3.

4896705528

ton/tahun
kapasitas MIBK 55000
(1 tahun = 330 hari)

Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16
 kg/jam kmol/jam
6944.4444 69.33351083

mponen
Tb, oC Sg, tidak ada satuan
56.2 0.79

100 1
167.9 0.9387
270 1.84
-252.8 0.0696
125 0.855
1.94
115.9 0.802
 TEKANAN UAP
Komponen A B C
Aseton 7.31742 1315.6735 240.479
Air 8.05573 1723.6425 233.08
MIBK 7.37701 1527.2068 223.816
MO 7.12851 1483.4864 219.745
DAA 8.62593 2568.7558 279.12
Asam Sulfat 8.28538 2976.837 213.95

ton/tahun kg/jam
kapasitas MIBK 55000 6944.4444
(1 tahun = 330 hari)
Mr MIBK = 100.16

Asumsi MIBK Data Kating Dulu

Hasil Bawah = 69.3335
Air Total =
Hasil Atas = 0.0348
Hasil Total = 69.3684
MO Total =

MIBK Total =

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 110.93232759549

Komponen F,kmol/jam Po

Air 15.1983 1.46051929258261

MO 0.0749 0.577418967976742
MIBK 69.3335 0.858900184816931
Total 84.6067

Kondisi Atas (Distilat)

P= 1.1 atm
T= 102.890352501891 oC

Komponen D,kmol/jam Po

Air 15.0463 1.10809075373933

MO 0.0742 0.446342621633675
MIBK 0.0000 0.663195314744814
Total 15.1205
 TEKANAN UAP
Komponen A B C
Air 8.05573 1723.6425 233.08
MO 7.12851 1483.4864 219.745
MIBK 7.37701 1527.2068 223.816

kmol/jam MIBK: 4-methyl-2-pentanone

69.33351083 CAS 108-10-1
Asumsi Kemurnian MIBK 99,5%
Produk Air = 3.48967055276

Data Kating Dulu

273.5691 kg/jam
15.1983 kmol/jam
7.3546 kg/jam
0.0749 kmol/jam
8231.8157 kg/jam
82.1867 kmol/jam

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
alfa
D xd B xb
2.5294 15.0463 0.9951 0.1520 0.0022
1.0000 0.0742 0.0049 0.0007 0.0000
1.4875 0.0000 0.0000 69.3335 0.9978
15.1205 1.0000 69.4862 1.0000

yd Ki Xi

0.9951 1.00735523067212 0.9878276808974

0.0049 0.40576601966698 0.0120922364306
0.0000 0.60290483158619 0
1 0.999919917328
thyl-2-pentanone

Kondisi Bawah (Bottom)

P= 1.3 atm
T= 118.974302689088 oC

Komponen B,kmol/jam Po xb

Air 0.1520 1.90090342986704 0.0022

MO 0.0007 0.737910817508952 0.0000
MIBK 69.3335 1.09894180155752 0.9978
Total 69.4862 1

Kemurnian MIBK = 0.997801978846162

 MIBK
Air
MO

Ki Yi

1.72809402715185 0.0012656929
0.670828015917229 1.607692E-05
0.999038001415924 0.9987627872
1.000044557
Air
MIBK <<

MO Semua
MIBK
Air <<
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
H2O = 273.569 15.18140954495
C6H10O = 735.4601 7.493989199103
C6H12O = 8273.1816 71.22229338843
C6H12O2 = 88.622 0.884804313099

Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 127.4787762005

Komponen F,kmol/jam
 Komponen F,kmol/jam

Air 15.1983
MO 7.4940
MIBK 69.6819
Total 92.3742

Kondisi Atas (Distilat)

P= 1.1
T = 116.3985234184

Komponen D,kmol/jam

Air 15.1983
MO 0.0749
MIBK 69.3335
Total 84.6067
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A B
Aseton 7.31742 1315.674
100 1 Air 8.05573 1723.643
167.9 0.9387 MIBK 7.37701 1527.207
270 1.84 MO 7.12851 1483.486
-252.8 0.0696 DAA 8.62593 2568.756
125 0.855 Asam Sulfat 8.28538 2976.837
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam ratio
H2O = 273.569 15.1814095449501 100
C6H10O = 7.3546 0.07493988180151 1
C6H12O = 8231.8156 70.8661811294766 99.5
C6H12O2 = 0 0 0

