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Bismillahirrohmannirrohim Neraca Massa

Kapasitas Pabrik =
1 Tahun Operasi Pabrik 330.000 hari
1 Hari Kerja 24.000 Jam
Kapasitas Produksi= 32000.000 ton/Tahun
Kapasitas Produksi = 4040.404 kg/jam 45.856

Kapasitas Bahan Baku


Etanol = 99% 0.990
Etanol
Air Air = 1% 0.010

Basis yg dipake = 1000.000 kmol/jam


Data Berat Molekul Masing2
komponen Rumus kimia berat molekul titik didih (K)
etil asetat CH3COOC2H5 88.110 77.100
air H2O 18.000 100.000
etanol CH3CH2OH 46.070 78.370
krotonaldehid C4H6O 70.090 102.000
Asetaldehid CH3CHO 44.050 20.200
Hidrogen H2 2.000 -252.900

N3
etil asetat 45.444
air 0.411
etanol 0.000
krotonaldehid 0.001

H2O 15.344 KG/JAM


ETANOL 3927.311 KG/JAM

REA
REA

Rumus kimia berat molekul titik didih (K) Input (kmol/jam)


etil asetat 88.110 77.100 0.000
air 18.000 100.000 0.852
etanol 46.070 78.370 85.247
krotonaldehid 70.090 102.000 0.000
Asetaldehid 44.050 20.200 0.000
Hidrogen 2.000 -252.900 0.000
TOTAL = 86.099

Neraca Massa kONDENSER 8.000

7.000
F7 3941.952
HIDROGEN 84.717
AIR 49.787
ETANOL 1975.858
ETIL ASETAT 1437.232
ASETALDEHID 260.241
KROTONALDEHID 134.116 9.000

komponen Rumus kimia berat molekul titik didih (K)


air 18.000 100.000
Asetaldehid 44.050 20.200
etanol 46.070 78.370
etil asetat 88.110 77.100
Hidrogen 2.000 -252.900
krotonaldehid 70.090 102.000
Total =

air 49.787
Asetaldehid 260.241
etanol 1975.858 FLARE
etil asetat 1437.232
Hidrogen 84.717
krotonaldehid 134.116

SEPARATOR DRUM

komponen Rumus kimia berat molekul titik didih (K)


air 18.000 100.000
Asetaldehid 44.050 20.200
etanol 46.070 78.370
etil asetat 88.110 77.100
Hidrogen 2.000 -252.900
krotonaldehid 70.090 102.000
Total =

Air 17.416
Etanol 1975.068
Etil Asetat 1436.513
Krotonaldehid 122.033

tangki
molecular sieve

menurut heuser 2019, kadar air yang terabsorbsi sebesar 0.771

komponen Rumus kimia berat molekul titik didih (K)


air 18.000 100.000
etanol 46.070 78.370
etil asetat 88.110 77.100
krotonaldehid 70.090 102.000
Total =
tangki molecular sleve
Air 13.433
Etanol 1975.068
Etil Asetat 1436.513
Krotonaldehid 122.033

produk atas
komponen Rumus kimia berat molekul titik didih (K)
air 18.000 100.000
etanol 46.070 78.370
etil asetat 88.110 77.100
krotonaldehid 70.090 102.000
Total =
T= 350.390 P sistem = 760.000
Rumus kimia A B C
ETANOL 23.844 -2864.200 -5.047
AIR 29.861 -3152.200 -7.304
etil asetat 0.696 -2249.800 5.464
krotonaldehid 34.317 -3113.800 -9.137

produk bawah
komponen Rumus kimia berat molekul titik didih (K)
air 18.000 100.000
etanol 46.070 78.370
etil asetat 88.110 77.100
krotonaldehid 70.090 102.000
Total =

T= 354.290 P sistem = 760.000


Rumus kimia A B C
Rumus kimia A B C

ETANOL 23.844 -2864.200 -5.047


AIR 29.861 -3152.200 -7.304
etil asetat 0.696 -2249.800 5.464
krotonaldehid 34.317 -3113.800 -9.137
Reaksi :

kmol/jam

Etanol
Summary Konversi Reaksi Mula-mula 85.247
Konversi Rx 1 15.40% Reaksi 13.129
Konversi Rx 2 30.31% Sisa 72.118
Konversi Rx 3
Konversi Rx 3 25.85% 2 Etanol
Konversi Rx 4 29.15% Mula-mula 72.118
Reaksi 25.836
Sisa 46.282

Etanol
Mula-mula 46.282
Reaksi 3.394
Sisa 42.888

2 asetaldehid
Mula-mula 9.735
Reaksi 3.827
Sisa 5.908

REAKTOR
REAKTOR

Input (kg/jam) Input (%) Output (kmol/jam) Output (kg/jam)


0.000 0.000 16.312 1437.232
15.344 0.004 2.766 49.787
3927.311 0.996 42.888 1975.858
0.000 0.000 1.913 134.116
0.000 0.000 5.908 260.241
0.000 0.000 42.358 84.717
3942.655 1.000 112.146 3941.952
3.943 3.942
1.000

F8 = 12.084 Fraksi Massa


air 32.372
Asetaldehid 260.241 komponen
etanol 0.790 air
etil asetat 0.719 asetaldehid
Hidrogen 84.717 etanol
krotonaldehid 12.084 134.116 etil asetat
F9= 122.033 hidrogen
Air 17.416 krotonaldehid
Etanol 1975.068 Total
Etil Asetat 1436.513
Krotonaldehid 122.033
1436.513
0.000

Input (Kg/Jam) Input (Kmol/jam) Input (%) Output (Kg/Jam)


F7 F7 F7 GAS
49.787 2.766 0.013 32.372
260.241 5.908 0.066 260.241
1975.858 42.888 0.501 0.790
1437.232 16.312 0.365 0.719
84.717 42.358 0.021 84.717
134.116 1.913 0.034 12.084
3941.952 112.146 390.922

air 32.372
Asetaldehid 260.241
etanol 0.790
etil asetat 0.719
Hidrogen 84.717
krotonaldehid 12.084
R DRUM
TANGKI MOLECULAR SLEVE
Air 17.416
Etanol 1975.068
Etil Asetat 1436.513
Krotonaldehid 122.033

Input (Kg/Jam) Input (Kmol/jam) Input (%) Output (Kg/Jam)


F7 F7 F7 FLARE
49.787 2.766 0.013 32.372
260.241 5.908 0.066 260.241
1975.858 42.888 0.501 0.790
1437.232 16.312 0.365 0.719
84.717 42.358 0.021 84.717
134.116 1.913 0.034 12.084
3941.952 112.146 390.922

Air 13.433
Etanol 1975.068
Etil Asetat 1436.513
Krotonaldehid 122.033

Diasumsi aja
99% air terjrap

Input (Kg/Jam) Output (Kg/Jam)


F7 F7
17.416 13.433 0.746
1975.068 1975.068 42.871
1436.513 1436.513 16.304
122.033 122.033 1.741
3551.030 3547.047 61.662
produk utama

Air 0.003
Etanol 1670.710
Etil Asetat 1215.147
Krotonaldehid 0.073 Distribusi Pemisahan Komponen Pada Fase Uap dan Cair (Heuser et al., 2019
komponen fraksi massa produk atas
air 0.001
etanol 0.846
etil asetat 0.846
krotonaldehid 0.001
Total 1.693

Coba pake persamaan ini

produk samping
𝐹= 𝐵+𝐷
Air
Etanol 𝑥_(𝑒𝑎, 𝑓) 𝐹=𝑥_(𝑒𝑎, 𝑏) 𝐵+𝑥_(𝑒𝑎,𝑑) 𝐷
3.980
304.358
Etil Asetat 221.367
Krotonaldehid 121.959 F= 3547.047
xea, f 40.50%
xea, d 99.10%
xea, b 33.97%
Input (Kg/Jam) Output (Kg/Jam) jumlah mol
F7 input (kg/mol) produk atas
3.983 0.221 0.003 0.000
1975.068 42.871 1670.710 36.265
1436.513 16.304 1215.147 13.791
122.033 1.741 0.073 0.001
3537.597 61.137 2885.933 50.057
P(ATM) 3.000
D E LOG P0 P0
0.000 0.000 2.861 725.969
0.000 0.000 2.501 317.271
-0.019 0.000 2.881 760.562
0.000 0.000 2.180 309.535

