t4 MD

Neraca massa masing-masing alat
Alat P-103
Input(kg/jam) Output(kg/jam)
Komponen
Arus 0 Arus 9
Nitrobenzen 0 0
Hidrogen 803.81 803.81
Anilin 0 0
Benzen 0 0
Nitrogen 11.2 11.2
Air 0 0
Jumlah 815.01 815.01
Alat CO-101
Input(kg/jam) Output(kg/jam
Komponen
Arus 9 Arus 17 Arus 10(arus 9+ar Arus 11
Nitrobenzen 0 0 0 0
Hidrogen 803.811 212.707 1016.52 1016.52
Anilin 0 0 0 0
Benzen 0 0 0 0
Nitrogen 11.2 0 11.2 11.2
Air 0 0 0 0
Jumlah 815.01 212.71 1027.72 1027.72
Alat HE-102
Komponen
Arus 11 Arus 12
Nitrobenzen 0 0
Hidrogen 1016.52 1016.52
Anilin 0 0
Benzen 0 0
Nitrogen 11.20 11.20
Air 0 0
Jumlah 1027.72 1027.72
Alat R-201
Komponen
Arus 12 Arus 17 Arus 13
Nitrobenzen 0 16529.90 165.299
Hidrogen 1016.52 0 212.63
Anilin 0 12.26 12391.4
Benzen 0 165.32 165.324
Nitrogen 11.2 0 11.2
Air 0 0 4789.345
Jumlah 1027.72 16707.48 17735.20
Total 17735.20 17735.20
Alat EV-101
Komponen
Arus 13 Arus 14 P1 2.5 atm
Nitrobenzen 165.299 165.299 P2 1.5 atm
Hidrogen 212.63 212.63
Anilin 12391.4 12391.4
Benzen 165.324 165.324
Nitrogen 11.2 11.2
Air 4789.345 4789.345
Jumlah 17735.20 17735.20
Alat HE-201
Komponen
Arus 14 Arus 15
Nitrobenzen 165.299 165.299
Hidrogen 212.63 212.63
Anilin 12391.4 12391.4
Benzen 165.324 165.324
Nitrogen 11.2 11.2
Air 4789.345 4789.345
Jumlah 17735.20 17735.20
Alat CD-201
Komponen
Arus 15 Arus 16
Hidrogen 212.63 212.63
Anilin 12391.4 12391.4
Benzen 165.324 165.324
Nitrogen 11.2 11.2
Air 4789.345 4789.345
Jumlah 17735.20 17735.20
Alat KD-201
Komponen Input(kg/jam) Output(kg/jam)
Nitrobenzen 165.299 165.299 0
Hidrogen 212.63 0 212.63
Anilin 12391.4 12391.4 0
Benzen 165.324 165.324 0
Nitrogen 11.2 11.2 0
Air 4789.345 4789.345 0
Jumlah 17735.20 17522.57 212.63
Total 17735.20 17735.20
Alat TP-301
Komponen
Arus 24 Arus 24 P 1 atm
Nitrobenzen 0.1647 0.1647 T 30C
Hidrogen 0 0
Anilin 12366.59 12366.59 97943431.56048 kg/tahun
Benzen 0 0 97943.43156048 ton/tahun
Nitrogen 0 0
Air 4.7894 4.7894
Jumlah 12371.55 12371.55
Alat HE-202
Komponen
Arus 18 Arus 19
Hidrogen 0 0
Anilin 12391.4 12391.4
Benzen 165.324 165.324
Nitrogen 11.2 11.2
Air 4789.345 4789.345
Jumlah 17522.57 17522.57
Alat MD-301
Komponen
Nitrobenzen 165.30 0.58 164.72
Hidrogen 0 0 0
Anilin 12391.40 12.39 12379.01
Benzen 165.32 165.32 0
Nitrogen 11.20 11.20 0
Air 4789.35 4784.60 4.747
Jumlah 17522.57 4974.10 12548.47
Total 17522.57 17522.57
Alat HE-303
Komponen
Arus 21 Arus 22
Hidrogen 0 0
Anilin 12379.01 12379.01
Benzen 0 0
Nitrogen 0 0
Air 4.747 4.747
Jumlah 12548.48 12548.48
Alat MD-302
Komponen
Nitrobenzen 164.72 0.16 164.55
Hidrogen 0 0 0
Anilin 12379.01 12366.59 12.38
Benzen 0 0.00 0
Nitrogen 0 0.00 0
Air 4.747 4.79 0
Jumlah 12548.48 12371.55 176.93
Total 12548.48 12548.48
Alat HE-304
Komponen
Arus 23 Arus 24
Hidrogen 0 0
Anilin 12366.59 12366.59
Benzen 0.00 0.00
Nitrogen 0.00 0.00
Air 4.79 4.79
Jumlah 12371.55 12371.55
Alat TK-101 P
Input(kg/jam) Output(kg/jam) T
Komponen
Arus 1 Arus 1
Nitrobenzen 16367 16367
Hidrogen 0 0
Anilin 0 0
Benzen 165.32 165.32
Nitrogen 0 0
Air 0 0
Jumlah 16532.32 16532.32
Alat P-101
Komponen Input(kg/jam) Output(kg/jam
Arus 1 Arus 25 Arus 2(Arus1+arusArus 3
Nitrobenzen 16367 164.55 16531.552 16531.552
Hidrogen 0 0 0.000 0.000
Anilin 0 12.38 12.379 12.379
Benzen 165.32 0 165.324 165.324
Nitrogen 0 0 0.000 0.000
Air 0 0.000 0.000 0.000
Jumlah 16532.32 176.93 16709.255 16709.255
Total 16709.255 16709.255
Alat HE-101
Komponen Input(kg/jam) Output(kg/jam
Arus 3 Arus 8 Arus 4(Arus 3+arusArus 5
Nitrobenzen 16531.552 4182.280 20713.832 20713.832
Hidrogen 0 0 0.000 0.000
Anilin 12.379 1.487 13.866 13.866
Benzen 165.324 11.06 176.384 176.384
Nitrogen 0 0 0.000 0.000
Air 0 0 0.000 0.000
Jumlah 16709.255 4194.827 20904.082 20904.082
Total 20904.082 20904.082
Alat VAP-101
Input(kg/jam) Output(kg/jam) Tin
Komponen
Arus 5 Arus 6 Tout
Nitrobenzen 20713.832 20713.832 (penguapan)
Hidrogen 0 0
Anilin 13.866 13.866
Benzen 176.384 176.384
Nitrogen 0 0
Air 0 0
Jumlah 20904.082 20904.082
Alat KD-101
Komponen Input(kg/jam) Output(kg/jam)
Nitrobenzen 20713.832 16529.900 4182.280
Hidrogen 0 0.000 0
Anilin 13.866 12.255 1.487
Benzen 176.384 165.324 11.06
Nitrogen 0 0.000 0
Air 0 0.000 0
Jumlah 20904.082 16707.479 4194.827
Total 20904.08 20902.31
1 atm
30 C
Alat P-101 T
Komponen
Arus 2 Arus 3 P1
Nitrobenzen 20713.832 20713.832 P2
ATAU Hidrogen 0 0
Anilin 13.866 13.866
Benzen 176.924 176.924
Nitrogen 0 0
Air 0 0
Jumlah 20904.62 20904.62
Tin 84.48 C
Tout 210 C
210
210
purge
1.652
0.000
0.124
0.000
0.000
0.000
1.776
32 C
1 atm
2.5 atm
Amar P-103
CO-101
HE-102
R-201
EV-101
HE-201
CD-201
KD-201
MD-302
AHYAR TK-101
P-101
VAP-101
KD-101
HE-202
MD-301
HE-304
TP-301
KOMPRESOR C - 02
TUGAS
Menaikkan tekanan gas hidrogen hingga mencapai tekanan operasi R-02
JENIS
Centrifugal compressor
KONDISI OPERASI
P inlet 1.5 atm P outlet 3.1 atm
22.05 psi 45.57 psi Nitrobenzen
T feed 333.15 K 60 C
139.67 F
Komposisi feed
Komponen Fm, kg/jam Fi, kmol/jam yi
H2 1016.5180 508.2590 0.9992
N2 11.2000 0.4000 0.0008
Total 1027.7180 508.6590 1.0000
PERHITUNGAN KOMPRESOR
PENENTUAN JUMLAH STAGE

n 1
P'/P 2.066666667
bagus, antara 3 - 5
PERHITUNGAN BEBAN KOMPRESOR

T in 333.15 K Data CP
Hidrogen
yi Mr Cpi yi.Mi yi.Cpi nitrogen
H2 0.9992 2 28.91 1.998427 28.89095
N2 0.0008 28 29.12 0.022019 0.022903 cp = A+BT+CT^2+DT^3+ET
sum 0.9992 30.0000 58.0386 2.0204 28.9139 kJ/kmol.K
M 2.0204
rho 0.110871542 kg/m3
Q 9269.448098 m3/jam
Cp 28.91 J/mol K
R 8.3144 J/mol K
gamma 1.4036223
T out 410.4858927 K 137.335892706 C
W 1137401.66 kJ/jam
315.9449051 kW
efisiensi 78 %
W net 405.0575706 kW
3.47756380188 0.287558
W tot 405.0575706 kW 1.232135
543.1903033 HP 0.232135
eff motor 85 %
P motor 639.0474157 HP 476.545425552 kW
dipilih motor HP
PENENTUAN KEBUTUHAN STEAM UNTUK TURBIN

Ps 150 psig
Ts 366 F
P out 0 psig
ms 19.37 lb/kWH (Perry, tab 24.6)
7845.965142 lb/jam
3558.874156 kg/jam
internal eff. 30 % (Perry, tab 24.7)

ms actual 11862.91385 kg/jam
Alat CO-101 Komponen
Input(kg/jam) Output(kg/jam Nitrobenzen
Komponen
Arus 9 Arus 17 Arus 10(ar Arus 11 Hidrogen
Nitrobenzen 0 0 0 0 Anilin
Hidrogen 803.811 212.707 1016.52 1016.52 Benzen
Anilin 0 0 0 0 Nitrogen
Benzen 0 0 0 0 Air
Nitrogen 11.2 0 11.2 11.2
Air 0 0 0 0
Jumlah 815.01 212.71 1027.72 1027.72
Tref 298.15
massa(kg/jammol T Cp H2 Q=mcpdT
803.811 401.9055 25 298.15 28.7640421 0 Qin
212.707 106.3535 160 433.15 154.449281 2217540 Qin
mtotal 508.259
Qout 2217540
Tout 333.152422 60.00242
cPH2 124.648852
Komponen A B C D E
H2 25.399 0.020178 -3.9E-05 3.19E-08 -8.759E-12
N2 29.342 -0.0035395 1E-05 -4.3E-09 2.5935E-13
cp = A+BT+CT^2+DT^3+ET^4
kJ/kmol.K
A B C D E
-16.202 0.56182 ### ### ###
25.399 ### ### ### ###
-22.062 0.57313 ### ### ###
-31.368 0.47460 ### ### ###
29.342 ### ### ### ###
33.933 ### ### ### ###
HEAT EXCHANGER - 01 - Sebelum
HOT FLUID
Komponen kmol/jam kg/jam xi
H2 508.2590 1016.5180 0.9992
N2 0.4000 11.2000 0.0008
Total 508.6590 1027.7180 1.0000

2265.7277 lb/jam
410.15 K
Tin 137 °C
279 °F
483.15 K
Tout 210 °C
410 °F
446.65 K
Taverage 174 °C
344 °F
Nilai Q
Komponen m, kmol/jam Cp, kJ/kmol.K m.Cp, kJ/jam.K
H2 508.2590 29.2132 14,847.8787
N2 0.4000 29.3973 11.7589
Total 14,859.6376
1084753.5476 kJ/jam
Q
1028163.0398 BTU/jam
COLD FLUID
1260.00372519237 lb/hr GoalSeek

water
water 571527.609717456 g/hr 571.527609717456
31751.533873192 mol/hr
214.0000 °C
Tin 487.1500 K
417.2000 °F
214.0000 °C
Tout 487.1500 K
417.2000 °F
487.1500 K
Taverage 214.0000 °C
417.2000 °F
0.0000 kJ/jam
Q
0.0000 BTU/jam
acc GoalSeek
LMTD
Hot Fluid Cold Fluid Diff.

417 High 410 7
417 Low 279 139
0 Diff 131 131
LMTD 44.4293 °F
Koreksi Nilai LMTD
R 0.0000 S 0.9481
FT 1 Fig.18
FT.LMTD 44.4293 °F
tc = ta = 344.3000 °F
Tc = Ta = 417.2000 °F
DARI SINI
Tinggal Trial Trial
Nilai A
UD =100 - 200 Table 8
Ud 60 BTU/ft2.F.hr
A 385.692993698493 ft2 (Digunakan HE shell n tube karen
Lay Out HE
Tube Side
Tube Pitch triangular pitch
OD 0.75 inch on
L 16 ft
Passes 2
a" 0.3271 ft2 (Table 10)

BWG 16
a' 0.985 sqin
ID tube 1.12 in
73.6955 tubes
Nt
302 tubes table 9
Shell Side
ID 21.25 inch
Passes 1
Tube Side
Nt 302
L 16 ft
OD 0.75 inch
BWG 16
Pitch 1 in. triangular pitch
Passes 2
Koreksi UD
A 1580.5472 ft2
UD 14.6415
Tube Side water

Flow Area tube
Nt  at '
at 
144  n
Nt 302
at' 0.985
n 2
at 1.0329 ft2
Mass Velocity
G_t=m_h/a_t
mc 2265.7277 lb/jam
at 1.0329 ft2
Gt 2193.59789310546 lb/ft2.jam
Reynold
1.12 inch (Table 10)

ID
0.093333333333333 ft
Gt 2193.59789310546 lb/ft2.jam
μ 0.0281 lb/ft.jam
ReT 7296.0901
jH
L x n /D 342.8571
jH 30 figure 24
hio untuk condensation of steam
v 0.009749323969358 fps cp
koreksi miu
Ta 417 F k
hi 10 BTU/jam.ft2.F D
hi kern muw
hicor
hio 14 BTU/jam.ft2.F
UC
hio 14.2044 BTU/jam.ft2.F

ho 3.5929 BTU/jam.ft2.F
UC 2.8676 BTU/jam.ft2.F
Rd
UD 14.6415 BTU/jam.ft2.F
Rd -0.2804 BTU/jam.ft2.F min 0,003
Pressure Drop
Tube Side
Re
Re 7296.0901
f
f 0.00035 figure 26
∆Pt
f 0.00035
Gt 2193.598 lb/ft2.jam
L 16 ft
n 2
D 0.093333333333333 ft
s 0.001548874727355
∆Pt 0.003570906628493 psi
∆Pr
∆Ptotal
∆Ptotal 0.0036 psi
Summary
Tube Shell
Nt 302 ID, in 21.25
OD, in 0.75 Pass, n 1
Pitch, in 1 L, ft 16
BWG 16
Pass, n 2
a", ft2/ft 0.3271
Triangle Pitch
HE-05, Heater
Hot Fluid, Tube Side, Cold Fluid, Shell Side,
Steam Hidrogen
214 Tin, °C 137
214 Tout, °C 210
14 h, Btu/jam. ft2.F 3.59
UC = 2.8676 Btu/jam. ft2.F
UD = 14.6415 Btu/jam. ft2.F
Rd calculated = -0.2804
Rd required = 0.003
0.004 ∆P calculated, psi 0.002
2 ∆P required, psi 10
- 01 - Sebelum R-01
Mr xi, massa Data CP Gas