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
Po alfa
 Po alfa
D xd B xb
2.47993683381 2.6252 15.1983 0.1796 0.0000 0.0000
0.94465819563 1.0000 0.0749 0.0009 7.4190 0.9551
1.40874011074 1.4913 69.3335 0.8195 0.3484 0.0449
84.6067 1.0000 7.7675 1.0000

atm
o
C

Po yd Ki Xi

1.74934367498 0.1796 1.590312431801 0.11295544002237

0.68303576835 0.0009 0.620941607591 0.00142645248904
1.01681984087 0.8195 0.924381673521 0.88651672708933
1 1.00089861960074
 Persamaan Antoine
N UAP TEKANAN UAP
C Komponen A B C
240.479 Air 8.05573 1723.6425 233.08
233.08 MO 7.12851 1483.4864 219.745
223.816 MIBK 7.37701 1527.2068 223.816
219.745 DAA
279.12
213.95

Hasil Bawah
kg/jam kmol/jam ratio
H2O = 0 0 0
C6H10O = 728.1055 7.419049317302 99.000000136
C6H12O = 41.366 0.356112258953 0.50000111203
C6H12O2 = 88.622 0.884804313099 100
Kondisi Bawah (Bottom)
P= 1.3 atm
T = 138.559028982626 oC

Komponen B,kmol/jam Po xb Ki Yi

Air 0.0000 3.4432486352162 0.0000 2.64865279632 0

MO 7.4190 1.2805477256744 0.9551 0.98503671206 0.9696540876
MIBK 0.3484 1.9131949004498 0.0449 1.47168838496 0.0304786843
Total 7.7675 1 1.0001327719
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-02 Kating

Feed
kg/jam
Urut H2O = 341.9631
Berdasarkan C6H12O = 10341.4769
Titik Didih C6H10O = 919.3251
C6H12O2 = 110.7877
Ni = 1285.7694

Hasil TH-02 Yosua

Asumsi - ayo

Komponen F, kmol/jam

Air 18.9980
MO 9.3675
MIBK 87.1024
Nikel 21.9078
 Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen
Aseton
100 1 Air
167.9 0.9387 MIBK
270 1.84 MO
-252.8 0.0696 DAA
125 0.855 Asam Sulfat
1.94
115.9 0.802

ton/tahun

Feed Hasil ke MD-2

kmol/jam
18.9768645949 H2O =
103.249569688 C6H12O =
9.36748624414 C6H10O =
0.95375086088 C6H12O2 =
21.9078105299 Ni =

D, kmol/jam R + P, kmol/jam R, kmol/jam P, kmol/jam

15.1982833333 3.7997 3.4197 0.3800

7.4939891991 1.8735 1.6861 0.1873
69.6819212109 17.4205 15.6785 1.7420
0 21.9078 19.7170 2.1908
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
A B C KomponenA B
7.31742 1315.6735 240.479 Air 8.05573 1723.6425
8.05573 1723.6425 233.08 MO 7.12851 1483.4864
7.37701 1527.2068 223.816 MIBK 7.37701 1527.2068
7.12851 1483.4864 219.745
8.62593 2568.7558 279.12
8.28538 2976.837 213.95

Hasil ke MD-2 Hasil Recycle + Purge

kg/jam kmol/jam Ratio kg/jam
273.569 15.18140954495 79.99957 H2O = 68.3923
8273.1816 82.59965654952 80 C6H12O = 2068.2954
735.4601 7.493989199103 80 C6H10O = 183.865
88.622 0.762930440771 79.99263 C6H12O2 = 22.1555
0 0 0 Ni = 1285.7694

8724.17629837 kg/jam yg wajib

UAP
C
233.08
219.745
223.816

il Recycle + Purge Hasil Recycle

kmol/jam Ratio kg/jam kmol/jam
3.79535516093 19.99991 H2O = 61.553 3.41581576
20.6499141374 20 C6H12O = 1861.4658 18.58492212
1.87349704504 20 C6H10O = 165.4785 1.686147341
0.19073261019 19.99816 C6H12O2 = 19.94 0.17165978
21.9078105299 100 Ni = 1157.1925 19.71703016
cle Hasil Purging
Ratio kg/jam kmol/jam Ratio
89.9998976493 H2O = 6.8393 0.37953940067 2.0000111123
89.9999970991 C6H12O = 206.8296 2.06499201278 2.0000005995
90 C6H10O = 18.3865 0.1873497045 1.9999997824
90.0002256776 C6H12O2 = 2.2155 0.01907283058 1.9997707327
90.000003111 Ni = 128.5769 2.19078037144 9.999996889
 Data Komponen
Komponen Komponen Mr Tb, oC
Aseton C3H6O 58.08 56.2
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George