Input (Kg/Jam) Output (Kg/Jam) jumlah mol


F7 input (kg/mol) produk bawah
3.983 0.221 3.980 0.221
1975.068 42.871 304.358 6.606
1436.513 16.304 221.367 2.512
122.033 1.741 121.959 1.740
3537.597 61.137 651.664 11.080

P(ATM) 3.000
D E LOG P0 P0
D E LOG P0 P0

0.000 0.000 2.927 846.040


0.000 0.000 2.570 371.810
-0.019 0.000 2.936 863.371
0.000 0.000 2.234 309.535
𝑟_1=𝑋_1.𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙, 0)
𝑟_2=𝑋_2.𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙, 0)
𝑟_3=𝑋_3.𝑁_(𝐴𝑠𝑒𝑡𝑎𝑙𝑑𝑒ℎ𝑖𝑑, 0)

Asetaldehid Hidrogen

13.129 13.129 r1
13.129 13.129
578.314
Etil Asetat 2Hidrogen
13.129
12.918 25.836 r2
12.918 38.965

Asetaldehid Etil Asetat Hidrogen


13.129 12.918 38.965
3.394 3.394 3.394 r3
9.735 16.312 42.358

krotonaldehid Air
0.852
1.913 1.913 r4
1.913 2.766

HIDROGEN 84.717 KG/JAM


AIR 49.787 KG/JAM
ETANOL 1975.858 KG/JAM
ETIL ASETAT 1437.232 KG/JAM
ASETALDEHID 260.241 KG/JAM
KROTONALDEHID 134.116 KG/JAM
Output (%)
36.46%
1.26%
50.12%
3.40%
6.60%
2.15%
1.000

Ini namanya
fraksi massa gas y fraksi massa cair x total Split Fraction
0.650 0.350 1.000
1.000 0.000 1.000
0.000 1.000 1.000
0.001 1.000 1.000
1.000 0.000 1.000
0.090 0.910 1.000
2.741 3.259

Output (Kg/Jam) OUTPUT KG/MOL


OUTPUT KONDENSER OUTPUT (%)
CAIR
17.416 49.787 0.013 2.766
0.000 260.241 0.066 5.908
1975.068 1975.858 0.501 42.888
1436.513 1437.232 0.365 16.312
0.000 84.717 0.021 42.358
122.033 134.116 0.034 1.913
3551.030 3941.952 1.000 112.146
3941.952
Output (Kg/Jam)
TANGKI FLARE KG/MOL TANGKI
17.416 1.798 0.968
0.000 5.908 0.000
1975.068 0.017 42.871
1436.513 0.008 16.304
0.000 42.358 0.000
122.033 0.172 1.741
3551.030 50.262 61.883
3941.952
ap dan Cair (Heuser et al., 2019)
fraksi massa produk bawah total
0.999 1.000
0.154 1.000
0.154 1.000
0.999 1.000
2.307

3547.047 B + D
1436.513 82.35% B + 99.10% D

𝐵+𝑥_(𝑒𝑎,𝑑) 𝐷 x = 116355217/167500 ∧ y = 1001123711/335000


B 694.658
D 2988.429

fraksi mol (y) output % output produk atas kg/mol

0.000 0.000 0.000


0.724 0.579 36.265
0.276 0.421 13.791
0.000 0.000 0.001
50.057

a y
P ATM K
0.955 0.955 2.345 0.000
0.417 0.417 1.025 0.017
1.001 1.001 2.457 0.983
0.407 0.407 1.000 0.000

fraksi mol (y) output% output produk bawah kg/mol

0.004 0.006 0.221


0.132 0.467 6.606
0.050 0.340 2.512
0.035 0.187 1.740
11.080

a y
P ATM K
P ATM K

1.113 1.113 2.733 0.000


0.489 0.489 1.201 0.017
1.136 1.136 2.789 0.983
0.407 0.407 1.000 0.000
1 Konversi siapa dulu nih yang mau kita pake?
2 Berapa % konversi reaksi 1 dan 2

3.000 konversi asetaldehid menjadi Etil asetat = 55%*(100%-47)%


Konversi asetaldehid menjadi krotonaldehid (55%*53%)
produk akhir
etil asetat 0.991
air 0.009
etanol 0.000
𝑑, 0) krotonaldehid 0.000 menurut Yuni

𝑋_2=𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙 𝑑𝑖 𝑟𝑒𝑎𝑘𝑠𝑖 2)/𝑁_(𝑒𝑡

3927.310862 3927.310862
𝑋_1=52.12%
3322.4774981 578.31364620911 26.2571462524 3927.04829053748
𝑋_2=47.07%
3322.4774981 26.2571462524 3348.73464432837 𝑋_(𝑒𝑡ℎ, 𝑡𝑜𝑡𝑎𝑙)=𝑋_1+
2132.2077586 1138.20997121123 77.9293728424 3348.347103

Reaksi Parallel
2132.2077586 578.31364620911 1216.13934405363 3926.660749

1975.858334 428.819568664055 1521.94890881151 3926.626811


Reaksi Seri

428.81956866 15.344388 444.163957

260.241 134.116 49.787 444.144822


Etil Asetat Ethanol Air Krotonaldehid Total
572.05087283 1948.172 3.983 122.033 2646.239
2961.5331272 26.896 2988.429

Zi Ki xi yi

0.004 0.318
0.701 0.139
0.267 0.334
0.028 0.136
1.000

Zi Ki xi yi
0.701 0.371
0.267 0.163
0.028 0.379
1.000 0.136
1.996
Menurut Damar
𝑋_2=𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙
𝑑𝑖 𝑟𝑒𝑎𝑘𝑠𝑖 2)/𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙 𝑑𝑖 𝑟𝑒𝑎𝑘𝑠𝑖 1)
𝑠𝑖𝑠𝑎 2)/𝑁_(𝑒𝑡ℎ𝑎𝑛𝑜𝑙 𝑚𝑢𝑙𝑎−𝑚𝑢𝑙𝑎)

=52.12% 15.40% ..>


=47.07% X_2=47.07%
𝐾𝑜𝑛𝑣𝑒𝑟𝑠𝑖 𝑠𝑒𝑙𝑎𝑙𝑢 𝑑𝑖ℎ𝑖𝑡𝑢𝑛𝑔
𝑒𝑡ℎ, 𝑡𝑜𝑡𝑎𝑙)=𝑋_1+𝑋_2
3.98% ..>

Menurut yang dihitung Yuni

𝐴→𝐵 Menurut TA Orang lain


𝐴→𝐶 Pemahaman
Reaksi 1 15.40%
𝐴→𝐵 Reaksi 2 7.33%
𝐵→𝐶
Didapat dari referensi
Menggunakan asumsi?

