LAMPIRAN

PERHITUNGAN NERACA MASSA

NERACA MASSA OVERALL

F1
Gliserol 100% F5 Gliserol
Asam Asetat
Asam Asetat 98% F2
Air
Air 2% Triacetin

Kapasitas produksi : 3360,21505 kg/jam

Laju Alir Massa F1 : 489,17338 kg/jam
Laju Alir Massa F2 : 2870,8193 kg/jam
Laju Alir Massa F3 : 3359,8341 kg/jam
Suhu : 200C

Input Output
Komponen BM
Kg/jam Kmol/jam Kg/jam Kmol/jam
Gliserol 92,09 489,1733764 5,311905488 2,445866882 0,026559527
Asam Asetat 60,05 2813,402935 46,85100641 1861,24786 30,99496852
Air 18 57,41638642 3,189799246 342,8250683 19,04583713
Triacetin 218,21 0 0 1153,315342 5,285345961
Total Laju Alir 3359,99269782 55,352711144 3359,834137182 55,352711138

Komponen Selektivitas (%)

Monoacetin 20,1
Diacetin 27,1
Triacetin 52,8

Reaksi Keseluruhan:
Gliserol + 3 Asam Asetat Triacetin + 3 Air
Awal : 5,311905488 46,85100641 0 3,189799246

Reaksi : 5,285345961 15,85603788 5,285345961 15,85603788

Sisa : 0,026559527 30,99496852 5,285345961 19,04583713

 NERACA MASSA REAKTOR 1

F1
Gliserol 100% F3 Gliserol
Asam Asetat
Asam Asetat 98% F2
Air
Air 2% Monoacetin

Laju Alir Massa F1 : 3419,966639 kg/jam

Laju Alir Massa F2 : 3360,158801 kg/jam
Laju Alir Massa F3 : 3359,8341 kg/jam
Suhu : 200C

Input Output
Komponen BM
Kg/jam Kmol/jam Kg/jam Kmol/jam
Gliserol 92,09 489,1733764 5,311905488 320,2043053 3,477080088
Asam Asetat 60,05 2813,402935 46,85100641 2723,637697 45,35616482
Air 18 57,41638642 3,189799246 84,41722784 4,684640835
Monoacetin 218,21 0 0 291,7071595 2,174809211
Total Laju Alir 3360,15880106 55,352711144 3360,15880106 55,352711148

Reaksi Nilai
r1 0,169991905
r2 0,169991905
r3 5,285345961
 NERACA MASSA REAKTOR 2

Gliserol F3 F4 Gliserol
Asam Asetat Asam Asetat
Air Air
Monoacetin Diacetin

Laju Alir Massa F3 : 3419,966639 kg/jam

Laju Alir Massa F4 : 3360,158801 kg/jam
Suhu : 200C

Input Output
Komponen BM
Kg/jam Kmol/jam Kg/jam Kmol/jam
Gliserol 92,09 320,2043053 3,477080088 18,10042146 0,196551433
Asam Asetat 60,05 2723,637697 45,35616482 2199,048913 36,6202983
Air 18 84,41722784 4,684640835 241,8375426 13,42050736
Monoacetin 218,21 291,7071595 2,174809211 0 0
Diacetin 176,17 0 0 901,171924 5,115354055
Total Laju Alir 3360,15880106 55,352711148 3360,15880106 55,352711148

Reaksi Nilai
r1 0,169991905
r2 0,169991905
r3 5,285345961
 NERACA MASSA REAKTOR 3

Gliserol F6 Gliserol
F5
Asam Asetat Asam Asetat
Air Air
Diacetin Triacetin

Laju Alir Massa F5 : 489,17338 kg/jam

Laju Alir Massa F6 : 2870,8193 kg/jam
Suhu : 200C
Input Output
Komponen BM
Kg/jam Kmol/jam Kg/jam Kmol/jam
Gliserol 92,09 18,10042146 0,196551433 2,445866882 0,026559527
Asam Asetat 60,05 2199,048913 36,6202983 1861,24786 30,99496852
Air 18 241,8375426 13,42050736 343,2059851 19,04583713
Triacetin 218,21 0 0 1153,315342 5,285345961
Diacetin 176,17 901,171924 5,115354055 0 0
Total Laju Alir 3360,15880106 55,352711148 3360,215053982 55,352711138

Reaksi Nilai
r1 0,169991905
r2 0,169991905
r3 5,285345961
 NERACA MASSA MENARA DISTILASI 1

F7
Asam Asetat
Air

Gliserol F6
Asam Asetat
Air
Triacetin

F8
Gliserol
Triacetin

Kondisi Proses
Suhu
Tekanan (Psig) Tekanan Total (Kpa)
C K
200 473,15 150 1034,25

Konstanta Antoine
Komponen A B C P Ki
Gliserol 18,3036 3816,4400 -46,1300 11686,8554 11,2998
Asam Asetat 16,8080 3405,3700 -30,3400 9114,6308 8,8128
Air 16,0477 2921,5200 -55,1500 8590,5471 8,3061
Triacetin 17,2312 4487,0400 -14,0200 42,7164 0,0413
Total 29434,7497 28,4600

Penentuan Dew Point

T dew : 102,7485 C
Komponen Xd Psat Ki Alfa yi/alfa xi
Air 0,8443 1032,0019 0,9978 0,9860 0,8563 0,8462
As. Asetat 0,1557 1046,6146 1,0120 1,0000 0,1557 0,1538
Penentuan Bubble Point
T bubble : 176,4231 C
Komponen Xw Psat Ki Alfa xi.alfa yi
Gliserol 0,0021 6932,1589 6,7026 1,0000 0,0021 0,0142
Triacetin 0,9979 1021,7421 0,9879 0,1474 0,1471 0,9858

Laju Alir Input (F6) Laju Alir Output (F7) Laju Alir Output (F8)
Komponen
Kg/jam Kmol/jam Kg/jam Kmol/jam Kg/jam Kmol/jam
Gliserol 2,4456 0,0266 0 0 2,4456 0,0266
Asam Asetat 1861,0369 30,9915 1861,0369 30,9915 0 0
Air 343,1671 19,0437 343,1671 19,0437 0 0
Triacetin 1153,1846 5,2847 0 0 1153,1846 5,2847
Total 3359,8341 55,3464 2204,2039 50,0352 1155,6302 5,3113
 NERACA MASSA MENARA DISTILASI 2

F8
Air

Asam Asetat F7
Air

F9
Asam Asetat

Laju Alir Input F7 : 3359,8341kg/jam

Laju Alir Output F8 : 343,1670789 kg/jam
Laju Alir Output F9 : 1861,0369 kg/jam
Suhu : 115C
Laju Alir Input (F7) Laju Alir Output (F8) Laju Alir Output (F9)
Komponen
Kg/jam Kmol/jam Kg/jam Kmol/jam Kg/jam Kmol/jam
Asam Asetat 1861,03687 30,9915 0 0 1861,0369 30,9915
Air 343,167079 19,0437 343,1670789 19,0437 0 0
Total 3359,8341 55,3464 343,1670789 19,0437 1861,0369 30,9915