Kapasitas Pabrik = 65000 ton/tahun

Hasil TH-02 Kating

Feed
kg/jam kmol/jam
Urut H2O = 280.4082 15.560943396226
Berdasarkan C6H12O = 0 0
Titik Didih C6H10O = 8372.4778 85.311573262686
C6H12O2 = 11.0778 0.0953667355372
Ni = 1285.7694 12.837154552716
H2 = 168.8556 83.757738095238

MO H2 MIBK
M 93.6748624414102 18.93665235623
R 84.3073761972692 18.9421934912 84.312917332268
S 9.36748624414102 103.2495696885

Konversi 90 %

Hasil TH-02 Yosua

Asumsi - ayo
 Feed (Biasa)
kg/jam kmol/jam
H2O = 18.997956944482
C6H12O = 0 0
C6H10O = 65.224556221642
Ni = 21.907810529903
H2 = 0

Input MO 65.2245562216422
Recycle MO 1.68614748827471

MO H2 MIBK
M 66.9107037099169 0
R 57.5432173016195 71.423929690229
S 9.36748640829745 87.10239914502

Konversi 90 %

Input Recycle TH
C6H12O = 0 15.678469454791
C6H10O = 65.2245562216 1.6861474882747

82.589173164708

Feed (Biasa)
kg/jam kmol/jam
H2O = 18.997956944482
C6H10O = 65.224556221642
 Sg, tidak ada satuan
0.79

1
0.9387
1.84
0.0696
0.855
1.94
0.802

Hasil ke MD-2
kg/jam kmol/jam
H2O = 341.9613 18.97676470588
C6H12O = 10341.4769 103.2495696885
C6H10O = 919.3251 9.367486244141
DAA C6H12O2 = 110.7877 0.953750860882
Ni = 1285.7694 12.83715455272
H2 = 0 0

Cek Jumlah MO
93.6748654982678

0.2245996575068
sa) Hasil ke TH-2
kg/jam kmol/jam
H2O = 18.99795694448
C6H12O = 87.10239914502
C6H10O = 9.367486408297
Ni = 21.9078105299
H2 = 0

Cek Jumlah MO Nikel

0 21.90781

21.90781

Cara Hitung Hidrogen masih bingung

- kalau olin perbadningan gitu

Output
87.1023991450198
9.36748640829745

96.4698855533172

sa)
2 Recycle Masuk dari TH-2
Ratio kg/jam kmol/jam Ratio
121.95124821599 H2O = 61.553 3.41581576 100
C6H12O = 1861.4658 18.5849221 17.999999594
10.980322933791 C6H10O = 165.4785 1.68614734 100
1000.0875625124 C6H12O2 = 19.94 0.17165978 100
100 Ni = 1157.1925 11.5534395 100
0
2 Recycle Masuk dari TH-2
Ratio kg/jam kmol/jam Ratio
100 H2O = 3.41970236 100
#DIV/0! C6H12O = 15.6784695
14.361901331249 C6H10O = 1.68614749 100
100 Ni = 19.7170302 100
#DIV/0!

Hitung Hidrogen masih bingung

u olin perbadningan gitu
 Recycle Masuk dari MD-2
kg/jam kmol/jam Ratio
H2O = 0 0 0
C6H12O = 35.2293 0.35173023163 1.89255693014
C6H10O = 655.295 6.67714489505 396.000084603
C6H12O2 = 79.7672 0.68670110193 400.036108325
Ni = 0 0 0

Sementara gk make
 Recycle Masuk dari MD-2
kg/jam kmol/jam Ratio
H2O = 0 0 0
C6H12O = 35.2293 0.35173023163 2.24339647849
C6H10O = 655.295 6.67714489505 396.000049905
Ni = 0 0 0
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
C3H6O = 3436.54 59.16907713499
H2O = 9346.9416 518.6982019978
C6H10O = 8414.5505 85.74027409823
C6H12O2 = 11.0778 0.095366735537

Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 127.4787762005

Komponen F,kmol/jam
 Komponen F,kmol/jam

Aseton
Air
MO
DAA
Total 0.0000

Kondisi Atas (Distilat)