𝑣𝑒𝑟𝑠𝑖 𝑠𝑒𝑙𝑎𝑙𝑢 𝑑𝑖ℎ𝑖𝑡𝑢𝑛𝑔 𝑑𝑎𝑟𝑖 𝑟𝑒𝑎𝑘𝑡𝑎𝑛 𝑚𝑢𝑙𝑎−𝑚𝑢𝑙𝑎

Didapat dari referensi


Menggunakan asumsi?
yang dihitung Yuni 7.33%

Menurut TA Orang lain Menurut Referensi


Setelah di-update
15.40% 44.90%
3.98% 41.62%

Ada di T.A tapi nggak ada di Heuser


Konversi reaksi
1. Cari di pengarang lain (Gaspar, Gadewar, Santacesaria)
2. Cari dari Konversi kesetimbangan equilibrium
Xeq Konversi kesetimbangan maksimum

Tabel Stoikiometri Reaksi 1


𝐸𝑡ℎ𝑎𝑛𝑜𝑙 → 𝐴𝑐𝑒𝑡𝑎𝑙𝑑𝑒ℎ𝑖𝑑+ 𝐻_2
m 85.247
b Xe1*(85.247) Xe1*(85.247) Xe1*(85.247) etil asetat
s 85.247*(1-Xe1) Xe1*(85.247) Xe1*(85.247) air
etanol
Keq= (produk)^(koef) krotonaldehid
(reaktan)^koef Asetaldehid
𝐾_(𝑒𝑞_1 )=([𝐴𝑐𝑒𝑡𝑎𝑙𝑑𝑒ℎ𝑖𝑑]^1.[𝐻_2 ]^1)/[𝐸𝑡ℎ𝑎𝑛𝑜𝑙]^1 Hidrogen
Total
Total
𝐾_(𝑒𝑞_1 )=([𝑋_(𝑒_1 ).(85.247)]^1.[𝑋_(𝑒_1 ).(85.247)]^1)/[(85.247).(1−𝑋_(𝑒_1 ))]^1

𝐾_(𝑒𝑞_1 )=exp⁡(𝐴+𝐵/𝑇)
𝐾_(𝑒𝑞_1 )=[𝑋_(𝑒_1 ).(85.247)]^2/[(85.247).(1−Dengan
𝑋_(𝑒_1 Keq1
))]^1=…1

𝐾_(𝑒𝑞_1 )=exp⁡〖
K_(eq_1 ) (16.5+"-9136.4"

Ini kalau Yuni dan teman-teman mau cari suhu optimum reaktor
T, C K Xe
200 0.060221 0.026
300 1.749485 0.133
400 18.678882 0.371 Di atas 350 C, sebaiknya gunakan

Tetapi tidak perlu dikasih tahu karena Author dari Paten sudah mencarikan suhu opera
Saat T= 200 C
Keq1 0.0599

Persamaan menjadi
0.0599=[𝑋_(𝑒_1 ).(85.247)]^2/[(85.247).(1−𝑋_( 𝑒_1 ))]^1
0.0599=𝐴𝑡𝑎𝑠/𝐵𝑎𝑤𝑎ℎ

Persamaan bisa diselesaikan secara aljabar


Misal, konversi Xe 0.54
54%

Konversi yang diinginkan 80-90% kesetimbangan


Faktor 0.087701411773476
Basis 46070 Basis 4040.404 kg/h
Masuk reaktor keluar reaktor Masuk reaktor keluar reaktor
kg/h kg/h kg/h kg/h
0 0
0 0
0 0
0 0
0 0
0 0
Total

_1 )=exp⁡(𝐴+𝐵/𝑇)

=exp⁡〖 (16.5+"-9136.4" /𝑇) …1 〗

s 350 C, sebaiknya gunakan Furnace

ah mencarikan suhu operasi reaktor

[𝑋_(𝑒_1 ).(85.247)]^2[(85.247).(1−𝑋_(𝑒_1 ))]^1


Xe Keq
0
0.1
0.2
0.371 1001.268326865 53.6041757444838 18.67892403827
0.4
0.5
0.6
Keq standar Selisih
0.0599

18.678882 4.20382736E-05
Selektivitas
Jenis proses Bahan Baku Katalis Kondisi Operasi Konversi Asetaldehid
PdO/m-ZrO2 + t-ZrO2 175 44.9 34.3
Cu-based 250 41.6
Cu dan Cu-Cr 65.0

(1) Konversi Etanol menjadi asetaldehid


(2) Konversi etanol langsung menjadi Etil Asetat

(3) Konversi Asetaldehid menjadi etil asetat


(4) Konversi asetaldehid menjadi krotonaldehid

4
Marking
Ea Asetat Produk Samping Referensi
67.5 Gaspar
Takeshita Reaksi 2
Santacesaria Reaksi 1

Konversi Selektivitas Total konv


asetaldehid 44.90% 34% 44.9%*34%
g menjadi Etil Asetat 44.90% 67.5% 44.9%*34%

enjadi etil asetat 55% 47% 55%*47%


njadi krotonaldehid 55% 53% 55%*53%

Mula2 20.1
Sisa 11.7
Reaksi 8.4

Konversi 41.62%
kapasitas panas fase cair
komponen A B C
etanol 59.342 3.64E-01 -1.22E-03
air 92.053 -4.00E-02 -2.11E-04
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

kapasitas panas fase gas


komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
air 33.933 -8.42E-03 2.99E-05
etanol 27.091 1.11E-01 1.10E-04
etil asetat 69.848 8.23E-02 -3.72E-04
asetaldehid 34.14 4.00E-02 1.56E-04
krotonaldehid 11.591 3.23E-01 -1.31E-04

vaporizer
tref 298

303
T1 30
etanol dan air Vaporixer
fasa cair 220 C, 1 atm

fase cair
Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
etanol 46.07 78.37 85.2406331938153
air 18 100 0.852406331938153
TOTAL = 86.0930395257535

fase gas
Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
etanol 46.07 78.37 85.2406331938153
air 18 100 0.852406331938153
TOTAL = 86.0930395257535

data untuk menghitung entalpi penguapan


komponen A Tc N
Etanol 43.122 516.25 0.079
Air 52.053 647.13 0.321

dari vaporizer
etanol 220 493 Reaktor
1 atm
air
fase gas masuk
Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
etanol 46.07 78.37 85.2406331938153
air 18 100 0.852406331938153

fase gas keluar


Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
Hidrogen 2 -252.9 0
air 18 100 0.852406331938153
etanol 46.07 78.37 85.2406331938153
etil asetat 88.11 77.1 0
asetaldehid 44.05 20.2 0
krotonaldehid 70.09 102 0

panas reaksi suhu 25 c


komponen mol ∆Hf (kj/mol) ∆Hf (kj/kmol)
Hidrogen 0.845587081282648 0 0
air 0.845587081282648 -241.8 -241800
etanol 0.845587081282648 -235 -235000
etil asetat 0.845587081282648 -334 -334000
asetaldehid 0.845587081282648 -166.2 -166200
krotonaldehid 0.845587081282648 -104 -104000

mol etanol awal 85.2406331938153


N 84.5587081282648

entalpi total
h in -2.20E+05
h out -3.05E+05
dq/dt -84671.4490094077

Q PENDINGIN -1282177.34960417
hidrogen, air, etanol, etil asetat
, asetaldehid, krotonaldehid fase gas
104 c
377 k

data untuk menhitung tekanan uap jenuh


1 ATM = 760 MMHG
Rumus kimia A B C
Hidrogen 3.4132 -4.13E+01 1.09E+00
air 29.8605 -3.15E+03 -7.30E+00
etanol 23.8442 -2.86E+03 -5.05E+00
etil asetat 0.6955 -2.25E+03 5.46E+00
asetaldehid 87.3702 -3.68E+03 -3.15E+01
krotonaldehid 34.3167 -3.11E+03 -9.14E+00

data masa vapor dalam kondesor


Rumus kimia berat molekul titik didih (K) massa
Hidrogen 2 -252.9 169.115266387631
air 18 100 20.087818466
etanol 46.07 78.37 0.012586324
etil asetat 88.11 77.1 1.76767676767677
asetaldehid 44.05 20.2 38.63185
krotonaldehid 70.09 102 10.836727044

K air 0.014731884878746

panas feed kondensor


T= 377
Rumus kimia berat molekul titik didih (K) Output (kG/jam)
Hidrogen 2 -252.9 169.115266387631
air 18 100 30.89483
etanol 46.07 78.37 31.46581
etil asetat 88.11 77.1 3535.35353535354
asetaldehid 44.05 20.2 38.63185
krotonaldehid 70.09 102 120.27444

T suhu pengembunan 35 308


DATA UNTUK MENGHITUNG ENTALPI PENGUAPAN
KOMPONEN A Tc N

etanol 43.122 516.25 0.079


etil asetat 49.346 523.3 0.385
krotonaldehid 52.2 571 0.375

qv 1.82E+06

kondensor keluar
T1 298 K
T2 296.5 K

komponen A B C
etanol 59.342 3.64E-01 -1.22E-03

etil asetat 62.832 8.41E-01 -2.70E-03


krotonaldehid 52.946 7.28E-01 -2.15E-03

komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
asetaldehid 34.14 4.00E-02 1.56E-04
Q LOSS 9.09E+04
Q PENDINGIN 3.72E+05