2.0000 0.98910206885546 Data
Compound a
28.0000 0.01089793114454 H2 25.399
N2 29.342
flowrate air pendingin > condensate 29.2134

(flowrate >> di shell : air pendingin di shell Cp 14.4589
T >> di tube : condensate di tube 3.4535
Thermal Conductivity of Gas
Compound A
H2 0.03951
N2 0.03090
mCpTin mCpTout
4,136,619.0061 6,087,630.2674
3,276.0399 4,821.1643 k campuran
0.2315
k
0.1338
4,139,895.0460 6,092,451.4316
Berdasarkan tabel 7 Kern, digunakan steam dengan spesifikasi sebagai berikut :

T= 420 F 215.5555555556 C
P= 308 psi 20.95238095238 atm
hfg = 816 Btu/lb
vg = 1.4811 ft3/lb
Heat Capacity of Inorganic liq Cp (J/mol.K) = A + B*T + C*T^2 + D*T^3 + E*T^4

Rumus Nama A B C
H2O Water 92.053 -0.039953 -0.00021103
84.3238 J/mol.K Viscosity

Cp 4.6847 J/g.K (Figure 15 Kern)
1.1189 BTU/lb.F
Mr 18 g/mol
Enthalpy of Evaporation 816 btu/lb (Table 7 Kern)

Specific volume (vapor) 1.5 ft3/lb
Rho (vapor) 0.6666667 lb/ft3
k 2.35E-02 W/m.K
0.0136 BTU/hr.ft.F
Hot Fluid Cold Fluid

214 High 210
214 Low 137
0 Diff 73
an HE shell n tube karena A > 200 ft2)
Shell Side
ID 21.25
Passes 1
1 in. triangular pitch Baffle 5.31
De 0.99
Shell Side
Jarak Baffle
IDs 21.25
B 5.3125
Clearance
PT 1
ODT 0.75
C 0.25
Flow Area shell
IDs 21.25
C 0.25
B 5.3
PT 1
as 0.1960
Mass Velocity
G_s=m_c/a_s
mh 1260.0037
Gs 6428.89651564
Reynold
0.99
De
3.4535 0.0825
0.0407174536240746 μ 0.0407
1.36E-02 Res 13025.9610
0.0933333333333333
ho
jH 28
k 0.1338
De 0.0825
Cp 1.1189
μ 0.0407
μ/μw 0.07596014072
ho 4
Shell Side
Re
Re 13025.9610
f
f 0.003 figure 29
Number of Crosses
L 16 ft
B 5.3125 in
N+1 36.1411764706
∆Ps
f 0.003
Gs 6428.89651564 lb/ft2.jam
Ds 1.7708 ft
N+1 37
De 0.0825 ft
s 1
∆Ps 0.00188646645 psi
Data CP Gas
joule/mol.K
b c d e Cpi, J/mol.K Cpi, J/g.K
0.020178 -0.000038549 3.188E-08 -8.7585E-12 29.213213541 14.6066067703
-0.0035395 0.000010076 -4.3116E-09 2.5935E-13 29.397343002 1.0499051072
total
J/mol.K
J/g.K
BTU/lb.F
al Conductivity of Gas
B C k, W/m.K x.k, W/m.K

0.00046 0.0000 2.3165E-01 0.2314666944198
0.00008 0.0000 6.2617E-02 4.924075509E-05
k campuran 0.2315159351749
W/m.K
BTU/hr.ft.F
miuw a b c
-10.2158 1.79E+03 0.0177
B*T + C*T^2 + D*T^3 + E*T^4 T (K)

D E
0.00000053469 0
Viscosity 0.0168316845 cp
(Figure 15 Kern) 0.04071745362 lb/ft/hr
a b c d e
cp 33.933 -8.42E-03 2.99E-05 -1.78E-08 0.0000
A B n Tc rho, gr/cm3
rho 0.34710 0.27400 0.2857 647.13 0.827205504
A B C k, W/m.K
k 0.00053 4.7093E-05 4.9551E-08 2.35E-02
a b c d μ, cp
miu -36.826 4.29E-01 -1.62E-05 1.68E-02
Diff.
4
77
73
hell Side
inch
inch 0.25 dari ID shell

inch figure 28
campuran
inch
inch
inch
inch
inch
ID s kecilin
in
in
in as kecilin
in
ft2
de besarin
gs besarin
lb/jam
lb/ft2.jam
inch (Fig. 28)
ft
lb/ft.hr
BTU/jam.F.ft
ft
BTU/lb.F
lb/ft.jam
(asumsi)
BTU/jam.ft2.F
∆Ps
f 0.003
Gs 6428.897 lb/ft2.jam
L 16 ft
n 1
D 0.0825 ft
s 1.00000
∆Ps 0.0002303349 psi
Data rho Gas
gr/ml
Compound A B n
x.Cp, J/g.K x.Cp, J/mol.K
14.4474249754 29.1902
0.01144179357 0.0231
rho campuran
14.4589 29.2134
1.5489 kg/m3 1000
rho campuran
0.0967 lb/ft3 62.4273708
Viscosity of Gas
Compound a b c d μ, cp
H2 27.758 2.12E-01 -3.28E-05 0.011590432
0 3.844 4.01E-01 -1.43E-04 0.01544703
N2 42.606 4.75E-01 -9.88E-05 0.023505452
total
0.0116 cP
μ
0.0281 lb/ft.hr
-10.2158 1.79E+03 0.0177 -1.26E-05 0.152709066
d μ, cp
-1.26E-05 0.152709065969
0.3694
Cpi, J/mol.K Cpi, J/g.K
35.076317987 1.948684332613
rho, kg/m3
827.205504002
gr/V=P/RT*Mr
Tc rho, gr/cm3 rho, kg/m3 x/rho, kg/m3
0.00056551214 0.565512144898 0.559349
0.00791717003 7.917170028578 0.086281
rho campuran 1.548875
xi.μ, cp
0.01158131789
0
1.84842516E-05
0.0115998021
4
HE-101
3
1 2
TK-101 P-101
12
10
11
CO-101 HE-102
0
9
10
11
CO-101 HE-102
0
9
P-103
25
5 6 19
HE-101 VAP-101 KD-101 HE-202
7
18
12 R-201
13
HE-102 EV-101 HE-201
14 15
13
HE-102 EV-101 HE-201
14 15
17
20
23
19
HE-202 MD-301 MD-302
22
HE-304
21 HE-303
24
18
TP-301
HE-201 CD-201 KD-201

15 16
HE-201 CD-201 KD-201
15 16
Viskositas liquid
log10μ = A+B/T+CT+DT^2
Komponen A B C D Tmin, K Tmax, K

Hidrogen -7.0154 4.08E+01 2.37E-01 -4.08E-03 14 33
Nitrobenzene -7.771 1.40E+03 0.0147 -1.15E-05 273 719
Anilin -13.863 2.51E+03 0.0257 -1.83E-05 268 699
Benzene -7.4005 1.18E+03 1.49E-02 -1.37E-05 285 562
Nitrogen -15.6104 4.65E+02 1.63E-01 -6.34E-04 63 125
Air -10.2158 1.79E+03 1.77E-02 -1.26E-05 273 643
Viskositas gas
μG = A + BT + CT2
Komponen A B C Tmin, K Tmax, K
Hidrogen 27.758 2.12E-01 -3.28E-05 150 1500
Nitrobenzene -16.569 2.92E-01 -2.55E-05 450 1000
Anilin -6.918 2.59E-01 -3.43E-05 458 1000
Benzene -0.151 2.57E-01 -8.98E-06 287 628
Nitrogen 42.606 4.75E-01 -9.88E-05 150 1500
Air -36.826 4.29E-01 -1.62E-05 280 1073
Kapasitas panas gas
Komponen A B C D E
Nitrobenzen -16.202 0.56182 -3.9302E-04 1.004E-07 -1.2252E-12
Hidrogen 25.399 2.0178E-02 -3.8549E-05 3.1880E-08 -8.7585E-12
Anilin -22.062 0.57313 -4.5651E-04 1.841E-07 -2.9867E-11
Benzen -31.368 0.47460 -3.1137E-04 8.524E-08 -5.0524E-12
Nitrogen 29.342 -3.5395E-03 1.0076E-05 -4.3116E-09 2.5935E-13
Air 33.933 -8.4186E-03 2.9906E-05 -1.7825E-08 3.6934E-12
Konduktivitas termal liquid
Komponen A B C
Nitrobenzen -1.3942E+00 6.5710E-01 7.1900E+02 1.6330E-01
Hidrogen -0.143 2.3627E-02 -5.1480E-04
Anilin -1.3485 6.89E-01 6.9900E+02 1.9620E-01
Benzen -1.6846 1.05E+00 5.6216E+02 1.9620E-01
Nitrogen 0.213 -4.2050E-04 -7.2951E-06
Air -0.2758 4.6120E-03 -5.5391E-06
Densitas liquid
Komponen A B n Tc Tmin
Nitrobenzen 0.3614 0.24731 0.2857 719 278.91
Hidrogen 0.03125 0.3473 0.2756 33.18 13.95
Anilin 0.3119 0.25 0.28571 699 267.13
Benzen 0.3009 0.2677 0.2818 562.16 278.68
Nitrogen 0.31205 0.28479 0.2925 126.1 63.15
Air 0.3471 0.274 0.28571 647.13 273.16
Densitas gas
Komponen A B n Tc Tmin
Nitrobenzen 0.3614 0.24731 0.2857 719 278.91
Hidrogen 0.03125 0.3473 0.2756 33.18 13.95
Anilin 0.3119 0.25 0.28571 699 267.13
Benzen 0.3009 0.2677 0.2818 562.16 278.68
Nitrogen 0.31205 0.28479 0.2925 126.1 63.15
Air 0.3471 0.274 0.28571 647.13 273.16
Vapor preassure
Komponen A B C D E
Nitrobenzen -54.4937 -2.11E+03 2.93E+01 -4.48E-02 2.02E-05
Hidrogen 3.4132 -4.13E+01 1.09E+00 6.6896E-10 1.46E-04
Anilin 124.3764 -7.17E+03 -4.28E+01 1.73E-02 5.71E-15
Benzen 31.7718 -2.73E+03 -8.4443 -5.35E-09 2.72E-06
Nitrogen 23.8572 -4.77E+02 -8.67E+00 2.01E-02 -2.41E-11
Air 29.8605 -3.15E+03 -7.30E+00 2.42E-09 1.81E-06
Enthalpy Vaporization
Komponen A Tc n Tmin Tmax
Nitrobenzen 67.414 719 3.80E-01 278.91 719
Hidrogen 0.659 33.18 3.80E-01 13.95 33.18
Anilin 72.038 699 0.459 267.13 699
Benzen 49.888 562.16 0.489 278.68 562.16
Nitrogen 9.43 126.1 0.533 63.15 126.1
Air 52.053 647.13 0.321 273.16 647.13
Enthalpy Formation
Komponen A B C deltaHF 298

Nitrobenzen 67.414 719 3.80E-01 278.91
Hidrogen 0.659 33.18 3.80E-01 13.95
Anilin 105.261 –7.3513E–02 3.7553E–05 86.86
Benzen 101.403 –7.2136E–02 3.2877E–05 82.93
Nitrogen 9.43 126.1 0.533 63.15
Air 52.053 647.13 0.321 273.16
Konduktivitas termal GAS
Komponen A B C
Nitrobenzen -1.0283E-02 5.7531E-05 1.0851E-08
Hidrogen 0.040 4.5918E-04 -6.4933E-08
Anilin -1.2794E-02 7.1020E-05 2.1005E-08
Benzen -5.6500E-03 3.4493E-05 6.9298E-08
Nitrogen 0.00309 7.5930E-05 -1.1014E-08
Air 0.00053 4.7093E-05 4.9551E-08
μG = A + BT + CT2
Komponen A
Nitrobenzen 51.773
Hidrogen 50.607
Anilin 63.288
Benzen -31.663
Nitrogen 76.452
Air 92.053
8.5964E-06 ###
-5.2139E-07 ###
-5.2139E-07 ###
Tmax
719
33.18
699
562.16
126.1
647.13
Tmax
719
33.18
699
562.16 BELUM
126.1
647.13
log10 Pv = A + B/T + C log10T + DT + ET2
Tmin Tmax
278.91 719 T 393.15 120
13.95 33.18
267.13 699 3.1724322974
276.68 562.16 1487.4154812
63.15 126.1 1.9571256331
273.16 647.13
TB
483.95
20.39
457.6
353.24
77.35
373.15
B C D
0.91277 -2.1098E-03 2.009E-06
### 3.0930E-01 -4.1480E-03
0.98960 -2.3583E-03 2.330E-06
1.30430 -3.6078E-03 3.824E-06
### -2.6690E-03 5.0057E-05
### -2.1103E-04 5.3469E-07
HEAT EXCHANGER-01
COLD FLUID
Nitrobenzen 1.337990415076 164.7200 0.0099
Anilin 132.92325698762 12379.0100 0.9881
Air 0.2637222222222 4.7470 0.0020
Total 134.5250 12548.4770 1.0000

27664.6234 lb/jam
423.1500 K
Tin 150.0000 °C
302.0000 °F
466.1500 K
Tout 193 °C
379.4000 °F
444.6500 K
340.7000 °F
Nilai Q
B 1.3380 217.1443 290.5370
T 132.9233 241.8486 32,147.3000
D 0.2637 79.5708 20.9846
DA 0.0000 0.0000 0.0000
DB 0.0000 0.0000 0.0000
DDB 0.0000 0.0000 0.0000
Total 32,458.8216
1395729.3272 kJ/jam
Q
1322915.5239 BTU/jam
HOT FLUID
15244.998580683 lb/hr
Sat. steam 6915009.3962093 g/hr
384167.1886783 mol/hr
199.0000 °C
Tin 472.1500 K
390.2000 °F
199.0000 °C
Tout 472.1500 K
390.2000 °F
472.1500 K
390.2000 °F
13430214.6848 kJ/jam
Q
12729573.8149 BTU/jam
acc 11406658.2910
LMTD

390.2000 High 379.4000 10.8000
390.2000 Low 302.0000 88.2000
0.0000 Diff 77.4000 -77.4000
LMTD 36.8561 °F
Koreksi Nilai LMTD
R 0.0000 S 0.8776
FT 1
FT.LMTD 36.8561 °F
tc = ta = 0.0000 °F
Tc = Ta = 0.0000 °F
Nilai A
UD =100 - 200
Ud 140 BTU/ft2.F.hr
A 256.3864038082 ft2 (Digunakan HE shell and tube karena A >
Lay Out HE
Tube Side
Tube Pitch triangular (Karena pressure drop yang dihasilkan lebih kecil)
OD 0.75 inch on
L 13 ft
Passes 4
a" 0.1963 ft2 (Table 10)

BWG 15
a' 0.289 sqin
ID tube 0.606 in
100.4688 tubes
Nt
422 tubes table 9
Shell Side
ID 25 inch
Passes 1
Tube Side
Nt 422
L 13 ft
OD 0.75 inch
BWG 15
Passes 4
Koreksi UD
A 1076.9018 ft2
UD 33.3309
Tube Side (Cold Fluid)

Flow Area tube
Nt  at '
at 
144  n
Nt 422
at' 0.289
n 4
at 0.2117 ft2
Mass Velocity
G_t=m_h/a_t
mc 27664.6560 lb/jam
at 0.2117 ft2
Gt 130658.4385617 lb/ft2.jam
Reynold