P= 1.1
T = 116.3985234184

Komponen D,kmol/jam

Aseton 0.0000
Air 0.0000
MO
DAA 0.0000
Total 0.0000
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam
C3H6O = 3436.54 59.1690771349862
H2O = 9066.5334 503.137258601554
C6H10O = 42.0728 0.42870185449358
C6H12O2 = 0 0

HK di D =
LK di B =

Distillat Bottom
Po alfa
 Po alfa
D xd B
7.26099970354476 2.9279 #DIV/0! 0.0000
2.47993683381189 1.0000 #DIV/0! 18.9980
65.2246
0.944658195634245 0.3809 #DIV/0!
0.0000 #DIV/0! 84.2225

atm
o
C

Po yd Ki Xi

5.6231761368285 #DIV/0! 5.111978306208 #DIV/0!

1.74934367498115 #DIV/0! 1.590312431801 #DIV/0!

0.683035768350579 #DIV/0! 0.620941607591 #DIV/0!

#DIV/0! #DIV/0!
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745 DAA 8.62593 2568.7558
2568.756 279.12
2976.837 213.95

Hasil Bawah
ratio kg/jam kmol/jam ratio
100 C3H6O = 0 0 0
97 H2O = 280.4082 15.56094339623 2.99999948646
0.500001 C6H10O = 8372.4778 85.311573262686 99.5000006239
0 C6H12O2 = 11.0778 0.095366735537 100

0.01
0.01

Bottom
 xb
0.0000
0.2256

0.0000
0.2256

Kondisi Bawah (Bottom)

P= 1.3 atm
T = 138.559028982626 oC

Komponen B,kmol/jam Po xb Ki

Aseton 0.0000 9.2367812941931 0.0000 7.10521638015

Air 18.9980 3.4432486352162 0.2256 2.64865279632
MO
DAA 0.0000 1.2805477256744 0.0000 0.98503671206
Total 18.9980 0.225568630409
C
240.479
233.08
219.745
279.12
 Yi

0
0.0851635332

0
0.0851635332
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
C3H6O = 3436.54 59.16907713499
H2O = 9346.9416 518.6982019978
C6H10O = 8414.5505 85.74027409823
C6H12O2 = 11.0778 0.095366735537

Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2 gk
Asumsi perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 118.1689476174

Komponen F,kmol/jam
 Komponen F,kmol/jam

Air 633.2652
MO 67.2418
Total 700.5070

Kondisi Atas (Distilat)

P= 1.1
T = 102.8218112658

Komponen D,kmol/jam

Air 614.2673
MO 2.0173
Total 616.2845
Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam
C3H6O = 3436.54 59.1690771349862
H2O = 9066.5334 503.137258601554
C6H10O = 42.0728 0.42870185449358
C6H12O2 = 0 0

HK di D =
LK di B =

Distillat Bottom
Po alfa
 Po alfa
D xd B
1.85239860596307 2.5714 614.2673 0.9967 18.9980
0.720386713175263 1.0000 2.0173 0.0033 65.2246
616.2845 1.0000 84.2225

atm
o
C

Po yd Ki Xi

1.10542295216996 0.9967 1.004929956518 0.99183703495109

0.445339624949905 0.0033 0.4048542045 0.00808501321497
1 0.99992204816606
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745
2568.756 279.12
2976.837 213.95

Hasil Bawah
ratio kg/jam kmol/jam ratio
100 C3H6O = 0 0 0
97 H2O = 280.4082 15.56094339623 2.99999948646
0.500001 C6H10O = 8372.4778 85.311573262686 99.5000006239
0 C6H12O2 = 11.0778 0.095366735537 100

0.01 Hasil atas 97%

0.01 Hasil bawah 3%

Bottom
 xb
0.2256 6.33265231482734
0.7744 614.267274538252
1.0000

Kondisi Bawah (Bottom)

P= 1.3 atm
T = 133.516083968983 oC

Komponen B,kmol/jam Po xb Ki

Air 18.9980 2.9728168061866 0.2256 2.28678215861

MO 65.2246 1.1176126300724 0.7744 0.85970202313
Total 84.2225 1
UAP
C
240.479
233.08
219.745
 Yi

0.098640191659768
0.900813710742681
0.999453902402449
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-02 Kating

Feed
kg/jam
Urut H2O = 7799.74
Berdasarkan
C6H10O = 33.1813
Titik Didih
C6H12O2 = 11078.7278
H3PO4 = 1117.4095