SEPARATOR DRUM

SEPARATOR
DRUM
SEPARATOR
DRUM
1 ATM

SEPARATOR DRUM : TANGKI SILINDER VERTIKAL


TUTUP BAGIAN ATAS : torispherical dished head
TUTUP BAGIAN BAWAHtorispherical
: dished head
inch m
td Tebal Tutup 0.3125 0.0079375
ID Diameter dalam shell 240 6.096
OD diameter luar shell 240.625 6.111875
b tinggi dish dalam 52.6619 1.33761226
sf straight flange 3 0.0762
phi 3.14
A lengkung 1.5708 D
A out 60.1396352648438
A in 59.8314158208

Konduktivitas Termal Steel Alloy SS-316 pada 2 Suhu Berbeda


T k (W/m.K)
100 16.2
500 21.4

pada suhu tetap 23.5 c


k 15.2055
Tabel 4.1-2 Geankoplis halaman 241 yaitu antara 1.100–2.800 W/m2 .K. Pada perancangan separator drum, diam
h in 1950
suhu udara (T1) 303 k
T2 trial 290 k
Tf 296.5

g.β.ρ.ρ μ.μ dilambangkan dengan x dan NPr pada Suhu Berbeda


Tk x (1.K.m^3) Npr
283.2 172000000 0.713
311 112000000 0.705
296.5 143294964.028777 0.709172661870504

L= 1.4217
NGr 5353011425.49605
Ngr x Npr 3796209361.64225
h out 2.89083291816805
q konveksi luar 2260.097285033 j/s 195272405.426851
q overall 2253.32166500331 j/s 194686991.856286
q loss 389959397.283137

T1 suhu ref 298


T2 suhu etanol out 296.5

Rumus kimia berat molekul Input (Kg/Jam) Input (Kmol/jam)


F7 F7
air 18 30.89489 1.71638277777778
Asetaldehid 44.05 38.6318500000002 0.877000000000005
etanol 46.07 31.74223 0.689
etil asetat 88.11 3535.352073 40.1243
Hidrogen 2 169.1152 84.5576
krotonaldehid 70.09 120.27444 1.716
3926.010683 129.680282777778
fasa cair
komponen A B C
etanol 59.342 3.64E-01 -1.22E-03
air 92.053 -4.00E-02 -2.11E-04
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

fasa gas
komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
asetaldehid 34.14 4.00E-02 1.56E-04

KOMPOSISI PRODUK KELUAR SEPARATOR MENUJU TANGKI MOLECULA


Output (Kg/Jam)
Rumus kimia berat molekul titik didih (K)
FLARE
air 18.000 100.000 20.087857478
Asetaldehid 44.050 20.200 38.6318500000002
etanol 46.070 78.370 0.012696892
etil asetat 88.110 77.100 1.7676760365
Hidrogen 2.000 -252.900 169.1152
krotonaldehid 70.090 102.000 10.836727044
240.4520074505

PERHITUNGAN Q KE TANGKI MOLECULAR SLEVE

Rumus kimia berat molekul titik didih (K)


TANGKI (KG/JAM)
air 18.000 100.000 10.807032522
Asetaldehid 44.050 20.200 0
etanol 46.070 78.370 31.729533108
etil asetat 88.110 77.100 3533.5843969635
Hidrogen 2.000 -252.900 0
krotonaldehid 70.090 102.000 109.437712956
3685.5586755495
fasa cair
komponen A B C
etanol 59.342 3.64E-01 -1.22E-03
air 92.053 -4.00E-02 -2.11E-04
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

PERHITUNGAN Q KE FLARE
Rumus kimia berat molekul titik didih (K)
FLARE
air 18.000 100.000 20.087857478
Asetaldehid 44.050 20.200 38.6318500000002
etanol 46.070 78.370 0.012696892
etil asetat 88.110 77.100 1.7676760365
Hidrogen 2.000 -252.900 169.1152
krotonaldehid 70.090 102.000 10.836727044
240.4520074505

fasa gas
komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
asetaldehid 34.14 4.00E-02 1.56E-04
air 33.933 -8.42E-03 2.99E-05
etanol 27.091 1.11E-01 1.10E-04
etil asetat 69.848 8.23E-02 -3.72E-04
krotonaldehid 11.591 3.23E-01 -1.31E-04

menara destilasi

Neraca Energy Menara


Destilasi 1
F11= #REF! Menara
Air 8.3354641842186 Destilasi 1
Etanol 31.729533108
Etil Asetat 3533.5843969635
Krotonaldehid 109.437712956

Komponen Rumus Kimia Berat Molekul Massa Masuk (Kg/Jam)


0 air 18.000 2.472
0 etanol 46.070 31.730
150 etil asetat 88.110 3533.584
4.69 krotonaldehid 70.090 109.438
3677.22321136528

#VALUE! T = 350.39
P= 1

Rumus Kimia A B
air 92.053 -4.00E-02
etanol 59.342 3.64E-01
etil asetat 62.832 8.41E-01
krotonaldehid 52.946 7.28E-01

komponen A B
air 29.8605 -3.15E+03
etanol 23.8442 -2.86E+03
etil asetat 0.6955 -2.25E+03
krotonaldehid 34.3167 -3.11E+03

Rumus Kimia Berat Molekul massa kg/jam


air 18.000 0.00173009783644698
etanol 46.070 26.8400120560572
etil asetat 88.110 2989.05904139142
krotonaldehid 70.090 0.0656626277736

trial titik didih


k krotonaldehid 0.406958654615391
sehingga trial cocok

panas hasil puncak kelua

#VALUE! T = 350.39
P= 1

Rumus Kimia Berat Molekul massa kg/jam


air 18.000 0.00173009783644698
etanol 46.070 26.8400120560572
etil asetat 88.110 2989.05904139142
krotonaldehid 70.090 0.0656626277736

Rumus Kimia A B
air 92.053 -4.00E-02
etanol 59.342 3.64E-01
etil asetat 62.832 8.41E-01
krotonaldehid 52.946 7.28E-01

panas hasil dasar keluar me

#VALUE! T = 354.29
P= 1

Rumus Kimia Berat Molekul massa kg/jam


air 18.000 2.46983823994495
etanol 46.070 4.8895210519428
etil asetat 88.110 544.525355572076
krotonaldehid 70.090 109.372050328226

Rumus Kimia A B
air 92.053 -4.00E-02
etanol 59.342 3.64E-01
etil asetat 62.832 8.41E-01
krotonaldehid 52.946 7.28E-01

q produk total 3.94E+05

PERHITUNGAN TRIAL TITIK EMBUN


trial T 78.08 351.08

komponen A B
air 29.8605 -3.15E+03
etanol 23.8442 -2.86E+03
etil asetat 0.6955 -2.25E+03
krotonaldehid 34.3167 -3.11E+03

KOMPOSISI FEED MASUK NE

Rumus Kimia Berat Molekul massa kg/jam


air 18.000 8.3354641842186
etanol 46.070 31.729533108
etil asetat 88.110 3533.5843969635
krotonaldehid 70.090 109.437712956

trial titik didih


k krotonaldehid 0.419581985653902
sehingga trial cocok

PERHITUNGAN TRIAL TITIK EMBUN


trial T 77.64 350.64

komponen A B
air 29.8605 -3.15E+03
etanol 23.8442 -2.86E+03
etil asetat 0.6955 -2.25E+03
krotonaldehid 34.3167 -3.11E+03