ID
0.0505 ft
Gt 130658.4385617 lb/ft2.jam
μ 0.9564 lb/ft.jam
ReT 6899.1648
jH
L x n /D 1029.7030
jH 160 figure 24
hi
jH 165
k 0.0855 BTU/jam.F.ft
De 0.0505 ft
Cp 0.6178 BTU/lb.F
μ 0.9564 lb/ft.jam
μ/μw 1 (Asumsi)
hi 531.9498 BTU/jam.ft2.F
hio
ID 0.606 in
OD 0.75 in
UC

Rd
Rd 0.0270 BTU/jam.ft2.F min 0,003
Pressure Drop
Tube Side
Re
Re 6899.1648
f
f 0.00016 figure 26
∆Pt
f 0.00016
Gt 130658.4385617 lb/ft2.jam
L 13 ft
n 4
D 0.0505 ft
s 0.882929022807
∆Pt 0.061025392317 psi
∆Pr
v2/2g' 0.09 figure 27

n 4
s 0.8829
∆Pr 1.6309 psi
∆Ptotal
Summary
Tube Shell
Nt 422 ID, in 25
Pitch, in 1 L, ft 13
BWG 15
Pass, n 4
a", ft2/ft 0.1963
Triangle Pitch

199.00 Tin, °C m, kmol/jam
199.00 Tout, °C 0.26
1500.0000 houtside 0.0000
UC 334.0854
UD 33.3309
Rd calculated 0.0270
Rd required 0.003
1.69196 ∆P Perhitungan 8.3052
10 ∆P yang diizinkan 10
HANGER-01
Mr xi, massa Data CP Liquid

123 0.0131266925859 Data joule/mol.K
93 0.9864950144946 Compound a b
18 0.0003782929195 Nitrobenzen 51.773 0.91277
Anilin 63.288 0.98960
Air 92.053 -3.9953E-02
flowrate air pendingin > condensate 241.2847 J/mol.K

(flowrate >> di shell : air pendingin di shell Cp 2.5867 J/g.K
T >> di tube : condensate di tube 0.6178 BTU/lb.F
Thermal Conductivity of liquid
Compound A B
Nitrobenzen -1.3942E+00 6.5710E-01
Anilin -1.3485 6.89E-01
Air -0.2758 4.6120E-03
mCpTin mCpTout
87,742.1710 110,229.7340
9,708,484.5960 12,196,685.6150
6,337.3447 7,961.5516 k campuran
0.0000 0.0000
0.0000 0.0000 0.1479 W/m.K
k
0.0000 0.0000 0.0855 BTU/hr.ft.F
9,802,564.1118 12,314,876.9007
Heat Capacity of Inorganic Gas Cp (J/mol.K) = A + B*T + C*T^2 + D*T^3 + E*T^4

Rumus Nama A B C D
H2O Water 33.933 -8.4186E-03 2.9906E-05 -1.7825E-08

Cp
0.4635 BTU/lb.F
Mr 18 g/mol
Enthalpy of Evaporation 835 btu/lb

(Table 7 Kern)
Specific volume (vapor) 2 ft3/lb
P 225 psia

199.0000 High 193.0000 6.0000
199.0000 Low 150.0000 49.0000
0.0000 Diff 43.0000 -43.0000
nakan HE shell and tube karena A > 200 ft2)
Shell Side
an lebih kecil) ID 25 inch
Passes 1
1 in. triangular pitch Baffle 6.25 inch
De 0.73 inch
Shell Side (Hot Fluid)
Jarak Baffle
IDs 25 inch
B 6.25 inch
Clearance
PT 1 inch
ODT 0.75 inch
C 0.25 inch
Flow Area shell
IDs 25 in
C 0.25 in
B 6.25 in
PT 1 in
as 0.2713 ft2
Mass Velocity
G_s=m_c/a_s
mh 15244.9986 lb/jam
Gs 56199.162768 lb/ft2.jam
Reynold
0.73 inch
De
0.0608 ft
μ 0.0556 lb/ft.hr
Res 61445.5725
Shell Side
Re
Re 61445.5725
f
f 0.0013 figure 29
Number of Crosses
L 13 ft
B 6.25 in
N+1 24.96
∆Ps
f 0.0013
Gs 56199.162768 lb/ft2.jam
Ds 2.0833 ft
N+1 24.96
De 0.0608 ft
s 0.0080955272
∆Ps 8.3051815935 psi
CP Liquid
Compound
c d Cpi, J/mol.K Cpi, J/g.K x.Cp, J/g.K x.Cp, J/mol.K Nitrobenzen
-2.1098E-03 2.009E-06 217.14429851 1.7638233978 0.023153168 2.1597
-2.3583E-03 2.330E-06 241.84857274 2.5969201081 2.56184874 238.9690
-2.1103E-04 5.3469E-07 79.570788452 4.4205993585 0.001672281 0.1560
total 2.5867 241.2847
vity of liquid Viscosity
C k, W/m.K x.k, W/m.K Compound

7.1900E+02 1.2729E-01 0.0012659849 Nitrobenzen
6.9900E+02 1.4706E-01 0.1453116086 Anilin
-5.5391E-06 6.7977E-01 0.001332619 Air
mpuran 0.1479102125
D*T^3 + E*T^4 T (K)

E
3.6934E-12
0.023 cp
0.0556391984 lb/ft/hr
0.25 dari ID shell
figure 28
(Fig. 28)
Data rho liquid
gr/ml
Compound A B n Tc rho, gr/cm3rho, kg/m3
x.rho, kg/m3
Nitrobenzen 0.3614 0.24731 0.2857 719 1.0441076 1044.1076 1.26E-05
Anilin 0.3119 0.25 0.28571 699 0.8811297 881.12969 0.00112
Air 0.3471 0.274 0.28571 647.13 0.8787681 878.76811 4.3E-07
882.9379 kg/m3
rho campuran
55.1195 lb/ft3
Viscosity of liquid
a b c d μ, cp xi.μ, cp
-7.771 1.40E+03 0.0147 -1.15E-05 0.4386242 0.0043626
-13.863 2.51E+03 0.0257 -1.83E-05 0.3953808 0.3906732
-10.2158 1.79E+03 1.77E-02 -1.26E-05 0.1591418 0.000312
total 0.395348
0.3953 cP
0.9564 lb/ft.hr
HEAT EXCHANGER - 01 - Sebelum
HOT FLUID
Nitrobenzen 1.33799041507595 164.7200 0.0099
Anilin 132.923256987619 12379.0100 0.9881
Air 0.263722222222222 4.7470 0.0020
Total 134.5250 12548.4770 1.0000

27664.6234 lb/jam
423.15 K
Tin 150 °C
302 °F
466.15 K
Tout 193 °C
379 °F
444.65 K
Taverage 172 °C
341 °F
Nilai Q
Nitrobenzen 1.3380 217.1443 290.5370
Anilin 132.9233 241.8486 32,147.3000
Air 0.2637 79.5708 20.9846
Total 32,458.8216
1395729.3272 kJ/jam
Q
1322915.5239 BTU/jam
COLD FLUID
122664.648627494 lb/hr GoalSeek

cold water
cold water 55639703.3002421 g/hr
3091094.62779123 mol/hr
199.0000 °C
Tin 472.1500 K
390.2000 °F
199.0000 °C
Tout 472.1500 K
390.2000 °F
472.1500 K
390.2000 °F
0.0000 kJ/jam
Q
0.0000 BTU/jam
acc -1322915.5239 GoalSeek
LMTD

302 High 390 -88
379 Low 390 -11
-77 Diff 0 -77
LMTD -36.8561 °F
Koreksi Nilai LMTD
R #DIV/0! S 0.0000
FT 0.97 Fig.18
FT.LMTD -35.7504 °F
tc = ta = 340.7000 °F
Tc = Ta = 390.2000 °F
DARI SINI
Tinggal Trial Trial
Nilai A
UD =100 - 200 Table 8
Ud 100 BTU/ft2.F.hr
A -370.042232300433 ft2 (Digunakan HE double pipe karen
Lay Out HE
Tube Side
Tube Pitch triangular (Karena pressure drop yang dihasilkan lebih kecil)
OD 0.75 inch on
L 12 ft
Passes 1
a" 0.1963 ft2 (Table 10)

BWG 12
a' 0.223 sqin
ID tube 0.532 in
-157.0904 tubes
Nt
203 tubes table 9
Shell Side
ID 17.25 inch
Passes 1
Tube Side
Nt 203
L 12 ft
OD 0.75 inch
BWG 12
Passes 1
Koreksi UD
A 478.1868 ft2
UD -77.3845
Tube Side water

Flow Area tube
N a '
at  t t
144  n
Nt 203
at' 0.223
n 1
at 0.3144 ft2
Mass Velocity
G_t=m_h/a_t
mc 122664.6486 lb/jam
at 0.3144 ft2
Gt 390194.380312335 lb/ft2.jam
Reynold

ID
0.044333333333333 ft
Gt 390194.380312335 lb/ft2.jam
μ 0.0392 lb/ft.jam
ReT 441098.2028
jH
L x n /D 270.6767
jH 40 figure 24
v 1.7341972458326 fps cp
koreksi 1.025 miu
Ta 390 F k
hi kern 560 muw
hicor 574
UC

Rd
UD -77.3845 BTU/jam.ft2.F
Pressure Drop
Tube Side
Re
Re 441098.2028
f
f 0.00025 figure 26
∆Pt
f 0.00025
Gt 390194.380 lb/ft2.jam
L 12 ft
n 1
D 0.044333333333333 ft
s 1
∆Pt 0.098685282880041 psi
∆Pr
Gt 390194.380 lb/ft2.jam
v2/2g' 0.0021 figure 27
n 1
s 1.0000
∆Pr 0.0084 psi
∆Ptotal
Summary
Tube Shell 17.25

Nt 203 ID, in 1
Pitch, in 1 L, ft
BWG 12
Pass, n 1
a", ft2/ft 0.1963
Triangle Pitch
HE-05, Heater
Steam Isooktan
199 Tin, °C 150
199 Tout, °C 193
86 h, Btu/jam. ft2.F 759.49
UC = 77.0833 Btu/jam. ft2.F
UD = -77.3845 Btu/jam. ft2.F
Rd required = 0.003
- 01 - Sebelum R-01
Mr xi, massa Data CP Liquid

123 0.01312669258588 Data
93 0.98649501449459 Compound a
18 0.00037829291953 Nitrobenzen 51.773
Anilin 63.288
Air 92.053

Thermal Conductivity of liquid
Compound A
Nitrobenzen -1.3942E+00
Anilin -1.3485
Air -0.2758
mCpTin mCpTout
87,742.1710 110,229.7340
9,708,484.5960 12,196,685.6150
6,337.3447 7,961.5516 k campuran
0.1479
k
0.0855
9,802,564.1118 12,314,876.9007

Rumus Nama A B C
H2O Water 33.933 -8.4186E-03 2.9906E-05

0.4635 BTU/lb.F
Mr 18 g/mol
Enthalpy of Evaporation 958.75 btu/lb (Table 7 Kern)

k 6.30E-01 W/m.K
0.3640 BTU/hr.ft.F

199 High 193
199 Low 150
0 Diff 43
an HE double pipe karena A < 200 ft2)
Shell Side
an lebih kecil) ID 17.25
Passes 1
1 in. triangular pitch Baffle 5.18
De 0.73
Shell Side
Jarak Baffle
IDs 17.25
B 5.175
Clearance
PT 1
ODT 0.75
C 0.25
Flow Area shell
IDs 17.25
C 0.25
B 5.2
PT 1
as
G_s=m_c/a_s 0.1550
Mass Velocity
G_s=m_c/a_s
mh 27664.6234
Gs 178503.933992
Reynold
0.73
De
0.4635 0.0608
0.039217157129656 μ 0.9564
3.64E-01 Res 11354.2141
0.0443333333333333
ho
jH 150
k 0.0855
De 0.0608
Cp 0.6178
μ 0.9564
μ/μw 24.3868786369
ho 759
Shell Side
Re
Re 11354.2141
f
f 0.0016 figure 29
Number of Crosses
L 12 ft
B 5.175 in
N+1 27.8260869565
∆Ps
f 0.0016
Gs 178503.933992 lb/ft2.jam
Ds 1.4375 ft
N+1 29
De 0.0608 ft
s 0.88191188857
∆Ps 0.75889921462 psi
Data CP Liquid
joule/mol.K
b c d Cpi, J/mol.K Cpi, J/g.K x.Cp, J/g.K
0.91277 -2.1098E-03 2.009E-06 217.14429850763 1.7638233978 0.02315316752
0.98960 -2.3583E-03 2.330E-06 241.84857274333 2.5969201081 2.56184873964
-3.9953E-02 -2.1103E-04 5.3469E-07 79.570788452404 4.4205993585 0.00167228144
total 2.5867
J/mol.K
J/g.K
BTU/lb.F
l Conductivity of liquid

6.5710E-01 7.1900E+02 1.2729E-01 0.0012659849179
6.89E-01 6.9900E+02 1.4706E-01 0.1453116085578
4.6120E-03 -5.5391E-06 6.7977E-01 0.0013326189752
k campuran 0.1479102124508
W/m.K
BTU/hr.ft.F
B*T + C*T^2 + D*T^3 + E*T^4 T (K)

D E
-1.7825E-08 3.6934E-12
a b c d e
cp 33.933 -8.4186E-03 2.9906E-05 -1.7825E-08 3.6934E-12
rho 0.34710 0.27400 0.2857 647.13 0.84604937656
A B C k, W/m.K
k -0.2758 4.61E-03 -5.54E-06 6.30E-01
a b c d μ, cp
miu -36.826 4.29E-01 -1.62E-05 1.62E-02
2.9768996637
2.98E+00
Diff.
6
49
-43
hell Side
inch

inch figure 28
campuran
inch
inch
inch
inch
inch
ID s kecilin
in
in
in as kecilin
in
ft2
de besarin
gs besarin
lb/jam
lb/ft2.jam
inch (Fig. 28)
ft
lb/ft.hr
BTU/jam.F.ft
ft
BTU/lb.F
lb/ft.jam
(asumsi)
BTU/jam.ft2.F
∆Ps
f 0.0016
Gs 178503.934 lb/ft2.jam
L 12 ft
n 1
D 0.0608 ft
s 0.88294
∆Ps 0.1090999445 psi
Data rho liquid
gr/ml
Compound A B n Tc
x.Cp, J/mol.K Nitrobenzen 0.3614 0.24731 0.2857 719
2.1597 Anilin 0.3119 0.25 0.28571 699
238.9690 Air 0.3471 0.274 0.28571 647.13
0.1560
rho campuran
241.2847
882.9379 kg/m3 1000
rho campuran
55.1195 lb/ft3 62.4273708
Viscosity of liquid
Nitrobenzen -7.771 1.40E+03 0.0147 -1.15E-05 0.438624211
Anilin -13.863 2.51E+03 0.0257 -1.83E-05 0.395380794
Air -10.2158 1.79E+03 1.77E-02 -1.26E-05 0.159141804
total
0.3953 cP
μ
0.9564 lb/ft.hr
-36.826 4.29E-01 -1.62E-05 1.62E-02