DAA
M 95.3747227961433
R 85.8372580922865
S 9.53746470385675

Konversi 90.0000079431503 %

Hasil TH-02 Yosua

Asumsi - Asumsi reaksi 1:1:1
 H2SO4 (98%) =

Feed (Biasa)
kg/jam
H2O (Feed bukan dari Katalis) =
C6H10O =
C6H12O2 =
H2SO4 =

Input MO 65.2245562216422

DAA
M 75.0885592561771
R 67.5797092949565
S 7.50884996122062

Konversi 90.0000079431503 %

Hasil MD-02 Yosua

- DAA udah hilang di RD jadi di MD-2
Asumsi gk perlu pisahin

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 141.34433484948

Komponen F,kmol/jam

Air 633.2652
MO 67.5797
DAA 7.5088
Total 708.3538

Kondisi Atas (Distilat)

P= 1.1
T= 106.5714565972

Komponen D,kmol/jam
Air 633.2652
MO 67.2418
DAA 0.0751
Total 700.5821
 P
Tb, C
o
Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

ton/tahun

Feed Hasil Atas

kmol/jam kg/jam
432.83795782464 H2O = 9346.942
0.3381016914612 C6H10O = 8414.551
95.374722796143 C6H12O2 = 11.0778
11.392837479608 H3PO4 = 0

MO Air H3PO4
0.3381016914612 432.837957824639 0.095367

86.171130018341 518.69820199778 0.095367

 67.241810537775 11.5446024936281

Feed (Biasa) Hasil Atas

kmol/jam kg/jam
554.14091969415 H2O =
0 C6H10O =
75.088559256177 C6H12O2 =
67.241810537775 Ikut kating H3PO4 =

Katalis
MO Air H2SO4
0 565.685522187777 67.24181
67.579709294957 67.5797092949565
67.579709294957 633.265231482734 67.24181

HK di D = 0.01
LK di B = 0.01

Distillat Bottom
Po alfa
D xd B xb
3.72794609557352 8.6235 633.2652 0.9039 0.0000 0.0000
1.37826419611347 3.1882 67.2418 0.0960 0.3379 0.0435
0.432300160245113 1.0000 0.0751 0.0001 7.4338 0.9565
700.5821 1.0000 7.7717 1.0000

atm
o
C

Po yd Ki Xi
 1.25943972525331 0.9039 1.144945 0.789481
0.5029649273031 0.0960 0.457241 0.209911
0.121614387797359 0.0001 0.110559 0.000969
1 1.000362
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B C
1315.6735 240.479 Air 8.05573 1723.643 233.08
1723.6425 233.08 MO 7.12851 1483.486 219.745
1527.2068 223.816 DAA 8.62593 2568.756 279.12
1483.4864 219.745
2568.7558 279.12
2976.837 213.95

Hasil Atas Hasil Bawah

kmol/jam Ratio kg/jam kmol/jam Ratio
518.698202 119.8365792 H2O = 0 0 0
85.7402741 25359.31534 C6H10O = 42.2842 0.430856 127.4338
0.095366736 0.099991625 C6H12O2 = 1096.794 9.442098 9.9
0 H3PO4 = 1117.41 11.39284

REAKSI Yield
DAA = 85.8372580922865 DAA = 0.333309
MO = 85.83302832688 Total 257.5305 MO = 0.333293
Air = 85.860244173141 Air = 0.333398

Hasil Bawah MO 0.00500000313

0.50000031336
Hasil Atas Hasil Bawah
kmol/jam Ratio kg/jam kmol/jam Ratio
633.2652315 #REF! H2O = 0 #REF!
67.24181054 #REF! C6H10O = 0.337899 #REF!
Gk tau #VALUE! C6H12O2 = #REF!
H3PO4 =

Cara Hitung Hidrogen masih bingung

Hasil atas 97%

Hasil bawah 3%

6.332652315

Kondisi Bawah (Bottom)