KOMPOSISI FEED MASUK NE

Rumus Kimia Berat Molekul massa kg/jam


air 18.000 8.3354641842186
etanol 46.070 31.729533108
etil asetat 88.110 3533.5843969635
krotonaldehid 70.090 109.437712956

trial titik didih


k krotonaldehid 0.418982369651358
sehingga trial cocok

DATA UNTUK MENGHITUNG ENT


T suhu pengembunan 23.5 296.5
DATA UNTUK MENGHITUNG ENTALPI PENGUAPAN
KOMPONEN A Tc
air 52.053 647.13
etanol 43.122 516.25
etil asetat 49.346 523.3
krotonaldehid 52.2 571

kapasitas panas feed menara destilasi


KOMPONEN kapasitas panas fraksi mol
air 75.1466 0.00456442246359704
etanol 114.9587 0.0154890779752694
etil asetat 183.619 0.945071625288388
krotonaldehid 159.4578 0.0149746391432281

q= 1.26836985625965
T AVG 352.34
PERHITUNGAN TRIAL TITIK EMBUN MENARA DESTILASI
trial T 352.34

komponen A B C
air 29.8605 -3.15E+03 -7.30E+00
etanol 23.8442 -2.86E+03 -5.05E+00
etil asetat 0.6955 -2.25E+03 5.46E+00
krotonaldehid 34.3167 -3.11E+03 -9.14E+00

1-q = -0.268369856259647
0.00080428040924
teta trial 1.01313
RM 0.707394916592251
ROP 1.06109237488838
L 0.001835793622065
V 0.006400216085662

KOMPONEN MASSA D MASSA L MASSA V


air 0.001730097836447 0.001835793622065 0.00356589145851175
etanol 26.8400120560572 28.4797321345944 55.3197441906516
etil asetat 2989.05904139142 3171.6677569116 6160.72679830303
krotonaldehid 0.0656626277736 0.069674113645701 0.135336741419301
TOTAL 3015.96644617309 3200.21899895346 6216.18544512655

Berat Molekul Rumus Kimia massa A


18.000 air 0.003565891458512 33.933
46.070 etanol 55.3197441906516 27.091
88.110 etil asetat 6160.72679830303 69.848
70.090 krotonaldehid 0.135336741419301 11.591

massa kmol KOMPONEN A Tc


0.0001981050810284 air 52.053 647.13
1.20077586695575 etanol 43.122 516.25
69.9208579991264 etil asetat 49.346 523.3
0.0019308994352875 krotonaldehid 52.2 571

qv 2.47E+06

Rumus Kimia A B C
air 92.053 -4.00E-02 -2.11E-04
etanol 59.342 3.64E-01 -1.22E-03
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

Q KONDENSOR 1.81E+06
Q REBOILER 2.29E+06
Q LOSS 1.16E+05
T1 81.299 354.299
T2 25 298
Rumus Kimia A B C
air 92.053 -4.00E-02 -2.11E-04
etanol 59.342 3.64E-01 -1.22E-03
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

Rumus Kimia Massa masuk KMOL/JAM


air 8.3354641842186 18 0.4630813435677
etanol 31.729533108 46.07 0.6887244
etil asetat 3533.5843969635 88.11 40.10423785
krotonaldehid 109.437712956 70.09 1.5613884

T1 30 303
T2 25 298
Rumus Kimia A B C
air 92.053 -4.00E-02 -2.11E-04
etanol 59.342 3.64E-01 -1.22E-03
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

Rumus Kimia Massa masuk Massa keluar atas Massa keluar bawah
air 8.3354641842186 18 0.4630813435677
etanol 31.729533108 46.07 0.6887244
etil asetat 3533.5843969635 88.11 40.10423785
krotonaldehid 109.437712956 70.09 1.5613884

q loss 2.47E+02
q pendingin =G624-G638 4270.63207098192

OIL HEATER
ALIRAN MASUK
273 T1 78 351
T2 220 493
T REF 25 298
Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
etanol 46.07 78.37 85.2406331938153
air 18 100 0.852406331938153
TOTAL = 86.0930395257535

ALIRAN KELUAR
273 T1 78 351
T2 220 493
T REF 25 298
Rumus kimia berat molekul titik didih (K) Input (kmol/jam)
etanol 46.07 78.37 85.2406331938153
air 18 100 0.852406331938153
TOTAL = 86.0930395257535

Q LOSS 15884.8568837877
Q PEMANAS 1026291.3079328

BOILER
ALIRAN MASUK
273 T1 220 493
T2 104 377
T REF 25 298

Rumus kimia berat molekul titik didih (K) Output (kG/jam)


Hidrogen 2 -252.9 169.115266387631
air 18 100 30.89483
etanol 46.07 78.37 31.46581
etil asetat 88.11 77.1 3535.35353535354
asetaldehid 44.05 20.2 38.63185
krotonaldehid 70.09 102 120.27444

ALIRAN KELUAR
273 T1 220 493
T2 104 377
T REF 25 298

Rumus kimia berat molekul titik didih (K) Output (kG/jam)


Hidrogen 2 -252.9 169.115266387631
air 18 100 30.89483
etanol 46.07 78.37 31.46581
etil asetat 88.11 77.1 3535.35353535354
asetaldehid 44.05 20.2 38.63185
krotonaldehid 70.09 102 120.27444

ENTALPI PENGUAPAN
DATA UNTUK MENGHITUNG ENTALPI PENGUAPAN
KOMPONEN A Tc N
air 52.053 647.13 0.321

Q LOSS 35269.1058950153
Q PENDINGIN 3645885.14119834

AFTER COOLER
ALIRAN MASUK
273 T1 35 308
T2 23.5 296.5
T REF 25 298
Rumus kimia berat molekul titik didih (K) Output (kG/jam)
Hidrogen 2 -252.9 169.115266387631
air 18 100 30.89483
etanol 46.07 78.37 31.46581
etil asetat 88.11 77.1 3535.35353535354
asetaldehid 44.05 20.2 38.63185
krotonaldehid 70.09 102 120.27444

komponen A B C
etanol 59.342 3.64E-01 -1.22E-03
air 92.053 -4.00E-02 -2.11E-04
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
asetaldehid 34.14 4.00E-02 1.56E-04

ALIRAN KELUAR
komponen A B C
etanol 59.342 3.64E-01 -1.22E-03
air 92.053 -4.00E-02 -2.11E-04
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

komponen A B C
Hidrogen 25.399 2.02E-02 -3.85E-05
asetaldehid 34.14 4.00E-02 1.56E-04
Q LOSS 4.92E+03
Q PENDINGIN 1.08E+05

HEATER 1

T1 30 303
T2 25 298
Rumus Kimia A B C
air 92.053 -4.00E-02 -2.11E-04
etanol 59.342 3.64E-01 -1.22E-03
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

Rumus Kimia Massa masuk KMOL/JAM


air 8.3354641842186 18 0.4630813435677
etanol 31.729533108 46.07 0.6887244
etil asetat 3533.5843969635 88.11 40.10423785
krotonaldehid 109.437712956 70.09 1.5613884

T1 78 351
T2 25 298
Rumus Kimia A B C
air 92.053 -4.00E-02 -2.11E-04
etanol 59.342 3.64E-01 -1.22E-03
etil asetat 62.832 8.41E-01 -2.70E-03
krotonaldehid 52.946 7.28E-01 -2.15E-03

Rumus Kimia Massa masuk KMOL/JAM


air 8.3354641842186 18 0.4630813435677
etanol 31.729533108 46.07 0.6887244
etil asetat 3533.5843969635 88.11 40.10423785
krotonaldehid 109.437712956 70.09 1.5613884