Cpi, J/mol.K Cpi, J/g.K
34.932359787 1.940686654832
rho, kg/m3
846.049376562
rho, gr/cm3 rho, kg/m3 x/rho, kg/m3
1.04410755402 1044.10755402 1.2572165E-05
0.88112969311 881.129693112 0.00111957981
0.87876811488 878.768114883 4.3048093E-07
882.937921692
xi.μ, cp
0.00436257292
0.39067321918
0.00031198097
0.3953477731
MENARA DISTILASI 302
Mr
Komponen
kg/kmol
Nitrobenzen 123.11
Hidrogen 2
Anilin 93.129
Benzen 78.114
Nitrogen 28
Air 18
Komposisi feed, distilat, dan bottom
Feed Distilat
Komponen
kg/jam kmol/jam x(massa) x(mol) kg/jam
Nitrobenzen 164.72 1.3380 0.0131 0.00995 0.16
Hidrogen 0 0 0 0 0
Anilin 12379.01 132.9233 0.9865 0.98809 12366.59
Benzen 0 0 0 0 0.00
Nitrogen 0 0 0 0 0.00
Air 4.747 0.2637 0.0004 0.00196 4.79
Total 12548.48 134.5250 1 1 12371.55
Tekanan uap
Komponen A B C D E
Nitrobenzen -54.494 -2112.3 29.321 -4.4839E-02 2.0162E-05
Hidrogen 3.4132 -4.1316E+01 1.0947E+00 -6.6896E-10 1.4589E-04
Anilin 124.38 -7167.6 -42.763 1.7336E-02 5.7138E-15
Benzen 31.772 -2725.4 -8.4443 -5.3534E-09 2.7187E-06
Nitrogen 23.8572 -4.7668E+02 -8.6689E+00 2.0128E-02 -2.4139E-11
Air 29.8605 -3.1522E+03 -7.3037E+00 2.4247E-09 1.8090E-06
1. Perhitungan Suhu Feed Masuk
T, K 465.4019843 K 192.401984331 C
P, mmHg 912 mmHg 1.2 atm
Komponen Fi,kmol/jam xi log P Pi, mmHg Ki, Pt/Po

Nitrobenzen 1.3380 0.00995 2.6896 489.3776 1.8636
Hidrogen - - - - -
Anilin 132.9233 0.98809 2.9630 918.3123 0.9931
Benzen - - - - -
Nitrogen - - - - -
Air 0.2637 0.00196 3.9942 9868.2957 0.0924
Total 134.5250 1.00000
2. Perhitungan Suhu Top Menara (Σx = 1)

Tdew
T,K 456.9773255 K 183.827325488 C
Pt,mmHg 760 mmHg 1 atm
Komponen Di, kmol/jam yi log P Pi, mmHg Ki, Pt/Po

Nitrobenzen 0.0013 0.00 2.59 393.0343 1.9337
Hidrogen - - - - -
Anilin 132.79 0.9980 2.87 745.2113 1.0198
Benzen - - - - -
Nitrogen - - - - -
Air 0.2661 0.0020 3.91 8189.6180 0.0928
Total 133.06 1.00
3. Perhitungan Suhu Bottom Menara (Σx = 1)
T,K 496.7828007 K 223.782800668

Pt,mmHg 1064 mmHg 1.4 atm
Komponen Bi, kmol/jam xi log P Pi, mmHg Ki, Pt/Po

Nitrobenzen 1.3366 0.9095 3.0089 1020.7988 1.0423
Hidrogen - - - - -
Anilin 0.1329 0.0905 3.2680 1853.6198 0.5740
Benzen - - - - -
Nitrogen - - - - -
Air 0.0000 0.0000 4.2697 18609.3262 0.0572
Total 1.47 1.00
4. Distribusi non-key component

Feed Tfeed 465.401984331 K Komponen αaverage
Komponen Pi αi Air 19.4900
Air 9868.30 25.1080 Anilin 1.8555
Anilin 918.3123 2.3365 Nitrobenzen 1
Nitrobenzen 393.0343 1
Distillat Tdistilat 456.977325488 Light Key

Komponen Pi αi Distilat 132.7899
Air 8189.62 20.8369 Bottom 0.1329
Anilin 745.2113 1.8960 d/b 998.9979
Nitrobenzen 393.0343 1 log(di/bi) 2.99956457143
α avg 1.8555
Bottom Tbottom 496.782800668 log α 0.2684647279
Komponen Pi αi
Air 18609.33 18.2302 A -2.9995674
Anilin 1853.6198 1.8159 LK C 22.3460713
Nitrobenzen 1020.7988 1 HK
Komponen α F, kmol/jam log(di/bi) di/bi bi

Air 19.4900 0.2637 25.8227 6.65E+25 0.0000
Anilin 1.8555 132.9233 2.9996 998.9979 0.1329
Nitrobenzen 1 1.3380 -2.9996 0.0010 1.3367
Jumlah 134.5250 1.4696
5. Jumlah Stage Minimum
Komponen xd xb α
Anilin(LK) 0.9980 0.0905 1.8555 LK
Nitrobenzen(HK) 0.000010 0.9095 1.0000 HK
Nm 22.346071297
Nmstandar 23
6. Refluks minimum
dengan q=1 saturated liquid

A B
Komponen α F xi,F α*xi,F α-θ
Air 19.4900 0.2637 0.0020 0.0382 18.4854
Anilin 1.8555 132.9233 0.9881 1.8334 0.8509
Nitrobenzen 1.0000 1.3380 0.0099 0.0099 -0.0046
Jumlah 134.5250 1.0000 sigma
tebak θ
θ 1.004612188
Komponen α di xi,d α*xi,di α-θ
Air 19.4900 0.2661 0.0020 0.0390 18.4854
Anilin 1.8555 132.7899 0.9980 1.8518 0.8509
Nitrobenzen 1.0000 0.0013 0.0000 0.0000 -0.0046
Jumlah 133.0574 1.0000 sigma
Rm+1
Rm
Rm/(Rm+1)
7. Perhitungan jumlag stage aktual
ambil R=1.5Rm
R= 1.76428014
R/(R+1)= 0.6382421646 0.65
Rm/(Rm+1)= 0.5404806157 0.55
Berdasarkan grafik disamping

diperoleh nilai Nm/N = 0.60
Nm/N= 0.6
Nm 22.346071297
N 37.243452161
Nact 38
7. Feed location
Komponen xf xd xb
Anilin(LK) 0.9881 0.9980 0.0905 .
Nitrobenzen(HK) 0.0099 0.0000 0.9095
D 133.05736132
B 1.4695 Ns=Nact/(Nr/Ns+1)
Log(Nr/Ns) -0.4015289422
Nr/Ns 0.3967080907
Nr/Ns= 0.3967080907
Ns 27.206830299 28 10.7931697009
Feed masuk pada stage 28
Nr 10 Nr=Nact-Ns
8. Effisiensi Plate
Data Viskositas Cairan log10μ = A+B/T+CT+DT^2
Komponen A B C D log μ
Air -1.0216E+01 1.7925E+03 1.7730E-02 -1.2631E-05 -8.7438E-01
Anilin -13.863 2.51E+03 0.0257 -1.83E-05 -4.9928E-01
Nitrobenzen -7.771 1.40E+03 0.0147 -1.15E-05 -4.3913E-01
Column Efficiency
Tavg = 476.88006308
μ avg = 0.3168588807
α avg = 1.8555
Eff = 58.496755123 0.58496755123 %
Sehingga N real stage= N/effisiensi

N real stage 63.6675522987
Sebelum Efisiensi Setelah Efisiensi

N Asli N Pembulatan N Asli N Pembulatan
N= 37.2434521612 38 63.6675522987 64
N tanpa Reboile36.2434521612 37 62.6675522987 63
Mechanical design
Perhitungan Diameter Menara
a.Perhitungan Diameter Puncak Menara

D = 12371.5490 kg/jam
R = 1.7643 V = Lo + D T, K =
Lo = R*D V = 34198.427202 kmol/jam P,atm =
Lo = 21826.8782 kg/jam
Komponen BM Di,kg/jam yd Li=R*Di Vi=Li+Di Vi,kmol/j
Air 18 4.7894 0.000387 8.4498 13.2392 0.7355
Anilin 93.129 12366.5949 0.999600 21818.1378 34184.7327 367.0686
Nitrobenze 123.11 0.1647 0.000013 0.2906 0.4553 0.0037
Total 12371.5490 1.0000 21826.8782 34198.4272 367.8078
Densitas uap, rho v = P.BM / ( Rgas.T) R gas = 0.08206 atm.m3/kmol.K

= 2.4827 kg/m3
Densitas cairan, rho L = 688.3707 kg/m3
Liquid vapor flow factor : FLV = 0.0383

Dari Fig 11.27 Coulson didapat u/plate spacing = 0,45 m, maka K1 = 8.10E-02
Maximum supervisial velocity terjadi pada keadaan flooding
Vf = 1.3463 m/s (pers. 11.81, Coulson)
Supaya tidak terjadi flooding maka diambil supervisial velocity 80 % flow rate max
Vf = 1.0771 m/s
Kecepatan volume fasa uap :
Qv = 3.8313 m3/s
Net Area ( An ) : An = 3.5572 m2
Luas downcomer 12 % dari luas total
Total area ( At ) : At = 4.0422 m2
Diameter puncak menara : D 2.12871695544
D = 2.2692 m
b.Perhitungan Diameter Dasar Menara

D = 12371.5490 kg/jam = 133.0574 kmol/jam
F = 12548.48 kg/jam = 134.5250 kmol/jam
R = 1.7643
q = 0
T, K = 496.7828007
P,atm = 1.4000
Komponen BM Bi,kg/jam Bi,kmol/j xi yi

Air 18 0.0000 0.0000 0.000000 0.000000
Anilin 93.129 12.3790 0.1329 0.090452 0.051920
Nitrobenzen 123.11 164.5520 1.3366 0.909548 0.948041
Total 176.9310 1.4695 1 1
Komponen BM Li,kmol/j Li=Fi+R*Di Vi=Li-Bi Vi,kmol/j BM mix

Air 18 0.0000 0.0000 0.0000 0.0000 0.0000
Anilin 93.129 19.2296 1790.8363 1778.4573 19.0967 4.8353
Nitrobenzen 123.11 350.0336 43092.6385 42928.0865 348.6970 116.7134
Total 369.2632 44883.4748 44706.54381 367.8078 121.5486
Densitas uap, rv = P.BM / ( Rgas.T) R gas = 0.08206 atm.m3/kmol.K

= 4.1743 kg/m3
Densitas cairan, rL = 948.4231 kg/m3
Liquid vapor flow factor : FLV = 0.067

Dari Fig 11.27 Coulson didapat u/plate spacing = 0,45 m, maka K1 = 7.80E-02
Maximum supervisial velocity terjadi pada keadaan flooding
Vf = 1.1731 m/s (pers. 11.81, Coulson)
Supaya tidak terjadi flooding maka diambil supervisial velocity 80 % flow rate max
Vf = 0.9385 m/s
Kecepatan volume fasa uap :
Qv = 2.9750 m3/s
Net Area ( An ) : An = 3.1699 m2
Luas downcomer 12 % dari luas total
Total area ( At ) : At = 3.6022 m2
Diameter bottom menara : D = 2.0095 m
D = 2.1421 m
Diambil D= 2.1421 m
Perhitungan Tinggi Menara
Jarak ruang kosong diatas plate pertama = 1m

Jarak ruang kosong dibawah plate terakhir = 2m
Plate Spacing = 0.45 m
N = 38
Tinggi Menara = 20.1 m
L/D = 9.3831
Distilat Bottom
kmol/jam x(massa) x(mol) kg/jam kmol/jam x(massa) x(mol)
0.0013 0.00001 0.0000 164.55 1.3366 0.9300 0.9095
0 0 0 0 0 0 0
132.7899 0.99960 0.9980 12.38 0.1329 0.0700 0.0905
0 0 0 0 0 0 0
0 0 0 0 0 0 0
0.2661 0.00039 0.0020 0 0 0 0
133.05736132 1 1 176.93 1.4695 1 1
yi
0.0185 0.6439179132
-
0.9813 1.2083056981
-
-
0.0002 12.984599542
1.0000
Tbubble
T,K 456.9773 K 183.8273 C
Pt,mmHg 760 mmHg 1 atm
xi Komponen Fi,kmol/ja xi log P

0.000005 Nitrobenzen 0.0013 0.00001 2.5944
- Hidrogen - -
0.9786 Anilin 132.79 0.9980 2.8723
- Benzen - -
- Nitrogen - -
0.0215 Air 0.2661 0.00200 3.9133
1.00 Total 133.0574 1.00000
T,K 503.00 K 230

yi Komponen Bi, kmol/j xi log P

0.9480 Nitrobenzen 1.3366 0.9095 3.0664
- Hidrogen - -
0.0519 Anilin 0.1329 0.0000 3.3232
- Benzen - -
- Nitrogen - -
0.0000 Air 0.0000 0.0000 4.3200
1.00 Total 1.4695 0.00
Tavg 476.8801
Heavy Key
Distilat 0.0013
Bottom 1.3366
d/b 0.0010
log(di/bi) -2.9995673779
α 1.0000
log α 0
xb di xd
0 0.2637 0.0020
0.0905 132.7903 0.9980
0.9095 0.0013 0.00001
1.0000 133.0554 1.0000
A/B=0
0.0020669363
2.1546775016
-2.156468627
0.0002758109
1.0046121875
A/B=0
0.0021083954
2.1762585659
-0.0021802013
2.17618676
2.17618676
1.17618676
0.5404806157
Tavg 476.88006308
μ xf μ*xf
0.1335415843 0.0020 0.0002617944
0.3167499948 0.9881 0.312978632
0.363808626 0.0099 0.0036184543
Jumlah 1.0000 0.3168588807
Komponen A
Nitrobenzen 0.3614
456.97732549 K Hidrogen 0.03125
1 atm Anilin 0.3119
Benzen 0.3009
Nitrogen 0.31205
BM vap mix xi ρi xi*ρi Air 0.3471
0.0070 0.0215 0.8644 0.0186
93.0917 0.9786 0.6844 0.6697
0.0016 0.0000 1.0298 0.0000
93.1003 1.0001 0.6884 gr/cm3
ρi xi*ρi
0.8147 0.0000
0.6174 0.0558
0.9813 0.8926
0.9484 gr/cm3
Pi, mmHg Ki, Pt/Po yi
393.0343 1.9337 0.0000
745.2113 1.0198 1.0178
8189.6179 0.0928 0.0002

1.0180
Pi, mmHg Ki, Pt/Po xi

1165.2571 0.9131 0.9961
- -
2104.5268 0.5056 0.0000
- -
- -
20890.7101 0.0509 0.0000
1.00
Air 100
Anilin 184
Nitrobenen 210
B n Tc Tmin Tmax
0.24731 0.2857 719 278.91 719
0.3473 0.2756 33.18 13.95 33.18
0.25 0.28571 699 267.13 699
0.2677 0.2818 562.16 278.68 562.16
0.28479 0.2925 126.1 63.15 126.1
0.274 0.28571 647.13 273.16 647.13
CONDENSER CD-301
Tugas : Mengkondensasi hasil atas MD-01
Neraca Massa Hot Fluid

Komponen Mr kg/jam kmol/jam xi (massfrac)
Nitrobenzen 123.11 0.164716 0.001337958 1.33141E-05
Anilin 93.129 12366.5949 132.7899 0.9996
Air 18 4.7894 0.2661 0.0004
Total 12371.5490 133.0574 1.0000
Qc = 11102773.5799679 kJ/jam
Kondisi Hot Fluid