P= 1.3 atm
T = 176.1172131 oC

Komponen B,kmol/jam Po xb Ki Yi
Air 0.0000 9.17619526192236 0.0000 7.058612 0
MO 0.3379 3.16384140984122 0.0435 2.433724 0.017865
DAA 7.4338 1.26602143684999 0.9565 0.973863 0.982194
Total 7.7717 1 1.000059
 Perbandingan Atas Bawah %
Ratio Bawah Ratio Atas
H2O = 0 100
C6H10O = 0.5000003134 99.499999687
C6H12O2 = 99.000082952 0.9999170482
H3PO4 = 100 0
 Sementara gk make
Recycle Masuk dari MD-2
kg/jam kmol/jam Ratio
H2O = 0 0 #DIV/0!
C6H12O = 35.2293 0.3517302316 104.0934
C6H10O = 655.295 6.677144895 #DIV/0!
Ni = 0 0 #DIV/0!
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000 ton/tahun

Hasil MD-02 Kating

Feed
kg/jam kmol/jam
C3H6O = 85913.5009 1479.226943871
H2O = 14026.8452 778.4042841287
C6H12O2 = 11078.7278 95.37472279614

Hasil MD-02 Yosua

Asumsi -

1. Asumsi awal distribusi awal komponen di Distilat dan Bottom

P avg = 1.2
T avg = 102.4250226021

Komponen F,kmol/jam

Aseton 1942.9003
Air 1022.4002
DAA 75.0886
Total 3040.3891

Kondisi Atas (Distilat)

P= 1.1
T = 76.14382770421

Komponen D,kmol/jam

Aseton 1942.9003
Air 468.2593
DAA 0.0000
Total 2411.1596
 Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen A
Aseton 7.31742
100 1 Air 8.05573
167.9 0.9387 MIBK 7.37701
270 1.84 MO 7.12851
-252.8 0.0696 DAA 8.62593
125 0.855 Asam Sulfat 8.28538
1.94
115.9 0.802

Hasil Atas
kg/jam kmol/jam
C3H6O = 82476.9608 1420.05786501377
H2O = 6424.2951 356.509162042175
C6H12O2 = 0 0

HK di D =
LK di B =

Distillat Bottom
Po alfa
D xd B
3.97878057849759 3.6500 1942.9003 0.8058 0.0000
1.09008355006937 1.0000 468.2593 0.1942 554.1409
0.10294519806434 0.0944 0.0000 0.0000 75.0886
 2411.1596 1.0000 629.2295

atm
o
C

Po yd Ki Xi

1.91105297999257 0.8058 1.737320890902 0.46381470861798

0.398862308442766 0.1942 0.362602098584 0.53558712971718
0.032700783524058 0.0000 0.029727985022 0
1 0.99940183833516
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
B C Komponen A B
1315.674 240.479 Aseton 7.31742 1315.6735
1723.643 233.08 Air 8.05573 1723.6425
1527.207 223.816 MO 7.12851 1483.4864
1483.486 219.745 DAA 8.62593 2568.7558
2568.756 279.12
2976.837 213.95

Hasil Bawah
ratio kg/jam kmol/jam ratio
96 C3H6O = 3436.54 59.16907713499 3.9999999581
45.8 H2O = 7602.5501 421.8951220866 54.2000000114
0 C6H12O2 = 11078.7278 95.37472279614 100

0.01
0.01

Bottom
xb
0.0000
0.8807
0.1193
1.0000

Kondisi Bawah (Bottom)

P= 1.3 atm
T = 128.706217500033 oC

Komponen B,kmol/jam Po xb Ki

Aseton 0.0000 7.4625002398418 0.0000 5.74038479988

Air 554.1409 2.574301803014 0.8807 1.98023215616
DAA 75.0886 0.2795525622769 0.1193 0.21504043252
Total 629.2295 1
C
240.479
233.08
219.745
279.12

REAKSI Yield
C3H6O = 1479.227 C3H6O =
H2O = 778.4043 Total 2353.006 H2O =
C6H12O2 = 95.37472 C6H12O2 =
 Yi

0
0.4447285923
0.5549381548
0.9996667471
0.628654
0.330813
0.040533
 Data Komponen
Komponen Komponen Mr
Aseton C3H6O 58.08
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02
Diaseton Alkohol C6H12O2 116.16
Asam Sulfat (Katalis 2) H2SO4 98.08
Gas Hidrogen H2 2.016
Mesitil Oksida (MO) C6H10O 98.14
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George
Kapasitas Pabrik = 65000

Hasil TH-01 Kating

Feed
kg/jam
Urut H2O = 17533.5565
Berdasarkan C3H6O = 114551.3345
Titik Didih C6H10O = 41.4767
C6H12O2 = 13848.4097
Ba(OH)2 = 296.8259