QLOSS 1.80E+03
Q PEMANAS 360453.283369856
D
1.80E-06
5.35E-07
3.66E-06
2.77E-06

D E
3.19E-08 -8.76E-12
-1.78E-08 3.69E-12
-1.50E-07 4.66E-11
-4.11E-07 1.24E-10
-1.64E-07 4.72E-11
1.08E-08 3.12E-12

vaporizer

351
T2 78
etanol dan air
fasa gas

Input (kg/jam) cp dt q feed


3927.03597123907 5.38E+02 4.59E+04
15.3433139748868 3.78E+02 3.22E+02
3942.37928521396 46216.2926491733

Input (kg/jam) cp dt q produk


3927.03597123907 3.70E+03 3.16E+05
15.3433139748868 1.79E+03 1.53E+03
3942.37928521396 317208.866334147
375.9 k
T suhu penguapan 77.9 c
∆Hv q penguapan q pemanas q loss
38.9056549777845 3316.342665126 2.90E+05 1.68E+04
39.3748481225404 33.56336985876 1.32E+03 8.21E+01
3349.906034985 2.91E+05 1.69E+04

reaktor

menuju kondenser
hidrogen
etanol t=
etil asetat
asetaldehid
krotonaldehid
air

Input (kg/jam) fraksi mol cp dt q feed


3927.03597123907 0.996108108108 1.55E+04 1.32E+06
15.3433139748868 0.003891891892 6.69E+03 5.70E+03
1.33E+06

Input (kg/jam) Input (%) Output (kmol/jam) Output (kg/jam)


0 0 84.5576331938154 169.115266387631
15.3433139748868 0.003891891892 1.716 30.89483
3927.03597123907 0.996108108108 0.683 31.46581
0 0 40.1243165969077 3535.35353535354
0 0 0.877 38.63185
0 0 1.716 120.27444

q
0 hin
-204462.956254144
-198712.964101422
-282426.085148404
-140536.572909176
-87941.0564533954
air, etanol, etil asetat, krotonaldehid (fase cair)
hidrogen dan asetaldehid (fasa gas)
35 c
308 k

D E LOG PO PO (mmHg)
-6.69E-10 1.46E-04 1.98E+01 6.96598229284912E+19
2.42E-09 1.81E-06 1.62E+00 41.885747495058
3.74E-11 2.74E-07 2.01E+00 102.351500698465
-1.95E-02 1.24E-05 2.17E+00 148.232349959474
2.01E-02 5.53E-13 3.10E+00 1262.75542546716
-4.24E-10 2.53E-06 1.71E+00 51.0847078034419

mol y y/a xi
84.5576331938154 0.975002333552 5.8625904909576E-19 1.06374340666917E-17
1.11598991477778 0.012868060872 0.0128680608719783 0.233485776130828
0.0002732 3.15016667E-06 1.28915633557158E-06 2.33912219222064E-05
0.0200621582984538 0.000231329218 6.53662794475129E-05 0.00118604478494675
0.877 0.010112357859 0.000335428111650889 0.00608620784157556
0.1546116 0.001782768333 0.00146174045933333 0.0265226912620911
86.7255700668916

cp dt q feed
2.28E+03 1.93E+05
2.68E+03 4.59E+03
5.66E+03 3.87E+03
3.22E+03 1.29E+05
4.72E+03 4.14E+03
8.38E+03 1.44E+04
3.49E+05

∆Hv (kj/mol) ∆Hv (kj/kmol) Q

40.1375783125009 40137.5783125 27413.9659874381


35.0553956424077 35055.39564241 1406573.79318583
39.0315113544529 39031.51135445 34230.6354578552
1468218.39463112

D Cp dt Q
1.80E-06 -1.61E+02 -1.36E+04

3.66E-06 -2.56E+02 -1.75E+02


2.77E-06 -2.28E+02 -9.13E+03
-22915.1208943228
D E Cp dt Q
3.19E-08 -8.76E-12 -4.31E+01 -3.65E+03
-1.64E-07 4.72E-11 -8.38E+01 -7.35E+01
ncangan separator drum, diambil hin di antara 1.100–2.800 W/m2 .K yaitu sebesar 1.950 W/m2 .K

j/hari
j/hari
j/hari

input (kmol/hari)

41.1931866666667
21.0480000000001
16.536
962.9832
2029.3824
41.184

D Cp dt Q
1.80E-06 -1.61E+02 -2.41E+00
5.35E-07 -1.13E+02 -1.08E+01
3.66E-06 -2.56E+02 -1.16E+02
2.77E-06 -2.28E+02 -5.57E+00
-1.35E+02

D E Cp dt Q
3.19E-08 -8.76E-12 -4.31E+01 -1.82E+03
-1.64E-07 4.72E-11 -8.38E+01 -1.67E+00
-1.83E+03
MENUJU TANGKI MOLECULAR SLEVE
Output (Kg/Jam)
TANGKI FLARE KG/MOL TANGKI
10.807032522 1.115992082111 0.600390695666667
0 0.877 0
31.729533108 0.0002756 0.6887244
3533.5843969635 0.02006215 40.10423785
0 84.5576 0
109.437712956 0.1546116 1.5613884
3685.5586755495 86.72554143211 42.9547413456667
3926.010683

TANGKI
0.600390695666667
0
0.6887244
40.10423785
0
1.5613884
42.9547413456667
air
D Cp dt Q
1.80E-06 -1.61E+02 -1.11E+02
5.35E-07 -1.13E+02 -6.81E+01
3.66E-06 -2.56E+02 -1.03E+04
2.77E-06 -2.28E+02 -3.55E+02
-10789.1968141759

FLARE KG/MOL
1.11599208211111
0.877000000000005
0.0002756
0.02006215
84.5576
0.1546116
86.7255414321111

fasa gas
D E Cp dt Q
3.19E-08 -8.76E-12 -4.31E+01 -3.65E+03
-1.64E-07 4.72E-11 -8.38E+01 -7.35E+01
-1.78E-08 3.69E-12 -5.05E+01 -5.63E+01
-1.50E-07 4.66E-11 -9.91E+01 0.0002756
-4.11E-07 1.24E-10 -7.75E+01 -1.55E+00
1.08E-08 3.12E-12 -1.45E+02 -2.23E+01
-3779.17412520601

F12 =
Air 0.00173009783644698 0.00173009783644698
Etanol 26.8400120560572 26.8400120560572
Etil Asetat 2989.05904139142 2989.05904139142
Krotonaldehid 0.0656626277736 0.0656626277736

Menara
Destilasi 1
F16= #REF!
Air 2.46983823994495
Etanol 4.8895210519428
Etil Asetat 544.525355572076
Krotonaldehid 109.372050328226

Massa Masuk (Kmol/Jam)Fraksi Umpan F distilat (Kg/Jam) N Distilat (Kmol/jam)


0.137309352098967 0.003231442408 0.00173009783644698 9.61165464692767E-05
0.6887244 0.016208460671 26.8400120560572 0.58259196996
40.10423785 0.943814335519 2989.05904139142 33.924174797315
1.5613884 0.036745761402 0.0656626277736 0.00093683304
42.491660002099 1 34.5077997168615

T1 SUHU REF 298


ATM T2 303

C D CP DT Q
-2.11E-04 5.35E-07 3.78E+02 5.18E+01
-1.22E-03 1.80E-06 5.38E+02 3.71E+02
-2.70E-03 3.66E-06 8.56E+02 3.43E+04
-2.15E-03 2.77E-06 7.62E+02 1.19E+03
35931.2336741027
C D E log po
-7.30E+00 2.42E-09 1.81E-06 2.50E+00
-5.05E+00 3.74E-11 2.74E-07 2.86E+00
5.46E+00 -1.95E-02 1.24E-05 2.88E+00
-9.14E+00 -4.24E-10 2.53E-06 2.49E+00

mol kmol/jam x x.a y


9.611654646928E-05 2.78535714E-06 2.85920064294614E-06 1.16348609172958E-06
0.58259196996 0.0168829069 0.0395565799728877 0.0160966425173368
33.924174797315 0.983087159299 2.41766549108666 0.983813493562816
0.00093683304 2.71484432E-05 2.71484431834765E-05 1.10474359797073E-05
34.5077997168615 2.45725207870338
panas hasil puncak keluar destilasi

T1 SUHU REF 298


ATM T2 303

mol kmol/jam
9.611654646928E-05
0.58259196996
33.924174797315
0.00093683304
34.5077997168615