456.8273 K
T in 183.8273 °C
362.8892 °F
456.8273 K
T out 183.8273 °C
362.8892 °F
456.8273 K
T average 183.8273 °C
362.8892 °F
Viskositas
Viskositas fungsi Suhu
Hot Fluid
Tin = 183.8273 C Tout =
456.8273 K
Komponen A B C D
Nitrobenzen -7.771 1.40E+03 0.0147 -1.15E-05
Anilin -13.863 2.51E+03 0.0257 -1.83E-05
Air -10.2158 1.79E+03 1.77E-02 -1.26E-05
Cold Fluid
Tin = 100.0000 C Tout =
373.0000 K
Komponen A B C D
Dowtherm A
Perhitungan Densitas Cairan
Sumber = Yaws
Kondisi Operasi
Tin = 183.8273 C Tout = 183.8273
456.827325488177 K 456.827325
P= 1 atm
Komponen A B n Tc
Nitrobenzen 0.3614 2.47E-01 2.86E-01 7.19E+02
Anilin 0.3119 2.50E-01 2.86E-01 6.99E+02
Air 0.3471 0.274 2.86E-01 6.47E+02

Tavg = 456.8273 K Tavg =
Formula Rho T, kg/m3 xi*densitas Formula
Nitrobenzen 1029.92898495299 0.013712574124 Dowtherm A

Anilin 868.484204895803 868.1364260679
Air 864.546117472459 0.334691195869
Rho campuran 868.4848298379 kg/m3

54.217224511335 lb/ft3
Heat Capacity for Liquid

Cp dalam
T dalam
Tin = 183.8273 C Tout = 183.8273
456.827325488177 K 456.827325
Komponen A B C D
Nitrobenzen 51.773 0.91277 -2.1098E-03 2.009E-06
Anilin 63.288 0.98960 -2.3583E-03 2.330E-06
Air 92.053 -3.9953E-02 -2.1103E-04 5.3469E-07
T= 183.8273 C 142.5000
456.827325244089 K 415.5
Komponen cp, J/mol K cp, J/g K xi * cp cp, J/mol K
Nitrobenzen 220.012886569737 1.787124413693 2.379395E-05 2.11E+02
Anilin 245.30223666435 2.634004839141 2.632950069 234.4362212
Air 80.7363958398402 4.485355324436 0.001736413 77.37465239
2.634710276
Thermal Conductivity for Liquid
Komponen A B C
Nitrobenzen 1.6330E-01 8.5964E-06 -1.9810E-07
Anilin 1.9620E-01 -5.2139E-07 -2.4460E-07
Air -0.2758 4.61E-03 -5.54E-06
T Hot Avg = 183.8273 C T Cold Avg=

456.977325244089 K
Komponen k Xi*k Komponen
Nitrobenzen 0.675058721612627 8.987797113E-06 Dowtherm A
Anilin 1.57024582994858 1.569617035261
Air 3.68992744861494 0.001428479297
Total 1.571054502356
Mencari Massa Pendingin

Fluida pemanas yang digunakan adalah air
Q= 11102773.5800 kJ/jam CP
10523552.9851 BTU/jam
massa air = 140804.7782 lb/jam

63868.6284 kg/jam
LMTD
362.8892 High 365.0000 2.1108
362.8892 Low 212.0000 150.8892
0.0000 Diff 153.0000 153.0000
LMTD = 34.8470189175164 F
Koreksi Nilai LMTD
R= 5.74326064701845E-09
S= 1.01398916767288
FT = 1
FT x LMTD = 34.8470189175164 F
Menentukan Nilai Rd dan Ud

Menentukan nilai A hasil trial Ud
Viskoditas= 0.3620 Vis Dowther

Ud = 55 BTU/ft .F.hr
2
A= 5490.7804 ft2 karena A >200ft2, maka digunakan HE shell and tube
Trial Layout HE
Tube Pitch Triangular (Pressure Drop yang dihasilkan lebih kecil)
OD 0.75 in 1 in triangular pitch

L 16 ft
BWG 16
a'' 0.2618 ft2/lin ft
1310.8242 tubes
Nt =
728 tubes sesuai standar
Tube Passes 2 Passes
Ukuran Standar
Shell Side
ID 31 in
Passes 1
Tube Side
Nt 728 tubes
L 16 ft
OD 3/4 in
ID 0.62 in
BWG 16
Pitch 1 in triangular pitch
Passes 2
Koreksi Ud 0.401618056
A 3049.4464 ft2
Ud 99.0320471548042 BTU/ft2.F.hr
Perhitungan hi dan ho
Tube (Cold Fluid)
1. Flow Area (a) 1. Flow Area (a)
Baffle Cut 25%
B = 0,25 ID
IDs =
at' 0.302 in2 B=
n= 2 passes
Nt = 728 tubes
at = 0.763388888888889 ft2 PT
ODT
C
2. Mass velocity (Ga)
63868.6284 kg/jam
W=
140806.055523321 lb/hr as =
G= 184448.657260737 lb/hr.ft2
3. Viskositas saat T rata-rata (μ) 2. Mass velocity (Ga)

0.4987 cP G_s=m_c/a_s
μ=
1.20640296700286 lb/ft.hr
W=
4. Reynold Number (Re)
D G t G=
Re 

0.62 in 3. Viskositas saat T rata-rata (μ)
D=
0.0516666666666667 ft
μ=
Ret= 7899.38979964572
5. Menentukan nilai jh
4. Reynold Number (Re)
L/D = 309.677419354839
De =
jh = 54 fig 24
Re =
6. Menghitung nilai hi (fig.24) 5. Menghitung loading G"
𝐺"=𝑊/𝐿 〖𝑁𝑡 " " 〗 ^(2/3)
k 0.1247 W/mK W=
0.0721 BTU/jam.F.ft L=
Cp 2.0452 J/g K Nt =
0.4885 BTU/lb.F G" =
μ 1.2064 lb/ft.jam sg =
μ/μw 2.08000511552218
hi 168.1076 BTU/jam.ft2.F Menghitung Tw
7. Menghitung hio ho =
ta =
Tv =
hio =
tw =
hio = 138.97 BTU/jam.ft2.F
tf =
Mencari V ρ
V= Gt/3600/rho g
V= 0.81977181004772 k
Cp
μ
μ/μw
ho
7. Menghitung nilai Uc A
B
Uc 133.622999563079 BTU/ft2.F.hr 6. Menghitung nilai ho

91.7468555120942
8. Menghitung nilai Rd
Rd 0.0026139997790328 ρ
-0.000801814739746115 min 0,003 g
k
Cp
μ
μ/μw
ho
A
B
PRESSURE DROP
Tube (Cold Fluid)
1. Menghitung Pressure Drop di Tube 1. Menghitung Pressure Drop di Shell
vg = 0.016 ft3/lb Res =
s= 0.879732802071587 f=
Ret = 7899.38979964572
f= 0.00032 dari fig 26 Number of Crosses (N+1)
(N+1) =
f= 0.00032
Gt = 184448.657260737 lb/hr.ft2 2. Menghitung Δ Pp
L= 16 ft
n= 2 passes
D= 0.0516666666666667 ft
s= 0.879732802071587
Δ Pt = 0.073415747498446 psi
Ds =
rho s =
v2/2g' = 0.006 dari fig 27
n= 2 s=
s= 0.879732802071587 De =
Δ Pr = 0.0545620214307913 psi Gs =
Δ Ptotal = 0.127977768929237 psi f=
batas 10 psi (N+1) =
Δ Ps =
CONDENSER CD-301
xi (molefrac) Mr camp
1.00554972E-05 1.34538322E-08
0.9980 132.5231
0.0020 0.0005
1.0000 132.5236
Kondisi Cold Fluid (dowterm A)

373.0000 K
T in 100.0000 °C
212.0000 °F
458.0000 K
T out 185.0000 °C
365.0000 °F
415.5000 K
T average 142.5000 °C
288.5000 °F
183.8273 C
456.8273 K
Viskositas, cp Xi.Vis
0.4080 0.0000
0.3620 0.3619
0.1484 0.0001
Vis camp 0.3620 cP
185.0000 C
458.0000 K
Viskositas, cp Xi.Vis
0.4987
C
K
415.5000 K Tavg = 449.8057 K

Rho T,
Rho T, kg/m3 xi*densitas Formula xi*densitas
kg/m3
Nitrobenze 1038.136902 0.01382186
Anilin 875.8074418 875.45673
Air 872.7951302 0.33788463
880.7563 Rho campuran 875.808437 kg/m3

54.9833001295 54.674418 lb/ft3
J/(mol.K)
K
C
K
C C
K 449.8057 K
cp, J/g K xi * cp cp, J/mol Kcp, J/g K xi * cp
1.71329454246 2.28109693E-05 2.18E+02 1.77E+00 2.36E-05
2.51732780599 2.51631975851 2.43E+02 2.61E+00 2.61E+00
4.29859179935 0.00166411115 8.00E+01 4.45E+00 1.72E-03
Dowtherm A 2.0452 2.61E+00
untuk organik
untuk anorganik
142.5000 C T Hot Avg = C

415.65 K 449.8057472 K
k Xi*k Komponenk Xi*k
Nitrobenze 6.78E-01 9.03E-06
Anilin 1.570249618 1.57E+00
Air 3.657778283 1.42E-03
Total 0.1247 Total 1.57104588
2.0452 Kj/Kg K
0.48848762778 Btu/lb.R
0.81
2, maka digunakan HE shell and tube
triangular pitch
ho 200 an
Shell (Hot Fluid)

Flow Area (a)
affle Cut 25%
31 in
7.75 in
1 in
3/4 in
1/4 in
0.41710069444 ft2
Mass velocity (Ga)

G_s=m_c/a_s
12371.5490 kg/jam
27274.5643564 lb/hr
65390.838998 lb/hr.ft2
Viskositas saat T rata-rata (μ)

0.3620 cP
0.87562952642 lb/ft.hr
Reynold Number (Re)

0.73 in
0.06083333333 ft
4542.95176864
Menghitung loading G"
=𝑊/𝐿 〖𝑁𝑡 " " 〗 ^(2/3)
27274.5643564 lb/jam
16 ft
728 tubes
21.0644562878 lb/jam/lin.ft
0.86747559218
Menghitung Tw
270 fig 12.9

288.50
362.8892
138.968942508
337.61150452 F
350.25034498 F
449.805747211 K
54.6744180465 lb/ft3 0.874791
416692887.137 ft/jam2
1.5710 W/mK
0.9077 BTU/jam.F.ft
2.6130 J/g K
0.6241 BTU/lb.F
lb/ft.jam
1
#DIV/0! BTU/jam.ft2.F
#DIV/0!
0
Menghitung nilai ho
Eq 12.42
54.2172245113 lb/ft3
416692887.137 ft/jam2
1.5711 W/mK
0.9077 BTU/jam.F.ft
2.6347 J/g K
0.6293 BTU/lb.F
0.8756 lb/ft.jam
1.50970608
3473.55875929 BTU/jam.ft2.F
0.21822443825
9.4236683E-05
Shell (Hot Fluid)

Menghitung Pressure Drop di Shell
4542.95176864
0.002 dari fig. 29
umber of Crosses (N+1)
24.7741935484
Menghitung Δ Pp
2.58333333333 ft
868.484829838 kg/m3
54.1456269237 lb/ft3
0.86633003078
0.06083333333 ft
65390.838998 lb/ft2 jam
0.002
24.7741935484
0.19895199692 psi
batas 10 psi
Umpan Masuk / Cold Fluid (L dari Qc dan Qh Bottom)
Komponen BM, kg/kmol Massa, kg/jam Mol, kmol/jam Fraksi Massa
Nitrobenzen 123.11 164.55 1.3366257818 0.9300
Anilin 93.129 12.38 0 0.0700
Air 18 0 0.1329231496 0
Total 176.931 1.4695489314 1
Sifat-Sifat Fisis Komponen dan Pemanas

1. Viskositas Komponen
Suhu Cold Average = 226.89140033388 C

500.04140033388 K
Komponen A B C D Viskositas, cp
Nitrobenzen -7.771 1.40E+03 0.0147 -1.15E-05 0.3197
Anilin -13.863 2.51E+03 0.0257 -1.83E-05 0.2744
Air -10.2158 1.7925E+03 1.7730E-02 -1.2631E-05 0.1192
Total Vis =
Suhu Hot Average = 237.77777777778 C

510.92777777778 K
Komponen A B C D Viskositas, cp
Nitrobenzen -7.7710 1.4019E+03 1.4700E-02 -1.1512E-05 0.3008
Anilin -13.8630 2.5109E+03 2.5700E-02 -1.8281E-05 0.2571
Air -10.2158 1.7925E+03 1.7730E-02 -1.2631E-05 0.1132
Total Vis = 0.1132

0.2740
2. Densitas Komponen
Suhu Cold Average = 226.89140033388 C

500.04140033388 K
Komponen A B n Tc Densitas, g/mL

Nitrobenzen 0.3614 0.24731 0.2857 719 0.9772
Anilin 0.3119 0.25 0.28571 699 0.8212
Air 0.3471 0.274 0.28571 647.13 0.8103
Suhu Hot Average = 237.77777777778 C

510.92777777778 K
Komponen A B n Tc Densitas, g/mL

C5H11Cl 0.3028 0.2695 0.2804 568 0.6027
C17H33COONa 0.3471 0.274 0.2857 647.13 0.7956
H2O 0.3471 0.274 0.2857 647.13 0.7956
NaOH 0.1998 0.0979 0.2538 2820 1.8182
C5H11OH 0.2692 0.2673 0.2506 586.15 0.5925
C5H10 0.23767 0.26648 0.2905 464.78 #NUM!
NaCl 0.22127 0.10591 0.37527 3400 1.8289
Total Rho =
3. Thermal Conductivity
Formula A B C
Nitrobenzen 0.1633 8.60E-06 -1.98E-07
Anilin 0.1962 -5.21E-07 -2.45E-07
Air -0.2758 4.61E-03 -5.54E-06
Suhu Cold Average = 226.89140033388 C Suhu Hot Average = 237.777777778
500.04140033388 K 510.927777778
Formula k, W/m K xi*k Formula k, W/m K

C5H11Cl 1.4705331294856 1.3676470914 C5H11Cl 1.47062038674
C17H33NaO2 1.3478.E-01 0.0094298409 C17H33NaO2 1.3208.E-01
H2O 6.4539.E-01 0.0000.E+00 H2O 6.3463.E-01
Total 1.3771 Total
Menentukan Kebutuhan Reboiler

8.55E+06 kJ/jam
Beban Reboiler =
8103147.2307 BTU/jam
Menghitung LMTD

460.0000 High 446.0000 14.0000
460.0000 Low 434.8090 25.1910
0.0000 Diff 11.1910
D.LMTD 19.050780991559 F
Menentukan Trial UD
Koefisien (transfer panas overall dengan dirt factor) ditentukan dengan menggunakan trial Ud sesuai range sehingga didapatk
nilai yang sesuai dengan Ud hasil perhitungan. Nilai Ud ditentukan dengan melihat range pada tabel 8 Kern.
Untuk Steam sebagai Hot Fluid : Cek Viskositas :