Hasil TH-01 Yosua

Asumsi - ayo

Komponen F, kmol/jam

Air 1278.0003
Aseton 2590.5338
DAA 93.8609
Ba(OH)2 1.7324
3964.1273
 Tb, oC Sg, tidak ada satuan TEKANAN UAP
56.2 0.79 Komponen
Aseton
100 1 Air
167.9 0.9387 MIBK
270 1.84 MO
-252.8 0.0696 DAA
125 0.855 Asam Sulfat
1.94
115.9 0.802

ton/tahun

Feed Hasil ke MD-1

kmol/jam
973.005355161 H2O =
1972.30259125 C3H6O =
0.42262787854 C6H10O =
119.218403065 C6H12O2 =
1.7323794794 Ba(OH)2 =

D, kmol/jam R + P, kmol/jam R, kmol/jam P, kmol/jam

1022.40022062 255.6001 232.4804 23.1197

1942.90034703 647.6334 589.0558 58.5777
75.0885592562 18.7723 17.0743 1.6980
0 1.7324 1.5757 0.1567
3040.3891 923.7382
 Persamaan Antoine
TEKANAN UAP TEKANAN UAP
A B C KomponenA B
7.31742 1315.6735 240.479 Air 8.05573 1723.6425
8.05573 1723.6425 233.08 MO 7.12851 1483.4864
7.37701 1527.2068 223.816 MIBK 7.37701 1527.2068
7.12851 1483.4864 219.745
8.62593 2568.7558 279.12
8.28538 2976.837 213.95

Hasil ke MD-1 Hasil Recycle + Purge

kg/jam kmol/jam Ratio kg/jam
14026.8452 778.4042841287 80 H2O = 3506.7113
85913.5009 1479.226943871 75 C3H6O = 28637.8337
33.1813 0.338101691461 79.99986 C6H10O = 8.2953
11078.7278 95.37472279614 80 C6H12O2 = 2769.682
0 0 0 Ba(OH)2 = 296.8259
UAP
C
233.08
219.745
223.816

il Recycle + Purge Hasil Recycle

kmol/jam Ratio kg/jam kmol/jam
194.601071032 20 H2O = 3189.52 176.9988901
493.075649105 25 C3H6O = 26047.4658 448.4756508
0.08452516813 19.9999 C6H10O = 7.545 0.076879967
23.8436811295 20 C6H12O2 = 2519.1569 21.68695678
1.7323794794 100 Ba(OH)2 = 269.9772 1.575681102
cle Hasil Purging
Ratio kg/jam kmol/jam Ratio
90.9547358518 H2O = 317.1913 17.6021809101 1.8090528296
90.9547351691 C3H6O = 2590.3679 44.5999982782 2.2613162136
90.9551191639 C6H10O = 0.7503 0.00764520073 1.8089674444
90.9547341536 C6H12O2 = 250.5251 2.15672434573 1.8090532085
90.9547313762 Ba(OH)2 = 26.8487 0.1566983775 9.0452686238
 Data Komponen
Komponen Komponen Mr Tb, oC
Aseton C3H6O 58.08 56.2
Barium Hidroksida (Katalis 1) Ba(OH)2 171.34
Air H2O 18.02 100
Diaseton Alkohol C6H12O2 116.16 167.9
Asam Sulfat (Katalis 2) H2SO4 98.08 270
Gas Hidrogen H2 2.016 -252.8
Mesitil Oksida (MO) C6H10O 98.14 125
Nikel Ni 58.69
Metil Iso Butil Keton (MIBK) C6H12O 100.16 115.9

Punya Kating Dulu

Asumsi Punya Pak Sarto, Mas George

Kapasitas Pabrik = 65000 ton/tahun

Hasil TH-02 Kating

Feed (Murni)
kg/jam kmol/jam
Urut C3H6O = 14584.5912 251.11210743802
Berdasarkan
H2O = 607.5822 33.717103218646
Titik Didih
C6H10O = 0 0
Ba(OH)2 = 26.8487 0.156698377495
C6H12O2 = 0 0

2 Aseton ---------> 1 DAA

M 1777.23969869146 21.686956783747
R 195.062892561984 97.531446280992
S 1972.30259125344 119.21840306474

Konversi 15 %

Hasil TH-02 Yosua

Asumsi - ayo

Feed (Biasa)
 kg/jam kmol/jam
C3H6O = -5517.3360536 -94.995455468924
H2O = 0
C6H10O = Gk ada MO
Ba(OH)2 = 0
C6H12O2 = 0