C D CP DT Q
-2.11E-04 5.35E-07 3.94E+03 3.79E-01
-1.22E-03 1.80E-06 5.81E+03 3.39E+03
-2.70E-03 3.66E-06 9.26E+03 3.14E+05
-2.15E-03 2.77E-06 8.23E+03 7.71E+00
317489.186995161

panas hasil dasar keluar menara destilasi

T1 SUHU REF 298


ATM T2 303

mol kmol/jam
0.137213235552497
0.10613243004
6.180063052685
1.56045156696
7.9838602852375

C D CP DT Q
-2.11E-04 5.35E-07 4.23E+03 5.81E+02
-1.22E-03 1.80E-06 6.26E+03 6.64E+02
-2.70E-03 3.66E-06 9.98E+03 6.17E+04
-2.15E-03 2.77E-06 8.86E+03 1.38E+04
76733.701026213

HITUNGAN TRIAL TITIK EMBUN MENARA DESTILASI

C D E log po
-7.30E+00 2.42E-09 1.81E-06 2.51E+00
-5.05E+00 3.74E-11 2.74E-07 2.87E+00
5.46E+00 -1.95E-02 1.24E-05 2.89E+00
-9.14E+00 -4.24E-10 2.53E-06 2.50E+00

KOMPOSISI FEED MASUK NERASA DISTILASI

mol kmol/jam x x.a y


0.4630813435677 0.01081525262 0.0111386472822388 0.00464764880175718
0.6887244 0.016085140279 0.0377744012684225 0.0157615324683297
40.10423785 0.936633422014 2.29794520399712 0.95882758500584
1.5613884 0.036466185086 0.0364661850863583 0.0152156736026212
42.8174319935677 2.38332443763414

HITUNGAN TRIAL TITIK EMBUN MENARA DESTILASI

C D E log po
-7.30E+00 2.42E-09 1.81E-06 2.51E+00
-5.05E+00 3.74E-11 2.74E-07 2.86E+00
5.46E+00 -1.95E-02 1.24E-05 2.88E+00
-9.14E+00 -4.24E-10 2.53E-06 2.49E+00

KOMPOSISI FEED MASUK NERASA DISTILASI

mol kmol/jam x x.a y


0.4630813435677 0.01081525262 0.0111152644666655 0.00456442246359704
0.6887244 0.016085140279 0.0377189446009881 0.0154890779752694
40.10423785 0.936633422014 2.3014348778626 0.945071625288388
1.5613884 0.036466185086 0.0364661850863583 0.0149746391432281
42.8174319935677 2.38673527201661

ATA UNTUK MENGHITUNG ENTALPI PENGUAPAN

N Tb ∆Hv (kj/mol) ∆Hv (kj/kmol)


0.321 373.15 40.5275367138073
0.079 351.44 39.422352902384 39422.352902384
0.385 350.21 32.217635533293 32217.635533293
0.375 377.25 36.5419240308503 36541.9240308503

stilasi
cpl
0.343000829102942
1.7806042682356
173.533106763828
2.38782301357304
178.04453487474

MBUN MENARA DESTILASI

D E log po po
2.42E-09 1.81E-06 2.54E+00 343.841466050762
3.74E-11 2.74E-07 2.89E+00 782.620639527497
-1.95E-02 1.24E-05 2.91E+00 810.682586912397
-4.24E-10 2.53E-06 2.52E+00 331.863369962643

T1 298
350.39
B C D E
-8.42E-03 2.99E-05 -1.78E-08 3.69E-12
1.11E-01 1.10E-04 -1.50E-07 4.66E-11
8.23E-02 -3.72E-04 -4.11E-07 1.24E-10
3.23E-01 -1.31E-04 1.08E-08 3.12E-12

N Tb ∆Hv (kj/mol) ∆Hv (kj/kmol)


0.321 373.15 40.5275367138073 40527.5367138073
0.079 351.44 39.422352902384 39422.352902384
0.385 350.21 32.217635533293 32217.635533293
0.375 377.25 36.5419240308503 36541.9240308503

D HD (L+D)*HD
5.35E-07 3.94E+03 7.81E-01
1.80E-06 5.81E+03 6.98E+03
3.66E-06 9.26E+03 6.47E+05
2.77E-06 8.23E+03 1.59E+01
6.54E+05
D cp dt q Q KG/JAM
5.35E-07 4.23E+03 1.09E+02 3.53E+04
1.80E-06 6.26E+03 9.36E+01 1.99E+05
3.66E-06 9.98E+03 4.54E+03 3.53E+07
2.77E-06 8.86E+03 1.97E+02 9.70E+05
4941.96386574915 =SUM(H620:H623)
3.65E+07

D cp dt q Q KG/JAM
5.35E-07 3.78E+02 9.71E+00 3.15E+03
1.80E-06 5.38E+02 8.05E+00 1.71E+04
3.66E-06 8.56E+02 3.90E+02 3.02E+06
2.77E-06 7.62E+02 1.70E+01 8.33E+04
424.233601479764 3.04E+06

Q LOSS 1.82E+06
Q PENDINGIN 3.16E+07

Tambah
OIL HEATER
MASUK

Input (kg/jam) cp dt q
3927.03597123907 3703.42759573 315682.513247475
15.3433139748868 2363.455493929 2014.62442827885
3942.37928521396 317697.137675754

ELUAR

Input (kg/jam) cp dt q
3927.03597123907 15542.58153606 1324859.49159997
15.3433139748868 3805.810683527 3244.09712479636
3942.37928521396 1328103.58872477

ER
MASUK

OUTPUT(KMOL/JAM) CP DT Q
84.5576331938154 5670.403283794 479475.880932043
1.71637944444444 6690.025587944 11482.6224019547
0.683 15542.58153606 10615.5831891267
40.1243165969077 3805.810683527 152705.552773735
0.877 12757.60126876 11188.4163127067
1.716 23259.94305987 39914.0622907401
705382.117900305

ELUAR

OUTPUT(KMOL/JAM) CP DT Q
84.5576331938154 2284.969165951 193211.584593676
1.71637944444444 2675.602496886 4592.3491271592
0.683 5664.072343471 3868.56141059052
40.1243165969077 3218.325955265 129133.129541088
0.877 4720.834461304 4140.17182256334
1.716 8383.234419419 14385.6302637238
349331.4267588
GUAPAN

∆Hv (kj/mol) ∆Hv (kj/kmol) Q


39.3235173497626 39323.51734976 3325103.55595186

AFTER COOLER
MASUK
OUTPUT(KMOL/JAM)
84.5576331938154
1.71637944444444
0.683
40.1243165969077
0.877
1.716

D Cp dt Q
1.80E-06 1.08E+03 7.38E+02
5.35E-07 7.54E+02 1.29E+03
3.66E-06 1.72E+03 6.89E+04
2.77E-06 1.53E+03 2.62E+03
73542.0566723984
D E Cp dt Q
3.19E-08 -8.76E-12 2.88E+02 2.43E+04
-1.64E-07 4.72E-11 5.64E+02 4.95E+02
2.48E+04
ELUAR
D Cp dt Q
1.80E-06 -1.61E+02 -1.10E+02
5.35E-07 -1.13E+02 -1.95E+02
3.66E-06 -2.56E+02 -1.03E+04
2.77E-06 -2.28E+02 -3.91E+02
-10955.10763684
D E Cp dt Q
3.19E-08 -8.76E-12 -4.31E+01 -3.65E+03
-1.64E-07 4.72E-11 -8.38E+01 -7.35E+01
-3.72E+03

HEATER 1

D cp dt q
5.35E-07 3.78E+02 1.75E+02
1.80E-06 5.38E+02 3.71E+02
3.66E-06 8.56E+02 3.43E+04
2.77E-06 7.62E+02 1.19E+03
3.61E+04

D cp dt q
5.35E-07 3.99E+03 1.85E+03
1.80E-06 5.88E+03 4.05E+03
3.66E-06 9.37E+03 3.76E+05
2.77E-06 8.33E+03 1.30E+04
394704.78620699
komponen A B
air 92.053 -4.00E-02
etanol 59.342 3.64E-01
etil asetat 62.832 8.41E-01
krotonaldehid 52.946 7.28E-01