Viskositas = 0.3165 cp
Steam-Light Organics = 100-200 BTU/(ft2.F.jam)
120 BTU/ft .F.hr
2
Ud =
A= Q/(Ud*LMTD)
A= 3544.5385127579 ft2
Menentukan Layout
Trial Layout HE
Tube Pitch Square Pitch (Biasanya pressure drop Square Pitch yang dihasilkan lebih kecil)
Table 9. Kern
OD 3/4 in Tabel 9
L 16 ft Trial (8,12,16)
BWG 16 Pilih dari Tabel 10
a'' 0.1963 ft2/lin ft Tabel 10
at 0.302 in2 Tabel 10
1128.5463935169 Tubes
Nt =
526 Tubes standar Tabel 9
Tube Passes 2 Passes Dari Table 9 setelah tube standar. Pasti Ganti kalau Tube Standar
Ukuran Standar
Shell Side
ID 29 in Dari Table 9 setelah tube standar. Pasti Ganti kalau Tube Standar
Passes 1
Tube Side
Nt 526 tubes Tabel 9
L 16 ft
OD 3/4 in Tabel 10
ID 0.620 in Tabel 10
BWG 16 Tabel 10
Pitch 1 Square Dari Table 9 setelah tube standar. Pasti Ganti kalau Tube Standar
Passes 2 Dari Table 9 setelah tube standar. Pasti Ganti kalau Tube Standar
Koreksi Ud
Flux
A 1652.0608 ft2 4904.87228479954
Ud 257.46305555519 BTU/ft2.F.hr
Perhitungan berikutnya, sebagai berikut :
Perhitungan hi dan ho
Tube (Hot Fluid) Shell (Cold Fluid)
1. Flow Area (a) 1. Flow Area (a)

B = 0,25 ID (25% cut)
N a '
at  t t
144  n IDs = 29
at' 0.302 in2 B= 7 1/4
n= 2 passes
Nt = 526 tubes
a= 0.5515694444444 ft2 PT 1
ODT 3/4
C 1/4
2. Mass velocity (Ga)
W= 10617.331277154 lb/hr
G= 19249.310098836 lb/hr.ft2 as = 0.3650
3. Viskositas saat T rata-rata (μ) dari fig. 15 2. Mass velocity (Ga)

μ= 0.0170 cP G_s=m_c/a_s
0.0411246249028 lb/ft.hr
W= 176.931
4. Reynold Number (Re) 390.06562122
D G t
G= 1068.6221
Re 

D= 5/8 in 3. Viskositas saat T rata-rata (μ)
0.0516666666667 ft μ= 0.3165
Ret= 24183.750995649
(untuk pressure drop) 0.76565295188
Mencari nilai v 4. Reynold Number (Re)
v= Gt/3600/rho De = 0.95
Rho = 1.0259 lb/ft3 0.07916666667
1.0259 lb/ft3 Re = 110.4929
v= 5.2122854123181 fps
5. Memilih nilai hio

1500 BTU/ft .F.hr
2
hio = 5. Mencari Nilai jh dari grafik figure 28
jh = 60
6. Menghitung nilai hi dan hio
1.3771
k
0.7957
1.9469
Cp
0.4650
μ 0.7657
μ/μw 1
ho 461.2398
Trial 300 (Maximum) karena o
461.2398
7. Menghitung nilai Uc
352.76650514746 BTU/ft .F.hr

2
Uc =
8. Menghitung nilai Rd
Rd = 0.0010493161543 tidak jauh lebih besar dari 0,003
PRESSURE DROP
Tube (Hot Fluid) Shell (Cold Fluid) DAPAT DIABAIKAN
1. Menghitung Pressure Drop di Tube 1. Menghitung Pressure Drop di Shell
vg = 0.9748 ft3/lb Res = 110.492945745
s= 0.0164136233073 sg f= 0.0034
Ret = 24183.750995649
f= 0.00022 dari fig 26 Number of Crosses (N+1)
(N+1) = 1.24137931034
f= 0.00022
Gt = 19249.310098836 lb/hr.ft2 2. Menghitung Δ Pp
L= 16 ft
n= 2 passes
D= 0.0516666666667 ft
s= 0.0164136233073
Δ Pt = 0.0589274418943 psi
Ds = 0.08333333333
966.31106533
rho s =
dari fig 27 tetapi v2/2g'
karena =Gt kecil dan tidk dapat
0 dicapai dari figure 27 dianggap bernili paling kecil atau Or60.2445968405
dapat diabaikan
n= 2 s= 0.96391354945
s= 0.0164136233073 De = 0.07916666667
Δ Pr = 0 psi Gs = 1068.62210617
f= 0.0034
Δ Ptotal = 0.0589274418943 psi (N+1) = 1.24137931034
Δ Ps = 1.0083227E-07
Diabaikan
Kondisi Operasi Umpan / Cold Fluid Pemanas / Hot Fluid
Tekanan = 1.2000 atm 237.777777778 C
223.78280067 C Suhu Masuk = 510.927777778 K
Suhu Masuk = 496.93280067 K 460 F
434.8090412 F 237.777777778 C
230 C Suhu Keluar = 510.927777778 K
Suhu Keluar = 503.15 K 13.99498 460 F
446 F 237.777777778 C
226.89140033 C T Avg = 510.927777778 K
T Avg = 500.04140033 K 460 F
440.4045206 F
Suhu Steam 460 F

237.777777778 C
Xi.Vis
0.2973
0.019200961402
0.0000.E+00
0.3165 cP
cP
lb/fth
Formula A B
Anilin 63.288 0.98960
Air 92.0530 -0.0400
Densitas, kg/m3 Xi. Rho
977.2239 908.8523
821.2482 57.458732423
810.3415 0.0000
Tavg Cold Fluid

Untuk T = 226.8914 C
500.0414 K
Total Rho = 966.31106533 Komponen cp1, J/mol K cp, J/g K
C5H11Cl 2.3188.E+02 1.8835.E+00
C17H33NaO2 2.5973.E+02 2.7889.E+00
H2O 8.6161.E+01 4.7867.E+00
Densitas, kg/m3
602.7376
795.5590
795.5590
1818.2386 cp, J/mol K
592.4590 cp, J/g K
#NUM!
1828.8772
795.5590
For organic compounds
For anorganic compounds

C
K
xi*k
Menghitung Caoric Temperature

tc = 440.4045 F Avg Cold
Tc = 460 F Avg Hot
hio = 1500 BTU/ft2.F.hr Tube

ho = 461 BTU/ft2.F.hr Shell
Tw = 455.3916
dTw = 14.9871
Pada grafik fig 15.11, pada dtw di atas, tidak bertemu dengan
latent heat transfer sehingga ho= 300
range sehingga didapatkan

8 Kern.
s:
Ganti kalau Tube Standar ganti

(Cold Fluid)
0,25 ID (25% cut)
in
in 5.8
in
in
in
ft2
kg/jam
lb/hr
lb/hr.ft2
cP
lb/ft.hr
in
ft
grafik figure 28
W/mK
BTU/jam.F.ft
J/g K
BTU/lb.F
lb/ft.jam
BTU/jam.ft2.F
300 (Maximum) karena organic compound dan dTw > dari 25
DAPAT DIABAIKAN
Drop di Shell
dari fig. 29
ft
kg/m3
lb/ft3
ft
lb/ft2 jam
psi
abaikan
Revisi : Cek Word, Q maksimum penguapan, TLMTD
Lamda / hfg = 763.2 BTU/lbF Ganti bila Suhu Steam Ganti

vg = 0.9748
C D
-2.1098E-03 2.009E-06
-2.3583E-03 2.330E-06
-0.0002 5.3469.E-07
xi * cp1 xi.cp2
2.1566.E+02 1.7518.E+00
1.8172.E+01 1.9513.E-01
0.0000.E+00 0.0000.E+00
2.3383.E+02
1.9468900017
v= 5.21228541232
g= 32.144
0.42259705107
Kondisi Operasi Atas
Pada kondisi atas, suhu yang digunakan adalah suhu pada kondisi Dew Point
Kondenser yang digunakan adalah kondenser total sehingga Xd = Yi
Pada keadaan Dew Point diinginkan Sxi=Syi/Ki=1
Kondisi Operasi Distilat :

Menggunakan Suhu Dew Point (Td)
T= 183.8273 C
T= 456.8273 K P= 1.0000
Komponen Top, kmol/jam Yi Pi Ki

Nitrobenzen 0.0013 0.0000 393.0343 1.9337
Anilin 132.7899 0.9980 745.2113 1.0198
Air 0.2661 0.0020 8189.6180 0.0928
Total 133.0574 1.0000
Data-Data Fisis Komponen Distilat

1. H Vapor
T= 273 K
T= C
Komponen A Tc n T Boiling 1 atm (K)
Nitrobenzen 67.414 719 3.80E-01 483.95
Anilin 72.038 699 0.459 457.6
Air 52.053 647.13 0.321 373.15
2. Heat Capacity Vapor

C dalam J/(mol.K)
T dalam K
T= 273 K
T= C
Komponen A B C D
Nitrobenzen -16.202 0.56182 -3.9302E-04 1.004E-07
Anilin -22.062 0.57313 -4.5651E-04 1.841E-07
Air 33.933 -8.4186E-03 2.9906E-05 -1.7825E-08
3. Heat Capacity Liquid

C dalam J/(mol.K)
T dalam K
T= 273.15 K
T= C
Komponen A B C D
Nitrobenzen 51.773 0.91277 -2.1098E-03 2.009E-06
Anilin 63.288 0.98960 -2.3583E-03 2.330E-06
Air 92.053 -3.9953E-02 -2.1103E-04 5.3469E-07
Mencari Beban Kondenser (Qc)
Nilai R (Rule of Thumb R = Hasil Optimas

R=
1. Mencari Nilai V1.H1 dengan V = (R+1)*D

T= 456.8273 K
Komponen V1, kmol/jam H1, J/(mol.K) V1.H1, kJ/jam
Nitrobenzen 0.0037 68919.2973 254.89737
Anilin 367.0686 66193.2000 24297445.9772
Air 0.7355 40566.8544 29837.4075
Total 24327538.2820
2. Mencari D.Hd dan L0.H0

T= 456.8273 K
Komponen D, kmol/jam Hd, J/(mol.K) D.Hd, kJ/jam
Nitrobenzen 0.0013 32417.9869 43.3739
Anilin 132.7899 36003.3767 4780886.4539
Air 0.2661 12148.4470 3232.4250
Total 4784162.2528
Komponen L0, kmol/jam H0, J/(mol.K) L0.H0, kJ/jam

Nitrobenzen 0.0024 32417.9869 76.5237
Anilin 234.2787 36003.3767 8434823.0222
Air 0.4694 12148.4470 5702.9033
Total 8440602.4492
Qc (Kondenser) = 11102773.5800 kJ/jam
Kondisi Operasi Bawah

Pada kondisi bawah, suhu yang digunakan adalah suhu pada kondisi Bubble Point
Kondenser yang digunakan adalah kondenser total sehingga Xd = Xi
Pada keadaan Bubble Point diinginkan Syi=Sxi*Ki=1
Kondisi Operasi Bottom

Menggunakan Suhu Bubble Point (Tb) Pake Excel MD Coba 1,5
T= 496.7828 K
T= 223.7828 C P= 1.4000
Komponen B, kmol/jam xi Pi Ki
Nitrobenzen 1.3366 0.9095 1020.7988 1.0423
Anilin 0.1329 0.0905 1853.6198 0.5740
Air 0.0000 0.0000 18609.3262 0.0572
Total 1.4695 1.0000
Data-Data Fisis Komponen Bottom

1. H Vapor
T= 273.15 K
T= C
Komponen A Tc n T Boiling 1 atm
Nitrobenzen 67.414 719 3.80E-01 483.95
Anilin 72.038 699 0.459 457.6
Air 52.053 647.13 0.321 373.15
2. Heat Capacity Vapor

C dalam J/(mol.K)
T dalam K
T= 273.15 K
T= C
Komponen A B C D
Nitrobenzen -16.202 0.56182 -3.9302.E-04 1.0040.E-07
Anilin -22.062 0.57313 -4.5651.E-04 1.8410.E-07
Air 33.933 -0.0084186 2.9906.E-05 -1.7825.E-08
3. Heat Capacity Liquid

C dalam J/(mol.K)
T dalam K
T= 273.15 K
T= C
Komponen A B C D
Nitrobenzen 51.773 0.91277 -0.0021098 0.0000020093
Anilin 63.288 0.9896 -0.0023583 0.0000023296
Air 92.053 -0.039953 -0.00021103 0.00000053469
Mencari Beban Reboiler
Nilai R (Rule of Thumb R = 1,5 Rm)

R=
Mencari Nilai L1.H1 dengan L1 = (F*q)+(R*D)

T= 496.7828 K
Komponen L1, kmol/jam H1, J/(mol.K) L1.H1, kJ/jam
Nitrobenzen 1.3404 41417.7337 55514.2986
Anilin 367.2019 46057.9902 16912582.5278
Air 0.7332 15467.1558 11339.8533
Total = 16979436.6796
Mencari Nilai Vb.Hb dengan Vb = L-B dan B.hB

T= 496.7828 K
Komponen Vb, kmol/jam Hb, J/(mol.K) Vb.Hb, kJ/jam
Nitrobenzen 0.0037 73037.9759 272.0786
Anilin 367.0690 69300.5052 25438067.0640
Air 0.7332 39404.0426 28889.3489
Total = 25467228.4915
Komponen B, kmol/jam hb, J/(mol.K) B. hB, kJ/jam

Nitrobenzen 1.3366 41417.7337 55360.0107
Anilin 0.1329 46057.9902 6122.1731
Air 0.0000 15467.1558 0.0000
Total = 61482.1838
Total Reboiler = 8549273.9956 kJ/jam
R= 1.7643
Kondenser = 1.1103E+07 kJ/jam
Reboiler = 8.55E+06 kJ/jam
i Operasi Atas
atm
xi
0.0000
0.9786
0.0215
1.0001 Trial Solver
is Komponen Distilat
E
-1.2252E-12
-2.9867E-11
3.6934E-12
ban Kondenser (Qc)
Rule of Thumb R = Hasil Optimasi)

1.7643
Operasi Bawah
atm
yi
0.9480
0.0519
0.0000
1.0000
s Komponen Bottom
E
-1.2252.E-12
-2.9867.E-11
3.6934.E-12
Beban Reboiler
Komponen BM
Rule of Thumb R = 1,5 Rm) Nitrobenze 123.11
1.7643 Anilin 93.129
Air 18
Massa, kg/jam
165.01
34197.15
13.20
34375.355202
Massa, kg/jam
0.46
34184.77
13.20
0.00
34198.424202
Massa, kg/jam
164.55
12.38
0.00
176.931
PERHITUNGAN AKUMULATOR UNTUK MD
Tugas = Menampung cairan hasil atas dari Menara Distilasi

Alat = Silinder Horizontal
Densitas Campuran
T= 456.8273 K Yaws
T= 183.8273 C
Komponen A B n Tc
Nitrobenzen 0.3614 0.24731 0.2857 719
Anilin 0.3119 0.25 0.28571 699
Air 0.3471 2.74E-01 2.86E-01 6.47E+02
Komponen BM, kg/kmol Mol, kmol/jam Massa, kg/jam xi

Nitrobenzen 123.11 0.001337957924 0.1647 0.0000
Anilin 93.129 132.7899461392 12366.5949 0.9996
Air 18 0.266077222222 4.7894 0.0004
Total 12371.5490 1
Densitas Cairan = 868.4826 kg/m3
Perhitungan Volume Tangki
Kondisi Operasi = T= 456.8273 K 183.8273

P= 1.0000 atm
Rangkuman Penentuan Volume Tangki

Umpan Masuk = 12371.5490 kg/jam
Dari V Top MD
27250.1079 lb/jam
Lama Penyimpanan = 10 menit 0.1667 jam
Densitas Cairan = 868.4826 kg/m3 56.1757 lb/ft3
Flowrate = 14.2450160759814 m3/jam
Massa yang disimpan = 2061.9248 kg
Volume Cairan = 2.37416934599691 m3 80.75077960998 ft3
Dengan,
Volume Tangki = Volume Cairan + Volume Ruang Kosong
Volume Tangki = Volume Cairan + 20/80 Volume Cairan V cairan = 0,8 V tangki
Sehingga,
Volume Tangki = 2.9677 m3
Volume Over Design = 120% V Tangki (Over Design = 20%) Peter & Timmerhaus hal 37
3.5613 m3
Volume Over Design = 22.3996 bbl Kategori sedang
Volume Over Design =
121.1262 ft3
Perhitungan Dimensi Tangki