Input MO 65.2245562216422
Recycle MO 0

2 Aseton ---------> 1 DAA

M 2436.96066616912 17.074304234242
R 153.573129118692 76.786564559346
S 2590.53379528781 93.860868793588

Konversi 15 %

Input Recycle TH
C6H12O = 0 232.48035500389
C6H10O = 2436.96066617 0

2669.441021173

Feed (Biasa)
kg/jam kmol/jam
H2O = -94.995455468924
C6H10O = 65.224556221642
 Sg, tidak ada satuan
0.79

1
0.9387
1.84
0.0696
0.855
1.94
0.802

rni) Hasil ke TH-1

Ratio kg/jam kmol/jam
11.5860527129905 C3H6O = 114551.3345 1972.302591253
3.46525361240887 H2O = 17533.5565 973.0053551609
0 C6H10O = 41.4767 0.422627878541
9.04526862379597 Ba(OH)2 = 296.8259 1.732379479398
0 C6H12O2 = 13848.4097 119.2184030647

Katalis
Ba(OH)2

10.9756096887552

sa) Hasil ke TH-1

 kg/jam kmol/jam
C3H6O = 150458.2028303 2590.533795288
H2O = 23029.56496953 1278.000275778
C6H10O = Gk ada MO 0
Ba(OH)2 = 296.8259 1.732379479398
C6H12O2 = 10902.87851906 93.86086879359

Katalis
Ba(OH)2

Recycle
1.732379

6.30183044193764 % Cara Hitung Hidrogen masih bingung

- kalau olin perbadningan gitu

Output
1278.00027577843
0

1278.00027577843

sa)
1 Recycle Masuk dari TH-1
kg/jam kmol/jam Ratio
C3H6O = 26047.4658 448.475651 20.692202315
H2O = 3189.52 176.99889 18.19094717
C6H10O = 7.545 0.07687997 18.190936116
Ba(OH)2 = 269.9772 1.5756811 90.954731376
C6H12O2 = 2519.1569 21.6869568 100

100
100
100
100
100

1 Recycle Masuk dari TH-1

 Ratio kg/jam kmol/jam Ratio
106.30183044194 C3H6O = 34212.3593892 589.055775 24.171739117
182.37875721159 H2O = 4189.29599717 232.480355 33.176423374
#DIV/0! C6H10O = Gk ada MO 0 #DIV/0!
109.94480274631 Ba(OH)2 = 269.9772 1.5756811 100
549.72002083313 C6H12O2 = 1983.35117985 17.0743042 100

Hitung Hidrogen masih bingung

u olin perbadningan gitu
 Recycle Masuk dari FD-1
kg/jam kmol/jam Ratio
C3H6O = 82476.9608 1420.05786501 65.5200000008
H2O = 6424.2951 356.509162042 36.6399999909
C6H10O = 0 0 0
Ba(OH)2 = 0 0 0
C6H12O2 = 0 0 0

Recycle Masuk dari MD-1

 kg/jam kmol/jam Ratio
C3H6O = 112843.652155573 1942.90034703 79.7263728547
H2O = 8438.03260273327 468.259300929 66.8235766257
C6H10O = Gk ada MO 0 #DIV/0!
Ba(OH)2 = Gk ada katalis recycle dr MD-1 0 0
C6H12O2 = 0 0 0
 Recycle Masuk dari MD-1
kg/jam kmol/jam Ratio
C3H6O = 2771.5695 47.71986053719 2.201744970728
H2O = 7312.1592 405.78019977802 41.70379922636
C6H10O = 33.9317 0.3457479111473 81.80906388406
Ba(OH)2 = 0 0 0
C6H12O2 = 0 0 0

Feed Awal + Recycle

 kg/jam kmol/jam
C3H6O = 141538.6754911 2436.9606661691
H2O = 12627.3285999 700.73965593249
C6H10O = Gk ada MO 0
Ba(OH)2 = 269.9772 1.5756811019026
C6H12O2 = 1983.35117985 17.074304234242
 Feed Awal + Recycle
kg/jam kmol/jam
C3H6O = 125880.5873 2167.3654838
H2O = 17533.5565 973.00535516
C6H10O = 41.4767 0.4226278785
Ba(OH)2 = 296.8259 1.7323794794
C6H12O2 = 2519.1569 21.686956784