STEAM
KOMPONEN Q IN KG/JAM Q OUT KG/JAM DELTA HS
etanol 2.11E+06 1.45E+07 1.24E+07
air 5.79E+03 2.75E+04 2.17E+04
1.25E+07

High pressure steam


T 150 C 423
P 4.69 atm
Hv 2746.5 kJ/kg
HL 633.2 kJ/kg
λ 2113.3 kJ/kg

F steam = 5.89E+03 kg/jam

215 c 488 k
q loss
1.32E+05
5.70E+02
1.33E+05

Output (%) cp dt q out


4.3% 5.52E+03 4.67E+05
0.8% 6.51E+03 1.12E+04
0.8% 1.51E+04 1.03E+04
90.1% 3.91E+03 1.57E+05
1.0% 1.24E+04 1.09E+04
3.1% 2.26E+04 3.87E+04
694976.54849194
Cooling water
T CW in
T CW out
T ref

CW in
CW out

K a Q pendingin
9.16576617E+16 1.663091316126E+18 Q pendingin
0.055112825651 1 372246.548
0.134673027235 2.44358777912561 372246.547653123
0.195042565736 3.53896871428554 N CW
1.661520296667 30.1476158594555 F CW
0.067216720794 1.21962029708242
Q CW in
Q CW out
Fraksi Distilat F Bottom (Kg/Jam) N Bottom (Kmol/jam) Fraksi Bottom
2.78535714E-06 2.46983823994495 0.137213235552497 0.0171863272465089
0.0168829069 4.8895210519428 0.10613243004 0.0132933726603713
0.983087159299 544.525355572076 6.180063052685 0.774069539281919
2.71484432E-05 109.372050328226 1.56045156696 0.195450760811201
1 7.9838602852375 1

po k a
317.4635725191 0.417715226998836 1.02651132153031
724.6055661678 0.953428376536518 2.34299580078686
760.5615107828 1.00073882997733 2.45925853899884
309.2645603225 0.406927053055889 1
po k a
326.5955233139 0.429730951728854 1.02990172057724
744.7099912223 0.97988156739781 2.34840359570304
778.0087144844 1.02369567695311 2.45340935950717
317.1132903156 0.417254329362609 1

po k a
320.7471146617 0.422035677186393 1.0277396984411
731.8369039421 0.962943294660629 2.34495590009873
766.846899051 1.00900907769866 2.45713512220522
312.0898367049 0.410644521980173 1

fraksi mol ∆Hv total


0.004564422464 0
0.015489077975 610.615898073615
0.945071625288 30447.9731763982
0.014974639143 547.20212596124
0.98009976487 31605.791200433
k a xif xid
0.452422981646 1.03609345644103 0.00456442246359704 2.78535714412158E-06
1.029763999378 2.35826159306342 0.0154890779752694 0.0168829069004747
1.066687614358 2.44282032995583 0.945071625288388 0.983087159299198
0.436662328898 1 0.0149746391432281 2.71484431834765E-05

Cooling water
T CW in
T CW out
T ref
CP DT Q
1.77E+03 3.51E-01
3.66E+03 4.39E+03 CW in
2.34E+03 1.64E+05 CW out
5.39E+03 1.04E+01
1.68E+05 Q pendingin
q Q pendingin
8.028710944571 1813800.190
47337.4099838 1813800.18971264
2252684.719191 N CW
70.55878047549 F CW
2300100.716666
Q CW in
Q CW out

High pressure steam


T
P
Hv
HL
λ

F steam =
Cooling water
T CW in 32 C 305
T CW out 40 C 313
T ref 25 C 298

ΔH CW out
CW in 238.794269382667 C
CW out 512.29265166

Q pendingin = Q CW out
Q pendingin = ΔH CW out *
4270.632 = 512.29265166 *
4270.6320709819 = 273.498382277333 N CW
N CW = 15.6148348499239 kmol/jam
F CW = 281.067027298631 kg/jam

Q CW in = 3728.73307951859
Q CW out = 7999.36515050051

Tambahan Alat
Cooling water
T CW in 32 C 305
T CW out 40 C 313
T ref 25 C 298

ΔH CW out
CW in 238.794269382667 C
CW out 512.29265166

Q pendingin = Q CW out
Q pendingin = ΔH CW out *
3645885.141 = 512.29265166 *
3645885.1411984 = 273.498382277333 N CW
N CW = 13330.5546849683 kmol/jam
F CW = 239949.984329429 kg/jam

Q CW in = 3183260.06646268
Q CW out = 6829145.20766102

Cooling water
T CW in 32 C
T CW out 40 C
T ref 25 C

ΔH CW out
CW in 238.794269382667 C
CW out 512.29265166

Q pendingin = Q CW out
Q pendingin = ΔH CW out
108135.912 = 512.29265166
108135.91152543 = 273.498382277333
N CW = 395.380442929927
F CW = 7116.84797273868

Q CW in = 94414.583997647
Q CW out = 202550.495523077

T1 30
T2 25
STEAM
KOMPONEN Q IN KG/JAM Q OUT KG/JAM
air 3.15E+03 3.32E+04
etanol 1.71E+04 1.87E+05
etil asetat 3.02E+06 3.31E+07
krotonaldehid 8.33E+04 9.11E+05

High pressure steam


T 150 C
P 4.69 atm
Hv 2746.5 kJ/kg
HL 633.2 kJ/kg
λ 2113.3 kJ/kg
F steam = 1.47E+04 kg/jam
C D
-2.11E-04 5.35E-07
-1.22E-03 1.80E-06
-2.70E-03 3.66E-06
-2.15E-03 2.77E-06

K
Cooling water
T CW in 32 C 305 K
T CW out 40 C 313 K
T ref 25 C 298 K

ΔH CW out
CW in 238.794269382667 C
CW out 512.29265166

Q pendingin = Q CW out
Q pendingin = ΔH CW out * N CW
-1282177.350 = 512.29265166 * N CW
-1282177.34960417 = 273.4983822773 N CW
N CW = -4688.0619144 kmol/jam
F CW = -84385.1144592 kg/jam

Q CW in = -1119482.31967
Q CW out = -2401659.66927
32 C 305 K
40 C 313 K
25 C 298 K

ΔH CW out
238.794269382667 C
512.29265166

= Q CW out -
= ΔH CW out * N CW -
= 512.29265166 * N CW -
= 273.498382277333 N CW
= 1361.05575672348 kmol/jam
= 24499.0036210226 kg/jam

= 325012.315015856
= 697258.862668979
xif.a xid.a
0.00472916824696533 2.88589031087563E-06
0.0365272977010424 0.0398143109226549
2.30864017951887 2.40150529885461
0.0149746391432281 2.71484431834765E-05

KONDENSER

32 C 305 K
40 C 313 K
25 C 298 K

ΔH CW out
238.794269382667 C
512.29265166

= Q CW out -
= ΔH CW out * N CW -
= 512.29265166 * N CW -
= 273.498382277333 N CW
= 6631.84979234504 kmol/jam
= 119373.296262211 kg/jam

= 1583647.72581862
= 3397447.91553126
150 C 423 K
4.69 atm
2746.5 kJ/kg
633.2 kJ/kg
2113.3 kJ/kg

1.08E+03 kg/jam
K
K
K

ut - Q CW in
N CW - ΔH CW in * N CW
N CW - 238.7942693827 * N CW
K
K
K

ut - Q CW in
N CW - ΔH CW in * N CW
N CW - 238.7942693827 * N CW

305 K
313 K
298 K

Q CW out - Q CW in
* N CW - ΔH CW in *
* N CW - 238.79426938 *
N CW
kmol/jam
kg/jam

303
298

DELTA HS
3.01E+04
1.70E+05
3.01E+07
8.28E+05
3.11E+07

423 K
512.292652
238.794269
- Q CW in
- ΔH CW in * N CW
- 238.79426938267 * N CW
Q CW in
ΔH CW in * N CW
238.7942694 * N CW
Q CW in
ΔH CW in * N CW
238.7942694 * N CW
Q CW in
N CW
N CW

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