L/D ratio = 4
dengan L = H
Apabila ingin mencari nilai ,

D = (Vt/phi)^(1/3) Sudah sesuai dengan Grafik di Evans
D= 0.981365273654119 m 3.179623486639 ft
L= 3.92546109461647 m 12.71849394656 ft
Appendix E Brownell (Akan Ganti bila Flowrate Ganti)
Data tidak tersedia untuk D = 2,3113 ft dan L = 9,2450 ft

Sehingga menggunakan Grafik Evans, sebagai berikut :
D= 3.5 ft 1.08024691358 m
L= 14 ft 4.320987654321 m
3.9582 m3
V sebenarnya =
134.6275 ft
Overdesign Actual 33.3758 %
Perhitungan Tekanan Design Sudah dibenarkan

Tekanan Total = Tekanan Operasi + Tekanan Hidrostatis -Tekanan Lingkungan
Tekanan Operasi = 1.0000 atm 14.7 psi
Tekanan Lingkungan = 1 atm
Mencari Tekanan Hidrostatis

H Cairan = 0.8642 m 2.8000 ft
Gravitasi = 9.8 m/s2
Tekanan Hidrostatis = 7355.2973 Pa 0.0726 atm
Sehingga,
Tekanan Total = 1.0726 atm 15.76708976664
P Overdesign = 1.2 P Total (Oberdesign = 20%)
Tekanan Overdesign = 1.2871 atm 18.9205 psi
Perhitungan Tebal Tangki

Bahan Konstruksi = Carbon Steel SA 53-A
Grade = SA-53 A
Suhu = 20 to 650 F apendix D
Specified Min Tensile = 48000 psi
Stress Value (f) = 10200 psi
Weld = Double welded butt joint Tabel 13.2 Brownel
E= 0.8 Sumber C di Internet
C= 3.175 mm 0.1250 in
rho = 56.1757379339615 lb/ft3
Dengan P design,
P Design = 1.2871 atm
18.9205 psi
Tebal Tangki = 0.174306273894238 in 4.427379356914

Tebal Standar = 3/16 in
Perhitungan Tebal Head
ID = 42.52942901235
Tebal Standar = 3/16
OD = 42.9044
OD Standar = 48
Dari tabel 5.7 dan 5.4 Brownell & Young untuk t=3/16
r= 48
icr = 3
Dari tabel 5.8 Brownell and Young untuk t=3/16

sf 1,5-2
dipilih straight Flange
Tebal Head 0.1686

Tebal Standar Hea 3/16
Perhitungan Detail
ID = 42.52942901235
a = ID/2 21.26471450617
AB = a-icr 18.26471450617
BC = r-icr 45
AC = ((BC^2)-(AB^ 41.12663618639
b = r-AC 6.873363813606
8.81086
Tinggi Head = OA
= t + b + sf 0.223795940866
0.725098848405
187.7394436766
Panjang Total
4.768581869386
N AKUMULATOR UNTUK MD
ensitas Campuran
Rho, g/ml Rho, kg/m3 xi.Rho

0.864546117762 864.5461 0.0115
0.868484205152 868.4842 868.1364
0.864546117762 864.5461 0.3347
2.5976 2597.5764 868.4826 kg/m3
ungan Volume Tangki
485.086781798 ft3/ajm
Dari Fig 5-4 Evans
0.00395694891 m3/s 0.13458463268 cuft/s
0.666666666667
0.004946186137 m3/s 0.16823079085 cuft/s
0.005935423365 m3/s 0.20187694902 cuft/s

6804.35195
ungan Dimensi Tangki
38.63644896029 in
154.5457958412 in
42.52942901235 in
170.1177160494 in
Perhitungan Tebal Bottom
34.02354320988 Tebal Bottom = 0.1278 in

Asumsi H Cairan = 0,8 H Tangki
34.02354320988 in
tungan Tebal Tangki

itungan Tebal Head
in
in
in
in
Brownell & Young untuk t=3/16 inch, OD= 42 inch

inch
inch
l and Young untuk t=3/16

inch
1.75 in
Satuan r dalam inch
in
in
ungan Detail Amil Klorida

in D=
in a=
in icr =
in AB =
in BC =
in AC =
in b=
m Head = in
ft m
ft
in
m NaOH
D=
a=
icr =
AB =
BC =
AC =
b=
Head = in
m
ft
Amil Alkohol
D=
a=
icr =
AB =
BC =
AC =
b=
Head =
rhitungan Tebal Bottom
PERHITUNGAN AKUMULATOR UNTUK MD
Tugas = Menampung cairan hasil atas dari Menara Distilasi

Alat = Silinder Horizontal
Densitas Campuran
T= 456.8273 K Yaws
T= 183.8273 C
Komponen A B n Tc
Nitrobenzen 0.3614 0.24731 0.2857 719
Anilin 0.3119 0.25 0.28571 699
Benzena 0.3009 0.2677 0.2818 562.16
Air 0.3471 2.74E-01 2.86E-01 6.47E+02
Komponen BM, kg/kmol Mol, kmol/jam Massa, kg/jam xi

Nitrobenzen 123.11 0.0530278 6.5283 0.0013
Anilin 93.129 0.1329943 12.3856 0.0025
78 2.116455 165.0835 0.0333
Air 18 265.4599 4778.2782 0.9629
Total 4962.2756 1
Perhitungan Volume Tangki
Kondisi Operasi = T= 456.8273 K 183.8273

P= 1.0000 atm
Rangkuman Penentuan Volume Tangki

Umpan Masuk = 4962.2756 kg/jam
Dari V Top MD
10930.1224 lb/jam
Lama Penyimpanan = 10 menit 0.1667 jam
Densitas Cairan = 858.5706 kg/m3 55.5346 lb/ft3
Flowrate = 5.77969417215704 m3/jam
Massa yang disimpan = 827.0459 kg
Volume Cairan = 0.963282362026174 m3 32.76337547248 ft3
Dengan,
Volume Tangki = Volume Cairan + Volume Ruang Kosong
Volume Tangki = Volume Cairan + 20/80 Volume Cairan V cairan = 0,8 V tangki
Sehingga,
Volume Tangki = 1.2041 m3
Volume Over Design = 120% V Tangki (Over Design = 20%) Peter & Timmerhaus hal 37
1.4449 m3
Volume Over Design = 9.0883 bbl Kategori sedang
Volume Over Design =
49.1451 ft3
Perhitungan Dimensi Tangki

L/D ratio = 3
dengan L = H
Apabila ingin mencari nilai ,

D = (Vt/phi)^(1/3) Sudah sesuai dengan Grafik di Evans
D= 0.726515121037803 m 2.353908992162 ft
L= 2.17954536311341 m 7.061726976487 ft
Appendix E Brownell (Akan Ganti bila Flowrate Ganti)
Data tidak tersedia untuk D = 2,3113 ft dan L = 9,2450 ft

Sehingga menggunakan Grafik Evans, sebagai berikut :
D= 3 ft 0.925925925926 m
L= 8 ft 2.469135802469 m
1.6618 m3
V sebenarnya =
56.5200 ft
Overdesign Actual 38.0078 %
Perhitungan Tekanan Design Sudah dibenarkan

Tekanan Total = Tekanan Operasi + Tekanan Hidrostatis -Tekanan Lingkungan
Tekanan Operasi = 1.0000 atm 14.7 psi
Tekanan Lingkungan = 1 atm
Mencari Tekanan Hidrostatis

H Cairan = 0.7407 m 2.4000 ft
Gravitasi = 9.8 m/s2
Tekanan Hidrostatis = 6232.5867 Pa 0.0615 atm
Sehingga,
Tekanan Total = 1.0615 atm 15.60420946544
P Overdesign = 1.2 P Total (Oberdesign = 20%)
Tekanan Overdesign = 1.2738 atm 18.7251 psi
Perhitungan Tebal Tangki

Bahan Konstruksi = Carbon Steel SA 53-A
Grade = SA-53 A
Suhu = 20 to 650 F apendix D
Specified Min Tensile = 48000 psi
Stress Value (f) = 10200 psi
Weld = Double welded butt joint Tabel 13.2 Brownel
E= 0.8 Sumber C di Internet
C= 3.175 mm 0.1250 in
rho = 55.5346027565582 lb/ft3
Dengan P design,
P Design = 1.2738 atm
18.7251 psi
Tebal Tangki = 0.166825931854258 in 4.237378669098

Perhitungan Tebal Head
ID = 36.4537962963
Tebal Standar = 3/16
OD = 36.8288
OD Standar = 48
Dari tabel 5.7 dan 5.4 Brownell & Young untuk t=3/16
r= 48
icr = 3
Dari tabel 5.8 Brownell and Young untuk t=3/16

sf 1,5-2
dipilih straight Flange
Tebal Head 0.1620

Tebal Standar Hea 3/16
Perhitungan Detail
ID = 36.4537962963
a = ID/2 18.22689814815
AB = a-icr 15.22689814815
BC = r-icr 45
AC = ((BC^2)-(AB^ 42.34550239147
b = r-AC 5.654497608531
7.59200
Tinggi Head = OA
= t + b + sf 0.192836739257
0.624791035192
112.3941186739
Panjang Total
2.854810614316
N AKUMULATOR UNTUK MD
ensitas Campuran
Rho, g/ml Rho, kg/m3 xi.Rho

0.864546117762 864.5461 1.1374
0.868484205152 868.4842 2.1677
0.684631840899 684.6318 22.7761
0.864546117762 864.5461 832.4894
3.2822 3282.2083 858.5706 kg/m3
ungan Volume Tangki
196.816432554 ft3/ajm
Dari Fig 5-4 Evans
0.001605470603 m3/s 0.05460562579 cuft/s
0.666666666667
0.002006838254 m3/s 0.06825703223 cuft/s
0.002408205905 m3/s 0.08190843868 cuft/s

2729.251562742
ungan Dimensi Tangki
28.60297296677 in
85.80891890031 in
36.4537962963 in
97.21012345679 in
Perhitungan Tebal Bottom
29.16303703704 Tebal Bottom = 0.1270 in

Asumsi H Cairan = 0,8 H Tangki
29.16303703704 in
tungan Tebal Tangki

itungan Tebal Head
in
in
in
in
Brownell & Young untuk t=3/16 inch, OD= 42 inch

inch
inch
l and Young untuk t=3/16

inch
1.75 in
Satuan r dalam inch
in
in
ungan Detail Amil Klorida

in D=
in a=
in icr =
in AB =
in BC =
in AC =
in b=
m Head = in
ft m
ft
in
m NaOH
D=
a=
icr =
AB =
BC =
AC =
b=
Head = in
m
ft
Amil Alkohol
D=
a=
icr =
AB =
BC =
AC =
b=
Head =
rhitungan Tebal Bottom
Komponen Mr(kg/kmol) Feed(kg/jam
Hidrogen 2 802.00
Nitrogen 28 11.2
Data Sifat Gas

Fi 802.00 kg/h 802000 g/h 401000 mol/h
R 8.314 J/mol K
Tin 30 C 303 K
MW 2 g/mol
Pin 1 atm 101325 Pa
Fv 9969.66141 m3/h 5867.9266945 ft3/m 2.76935 m3/s
rho 0.0822 kg/m3
miu 8.898E-06 kg/m/s
Pipe characteristics
L 100 km 1.00E+05 m jarak dr suplier sampai titik terluar Cilegon (plant site)
D pipe 14 in 0.3556 m
As 0.09931467 m2
abslt rough 0.000015 m
reltve roug 4.2182E-05
Moody Diagram
v 27.8846066 m/s
Re 9.16E+04
f 0.02 baca grafik
dP 1.80E+05 Pa 1.7738728927 atm
Kompresi
P1 2.7738729 atm
P0 1 atm
n 1
r 2.77387289
Mencari Ep
Ep 0.7 v 2.76935
y 1.4
m 0.40816327
T2 459.509277
Tmean 762.509277
Tc 33.2 K
Tr 22.9671469
Pmean 1.88693645
Pc 12.8 atm
Pr 0.14741691
Perhitungan Daya Kompresor

cp 29.598183 J/mol K
X 0
Y 1
Z 1
m 0.40127945
n 1.6702283
gamma 2.49202891
Wn 36759.9497 kJ/kg
Wn 8189.29991 kW
Perhitungan Daya Motor

ef motor 0.94
P motor 8712.02118
uar Cilegon (plant site)
T,K 443.6923 K 170.5423 C
Komponen Fi, kmol/jamyi log P Pi, mmHg Ki, Pt/Po xi

Nitrobenzen 165.2990 0.01 2.43 272.14 7.54 0.001236
Hidrogen 212.63 0.01 34.94 ### 0.00 -
Anilin 12391.40 0.70 2.72 525.11 3.91 0.178795
Benzen 165.32 0.01 3.81 6485.00 0.32 0.029460
Nitrogen 11.20 0.00 8.77 ### 0.00 -
Air 4789.3450 0.27 3.78 6007.05 0.34 0.790540
Total 17735.20 1.00 1.00
Agar hasil keluar reaktor fase cair suhunya diturunkan sampai dibawah 170
Komponen A B C D E
Nitrobenzen -54.494 -2112.3 29.321 ### ###
Hidrogen 3.4132 ### ### ### ###
Anilin 124.38 -7167.6 -42.763 ### ###
Benzen 31.772 -2725.4 -8.4443 ### ###
Nitrogen 23.8572 ### ### ### ###
Air 29.8605 ### ### ### ###
HEAT EXCHANGER - 03 - Setelah R
HOT FLUID
Komponen kmol/jam kg/jam xi,kmol
Nitrobenzen 1.34269352611486 165.2990 0.0026
Hidrogen 106.316 212.6320 0.2087
Anilin 133.056298252961 12391.4000 0.2613
Benzen 2.11644519548352 165.3240 0.0042
Nitrogen 0.4 11.2000 0.0008
Air 266.074722222222 4789.3450 0.5224
Total 509.306159196781 17735.2000 1.0000
39099.3766 lb/jam
513.15 K
Tin 240 °C
464 °F
433.15 K
Tout 160 °C
320 °F
473.15 K
Taverage 200 °C
392 °F
Nilai Q
Nitrobenzen 1.3427 172.2108 231.2263
Hidrogen 106.3160 29.2541 3,110.1825
Anilin 133.0563 164.9190 21,943.5077
Benzen 2.1164 132.2581 279.9170
Nitrogen 0.4000 29.4793 11.7917
Air 266.0747 34.9418 9,297.1364
Total 34,873.7617
2789900.9323 kJ/jam
Q
2644354.5906 BTU/jam
COLD FLUID
29465.2530686409 lb/hr GoalSeek

water
water 13365203.069911 g/hr 13365.203069911
742511.28166172 mol/hr
25.0000 °C
Tin 298.1500 K
77.0000 °F
75.0000 °C
Tout 348.1500 K
167.0000 °F
323.1500 K
122.0000 °F
2789900.9323 kJ/jam
Q
2644354.5906 BTU/jam
acc 0.0000 GoalSeek
LMTD

