109.6 cp
C16H14O2 : C = 16 = 16 x 50.2 = 803.2

H = 14 = 14 x 2.7 = 37.8
O = 2= 2 x 29.7 = 59.4
Double bond = 9= 9 x (-15.5) = -139.5
Six-member ring = 3= 3 x (-21) = -63
Side group BM < 17 = 1= 1 x (-9) = -9
Ortho / para position = 3= 3x3 = 9
Total (I) = 688.9
= 1089.1 kg/m3
BM = 238.3 kg/kgmol
log(log 10) = 697.9 x 1089.1 x 0.001 2.9 = 0.2485

238.3
log 10 = 1.772
= 5.9161 cp
Tabel 8.1 Hal. 317)
Kompresor (C-01)
Fungsi : Mengalirkan udara dari udara langsung menuju reaktor

oksidasi (R-02)
Kondisi operasi : - Temperatur (Ts) = 30 C = 303.15
- Tekanan (Ps) = 1 atm = 14.696
(Pd) = 3 atm = 44.088
- Zav = 1.002
Komponen F (kg/jam) Xi BM %
N2 23764.8305 0.9320 28 79 0.79
O2 1732.7269 0.0680 32 21 0.21
TOTAL 25497.5573 1.0000 100 1
BM Campuran = (BM N2 x %Berat N2) + (BM O2 x %Berat O2)

= (28 x 0.79) + (32 x 0.21)
= 28.84
BM udara = 28.9644 k (Cp/Cv) = 1.2089
R = 0.08206 Ef. Kompresor = 0.75
1 MMScfd = 1177.17 m3/jam Ef. Politropik = 0.7922
pgas = Ps x BM
RxT
= 1 x 28.84
0.08206 x 303.15
= 1.1593 g/L
= 1.1593 kg/m3
a. Penentuan laju alir (Qg)

Laju alir (Qg) = Laju alir
Densitas
= 25497.5573 kg/jam
1.1593 kg/m3
= 21993.40169 m3/jam
= 21993.40169 m3/jam x 1 MMScfd
1177.17 m3/jam
= 18.6833 MMScfd
b. Penentuan specific gravity
Specific gravity (S)= BM gas
BM udara
= 28.84
28.9644
= 0.9957
c. Perhitungan daya kompresor (BHP)

k-1
BHP = 0.0857 x Zav x Qg x Ts x k x Pd
E k1 Ps
= 0.0857 x 1.002 x
ara langsung menuju reaktor
303.15 K
14.696 psia
44.088 psia
1.2089
0.75
0.7922
k-1
k 1

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Tangki 1

Komponen Densitas (g/ml) Densitas(lb/cu.ft)

Lingkaran Bawah (ft.sq) 5526.7495567726

Tebal Allowable stress (S/F) (psi) 12650

Komponen Densitas (g/ml) Densitas(lb/cu.ft)

Tebal Allowable stress (S/F) 17890

Tutup Tangki Young 267 conical

tebal tutup (t) 5.9479803511 irwan (in)

Komponen Densitas (g/ml) Densitas(lb/cu.ft)

Lingkaran Bawah (ft.sq) 6539.7999201017

Tebal Allowable stress (S/F) 12650

tebal tutup (t) 9.2369355835 irwan (in)

Fraksi (%) Densitas(lb/cu.ft) Massa (kg/jam) Massa (lbm/jam)

young tabel 13.1

Fraksi (%) Densitas(lb/cu.ft) Massa (kg/jam) Massa (lbm/jam)

young tabel 13.1

30 derajat kemiringan 0.5

Fraksi (%) Densitas(lb/cu.ft) Massa (kg/jam) Massa (lbm/jam)

young tabel 13.1

waktu penyimpanan 720 jam H/D 2

1 g/ml 62.428 (lb/cu.ft)

1 g/ml 62.428 (lb/cu.ft)

A. Perhitungan Tangki Penyimpanan

Volume gas = massa total

Komposisi fase cair :

Komposisi kg/jam BM kmol/jam xi wi

C16H12O2 40514.403 236.28 171.4678 0.0484 0.0990

1 Perhitungan Gas-Liquid separation factor :

2 Perhitungan Maximum design vapor velocity :

3 Perhitungan Liquid Flowrate :

Minimum vessel cross sectional area :

4 Perhitungan Vapor Flowrate :

Minimum vessel cross sectional area :

5 Perhitungan diameter vessel :

6 Estimasi vapor liquid nozzle

uv max nozzle = 100 p

OD = 5.563 in (Appendix F, Brownell)

Melakukan Pengecekan Geometri

8 Menghitung Tebal Shell

BM = (BM N2 x %Berat N2) + (BM O2 x %Berat O2)

Volume gas = massa total

Komposisi fase cair :

Komposisi kg/jam BM kmol/jam xi wi

C16H12O2 81028.807 236.28 342.9355 0.0923 0.1954

p cair = 0.9465 g/cm3

Volume cair = massa total

1 Perhitungan Vapor-Liquid separation factor :

2 Perhitungan Maximum design vapor velocity :

3 Perhitungan Liquid Flowrate :

Minimum vessel cross sectional area :

4 Perhitungan Vapor Flowrate :

5 Perhitungan diameter vessel :

6 Estimasi vapor liquid nozzle

Uv max nozzle = 100 p

OD = 5.563 in (Appendix F, Brownell)

Hv = 36 in + 0.5 (Feed Nozzle OD)

Komponen F (kg/jam) Xi (kg/m3)

C16H12O2 40514.4032921938 0.0990066231 1122.3

Perhitungan Dimensi Separator 1 (S-0

Komponen F (kg/jam) Xi (kg/m3)

C16H12O2 81028.8065843748 0.1953932729 1122.3

Perhitungan tebal shell heater dan dimensi ves

an Dimensi Separator 1 (S-02)

ell heater dan dimensi vessel separator