❑ 1000
Kadar ( Sampel+ SpikeCl ) = + V ( titrasi Sp+ Spike ) N AgNO 3 x BA Cl …
V Sp+ Spike
No Volume Sampel Volume Kadar Kadar spike Kadar spike
Klorida (NaCl AgNO3 Klorida target (ppm) percobaan=
0,0141 N=500 0,01 N (mL) Terukur KadarTeruku
ppm Klorida (mL) (mg/L) r –kadar
target
Sp 45,00 mL sampel 50,00
+
5,0 mL akuades
(Sp + spike) 1 45,00 mL sp + 5,0 50,00
Klorida 500 ppm
(Sp + spike) 2 45,00 mL sp + 5,0 50,00
Klorida 500 ppm
(Sp + spike) 3 45,00 mL sp + 5,0 50,00
Klorida 500 ppm
(Sp + spike) 4 45,00 mL sp + 5,0 50,00
Klorida 500 ppm
(Sp + spike) 5 45,00 mL sp + 5,0 50,00
Klorida 500 ppm
1000
x ml titrasi x N AgNO3 x 35,45 ( BA Cl− ) =.... mg / L
Volume sampel
1000
( Kadar Klorida Terukur )❑ = x … … … x … … … ….. x 35,45=… … … … mg/ L
50,00
Pembuatan spike matrix:
45,00 mL contoh uji Klorida ditambah 5,00 mL larutan Standart klorida 500 mg/L, sehingga volume
total 50,00 mL.
G = ( y )( z ) / v
SD= √
2
( R 1−R rata2)
( n−1)
Contoh:
2.11
1.50
0.89
0.28
0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31
-0.33
-0.94