464 High 167 297
320 Low 77 243
144 Diff 90 54
LMTD 269.0976 °F
Koreksi Nilai LMTD
R 1.6000 S 0.2326
FT 1 Fig.18
FT.LMTD 269.0976 °F
tc = ta = 392.0000 °F
Tc = Ta = 122.0000 °F
DARI SINI
Tinggal Trial Trial
Nilai A
UD =75-150 Table 8 (Hot = Light organic, cold=water
Ud 90 BTU/ft2.F.hr
A 109.186105914822 ft2 (Digunakan HE double pipe karen
Lay Out HE
Tube Side
Tube Pitch squarepitch
OD 1 inch on
L 6 ft
Passes 1
a" 0.2618 ft2 (Table 10)

BWG 10
a' 0.421 sqin
ID tube 0.732 in
69.5099 tubes
Nt
21 tubes table 9
Shell Side
ID 8 inch
Passes 1
Tube Side
Nt 21
L 6 ft
OD 1 inch
BWG 10
Pitch 1.25 in. triangular pitch
Passes 1
Koreksi UD
A 32.9868 ft2
UD 297.8994
Tube Side water

Flow Area tube
Nt  at '
at 
144  n
Nt 21
at' 0.421
n 1
at 0.0614 ft2
Mass Velocity
G_t=m_h/a_t
mc 39099.3766 lb/jam
at 0.0614 ft2
Gt 636840.881558195 lb/ft2.jam
Reynold

ID
0.061 ft
Gt 636840.881558195 lb/ft2.jam
μ 0.0335 lb/ft.jam
ReT 1160875.8307
jH
L x n /D 98.3607
jH 130 figure 24
v 2.83040391803642 fps cp
koreksi miu
Ta 122 F k
hi kern muw
hicor
UC

Rd
Pressure Drop
Tube Side
Re
Re 1160875.8307
f
f 0.0008 figure 26
∆Pt
f 0.0008
Gt 636840.882 lb/ft2.jam
L 6 ft
n 1
D 0.061 ft
s 5.6558952997E-05
∆Pt 5404.69775514948 psi
∆Pr
∆Ptotal
Summary
Tube Shell
Nt 21 ID, in 8
OD, in 1 Pass, n 1
Pitch, in 1.25 L, ft 10
BWG 10
Pass, n 1
a", ft2/ft 0.2618
Triangle Pitch
HE-05, Heater
Steam Isooktan
25 Tin, °C 240
75 Tout, °C 160
708 h, Btu/jam. ft2.F 204.83
UC = 158.8865 Btu/jam. ft2.F
UD = 297.8994 Btu/jam. ft2.F
Rd required = 0.003
- 03 - Setelah R-201
Mr xi, massa Data CP Gas

123.11 0.00932039108665 Data
2 0.01198926428797 Compound a
93.129 0.69868961161983 Nitrobenzen -16.202
78.114 0.00932180071271 Hidrogen 25.399
28 0.00063151247237 Anilin -22.062
18 0.27004741982047 Benzen -31.368
1 Nitrogen 29.342
Air 33.933

Thermal Conductivity of Gas
Compound A
Nitrobenzen -1.0283E-02
Hidrogen 0.040
Anilin -0.01796
mCpTin mCpTout Benzen -0.00565
107,289.0159 73,992.4247 Nitrogen 0.00309
1,443,124.6977 995,258.4122 Air 0.00053
10,181,787.5608 7,021,922.4558 k campuran
129,881.4880 89,573.4400
5,471.3586 3,773.3508 0.0565
k
4,313,871.2866 2,975,083.6459 0.0326
16,181,425.4076 11,159,603.7294

Rumus Nama A B C
H2O Water 92.053 -0.039953 -0.00021103

0.9972 BTU/lb.F
Mr 18 g/mol
Enthalpy of Evaporation 945.3 btu/lb (Table 7 Kern)

k 6.80E-01 W/m.K
0.3929 BTU/hr.ft.F

25 High 160
75 Low 240
-50 Diff -80
ght organic, cold=water)
an HE double pipe karena A < 200 ft2)
Shell Side
ID 8
Passes 1
1.25 in. square pitch Baffle 2.00
De 0.99
Shell Side
Jarak Baffle
IDs 8
B 2
Clearance
PT 1.25
ODT 1
C 0.25
Flow Area shell
IDs 8
C 0.25
B 2.0
PT 1.25
as 0.0222
Mass Velocity
G_s=m_c/a_s
mh 29465.2531
Gs 1325936.38809
Reynold
0.99
De
0.4697 0.0825
1.29141157837652 μ 1.2914
3.93E-01 Res 84705.5686
0.061
ho
jH 54
k 0.0326
De 0.0825
Cp 0.9972
μ 1.2914
μ/μw 0.10461287752
ho 205
Shell Side
Re
Re 84705.5686
f
f 0.0022 figure 29
Number of Crosses
L 6 ft
B 2 in
N+1 36
∆Ps
f 0.0022
Gs 1325936.38809 lb/ft2.jam
Ds 0.6667 ft
N+1 37
De 0.0825 ft
s 1
∆Ps 22.1540980143 psi
Data CP Gas
joule/mol.K
b c d e Cpi, J/mol.K Cpi, J/g.K
0.56182 -3.9302E-04 1.004E-07 -1.2252E-12 172.21080074 1.39883681863
2.0178E-02 -3.8549E-05 3.1880E-08 -8.7585E-12 29.254134262 14.627067131
0.57313 -4.5651E-04 1.841E-07 -2.9867E-11 164.91897011 1.77086589685
0.47460 -3.1137E-04 8.524E-08 -5.0524E-12 132.2580904 1.69314195148
-3.5395E-03 1.0076E-05 -4.3116E-09 2.5935E-13 29.479302952 1.05283224829
-8.4186E-03 2.9906E-05 -1.7825E-08 3.6934E-12 34.941825048 1.94121250264
total
J/mol.K
J/g.K
BTU/lb.F
al Conductivity of Gas

5.7531E-05 1.0851E-08 1.9367E-02 5.105763316E-05
4.5918E-04 -6.4933E-08 2.4223E-01 0.0505656424621
8.35E-05 1.5022E-09 2.1867E-02 0.0057128323979
3.45E-05 6.9298E-08 2.6184E-02 0.0001088095247
7.5930E-05 -1.1014E-08 3.6551E-02 2.870616387E-05
4.7093E-05 4.9551E-08 3.3905E-02 0.0177128920479
k campuran 0.0564670481817
W/m.K
BTU/hr.ft.F
miuwater a b c
-10.2158 1.79E+03 0.0177
B*T + C*T^2 + D*T^3 + E*T^4 T (K)

D E
0.00000053469 0
a b c d Cpi, J/mol.K
cp 92.053 -0.039953 -0.00021103 5.3469E-07 75.1484263193
rho 0.34710 0.27400 0.2857 647.13 1.00428740695
A B C k, W/m.K
k -0.2758 4.61E-03 -5.54E-06 6.80E-01
a b c d μ, cp
miu -10.2158 1.79E+03 0.0177 -1.26E-05 0.53384065835
Diff.
-135
-165
30
hell Side
inch

inch figure 28
campuran
inch
inch
inch
inch
inch
ID s kecilin
in
in
in as kecilin
in
ft2
de besarin
gs besarin
lb/jam
lb/ft2.jam
inch (Fig. 28)
ft
lb/ft.hr
BTU/jam.F.ft
ft
BTU/lb.F
lb/ft.jam
(asumsi)
BTU/jam.ft2.F
∆Ps
f 0.0022
Gs 1325936.388 lb/ft2.jam
L 6 ft
n 1
D 0.0825 ft
s 1.00000
∆Ps 2.6944173261 psi
Data rho Gas
gr/ml
Compound A B n
x.Cp, J/g.K x.Cp, J/mol.K
0.01303770622 0.4540
0.17536777359 6.1067
1.2372856057 43.0851
0.01578313185 0.5496
0.0006648767 0.0232
0.52421942766 18.2545 rho campuran
1.9664 68.4731
0.0566 kg/m3 1000
rho campuran
0.0035 lb/ft3 62.4273708
Viscosity of Gas
Nitrobenzen 27.758 2.12E-01 -3.28E-05 0.012072283
Hidrogen -16.569 2.92E-01 -2.55E-05 0.011580124
Anilin -6.918 2.59E-01 -3.43E-05 0.010810393
Benzen -0.151 2.57E-01 -8.98E-06 0.011946665
Nitrogen 42.606 4.75E-01 -9.88E-05 0.02452338
Air -36.826 4.29E-01 -1.62E-05 0.016252864
total
0.0138 cP
μ
0.0335 lb/ft.hr
-10.2158 1.79E+03 0.0177 -1.26E-05 0.132232078
d μ, cp
-1.26E-05 0.132232078364
0.3199 Komponen
Nitrobenzen
Hidrogen
Anilin
Benzen
Nitrogen
Air
Cpi, J/g.K
4.17491257329 Kebutuhan panas pengembunan
rho, kg/m3 Komponen
1004.28740695 Nitrobenzen
Hidrogen
Anilin
Benzen
Nitrogen
Air
gr/V=P/RT*Mr
Tc rho, gr/cm3 rho, kg/m3 x/rho, kg/m3
0.03286046962 32.86046961933 0.30627242814
0.00053383916 0.533839162039 0.0064003388
0.02485795366 24.85795366078 17.3679939889
xi.μ, cp
3.18263905E-05
0.00241731309
0.00282421664
4.96449145E-05
1.92602268E-05
0.00849091695
0.0138331782
A Tc n Hcond(Kj/mol)
67.414 719 3.80E-01 61.2646004276
0.659 33.18 3.80E-01
72.038 699 0.459 63.9360595183
49.888 562.16 0.489 42.3511912964
9.43 126.1 0.533
52.053 647.13 0.321 47.5172706938
215.0691219361
s pengembunan
Hcond(KJ/mol) kmol/jam mol/jam deltaH(Kj/mol)
61.2646004276 1.3427 1342.693526115 82259.5823742
0 106.3160 106316
63.9360595183 133.0563 133056.298253 8507095.404386
42.3511912964 2.1164 2116.445195484 89633.97534231
0 0.4000 400
47.5172706938 266.0747 266074.7222222 12643144.60061
215.069121936 21322133.56271
Mr
Komponen
kg/kmol
Nitrobenzen 123.11
Hidrogen 2
Anilin 93.129
Benzen 78.114
Nitrogen 28
Air 18
Data Sifat-sifat gas
1. Data kapasitas panas (cp) gas
Komponen A B C D E
Nitrobenzen -16.202 0.56182 -3.9302E-04 1.004E-07 -1.2252E-12
Hidrogen 25.399 2.0178E-02 -3.8549E-05 3.1880E-08 -8.7585E-12
Anilin -22.062 0.57313 -4.5651E-04 1.841E-07 -2.9867E-11
Benzen -31.368 0.47460 -3.1137E-04 8.524E-08 -5.0524E-12
Nitrogen 29.342 -3.5395E-03 1.0076E-05 -4.3116E-09 2.5935E-13
Air 33.933 -8.4186E-03 2.9906E-05 -1.7825E-08 3.6934E-12
2. Viskositas gas
Komponen A B C
Nitrobenzen -16.569 2.92E-01 -2.5523E-05
Hidrogen 27.758 2.1200E-01 -3.2800E-05
Anilin -6.918 2.59E-01 -3.4348E-05
Benzen -0.151 2.57E-01 -8.9797E-06
Nitrogen 42.606 4.7500E-01 -9.8800E-05
Air -36.826 4.2900E-01 -1.6200E-05
3. Konduktivitas termal
Komponen A B C
Nitrobenzen -1.0283E-02 5.7531E-05 1.0851E-08
Hidrogen 0.040 4.5918E-04 -6.4933E-08
Anilin -0.01796 8.35E-05 1.5022E-09
Benzen -0.00565 3.45E-05 6.9298E-08
Nitrogen 0.00309 7.5930E-05 -1.1014E-08
Air 0.00053 4.7093E-05 4.9551E-08

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Neraca massa masing-masing alat

PENENTUAN JUMLAH STAGE

PERHITUNGAN BEBAN KOMPRESOR

T out 410.4858927 K 137.335892706 C

PENENTUAN KEBUTUHAN STEAM UNTUK TURBIN

internal eff. 30 % (Perry, tab 24.7)

N2 0.4000 11.2000 0.0008

Total 508.6590 1027.7180 1.0000

N2 0.4000 29.3973 11.7589

1260.00372519237 lb/hr GoalSeek

Hot Fluid Cold Fluid Diff.

Koreksi Nilai LMTD

A 385.692993698493 ft2 (Digunakan HE shell n tube karen

a" 0.3271 ft2 (Table 10)

Tube Side water

1.12 inch (Table 10)

hio 14.2044 BTU/jam.ft2.F

Mr xi, massa Data CP Gas

flowrate air pendingin > condensate 29.2134

Thermal Conductivity of Gas

3,276.0399 4,821.1643 k campuran

Berdasarkan tabel 7 Kern, digunakan steam dengan spesifikasi sebagai berikut :

Heat Capacity of Inorganic liq Cp (J/mol.K) = A + B*T + C*T^2 + D*T^3 + E*T^4

84.3238 J/mol.K Viscosity

Enthalpy of Evaporation 816 btu/lb (Table 7 Kern)

Hot Fluid Cold Fluid

Flow Area shell

-0.0035395 0.000010076 -4.3116E-09 2.5935E-13 29.397343002 1.0499051072

B C k, W/m.K x.k, W/m.K

0.00008 0.0000 6.2617E-02 4.924075509E-05

B*T + C*T^2 + D*T^3 + E*T^4 T (K)

inch 0.25 dari ID shell

-10.2158 1.79E+03 0.0177 -1.26E-05 0.152709066

0.00791717003 7.917170028578 0.086281

rho campuran 1.548875

HE-201 CD-201 KD-201

Komponen A B C D Tmin, K Tmax, K

Kapasitas panas gas

Konduktivitas termal liquid

Komponen A B C deltaHF 298

Konduktivitas termal GAS

log10 Pv = A + B/T + C log10T + DT + ET2

Total 134.5250 12548.4770 1.0000

Hot Fluid Cold Fluid Diff.

Koreksi Nilai LMTD

A 256.3864038082 ft2 (Digunakan HE shell and tube karena A >

a" 0.1963 ft2 (Table 10)

Tube Side (Cold Fluid)

0.606 inch (Table 10)

hio 429.8154 BTU/jam.ft2.F

v2/2g' 0.09 figure 27

Hot Fluid Cold Fluid

Mr xi, massa Data CP Liquid

flowrate air pendingin > condensate 241.2847 J/mol.K

Thermal Conductivity of liquid

Heat Capacity of Inorganic Gas Cp (J/mol.K) = A + B*T + C*T^2 + D*T^3 + E*T^4

34.9324 J/mol.K Viscosity

Enthalpy of Evaporation 835 btu/lb

Hot Fluid Cold Fluid Diff.

Flow Area shell

total 2.5867 241.2847

vity of liquid Viscosity

C k, W/m.K x.k, W/m.K Compound

Heat Capacity of Inorganic liq Cp (J/mol.K) = A + BT + CT^2 + DT^3 + ET^4

BT + CT^2 + DT^3 + ET^4 T (K)

Heat Capacity of Inorganic Gas Cp (J/mol.K) = A + BT + CT^2 + DT^3 + ET^4

DT^3 + ET^4 T (K)

Heat Capacity of Inorganic liq Cp (J/mol.K) = A + BT + CT^2 + DT^3 + ET^4

BT + CT^2 + DT^3 + ET^4 T (K)